• Title/Summary/Keyword: Cold pressing

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Extrusion of CP Grade Titanium Powders Eliminating the need for Hot Pre-compaction via Hot Isostatic Pressing

  • Wilson, Robert;Stone, Nigel;Gibson, Mark
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1273-1274
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    • 2006
  • Chemically pure, hydride/dehydride titanium powders were cold pre-compacted then extruded at $850^{\circ}C$ and $\sim450MPa$ under argon. The extrusions were 100% dense with a narrow band of surface porosity and equiaxed microstructure of similar magnitude to the starting material. The tensile properties of the bars were better than conventionally extruded CP titanium bar product. Outcomes from this study have assisted in the identification of a number of key characteristics important to the extrusion of titanium from pre-compacted CP titanium powders, allowing the elimination of canning and hot isostatic pressing (HIPping) of billets prior to extrusion as per conventional PM processes.

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Comparison of the Cold-Pressed Peel Oil Composition between ]Korean and Japanese Satsuma Mandarin (Citrus unshiu Marcov. forma Miyagawa-wase) by GC, GC-MS and GC-O

  • Park, Hyang-Sook;Sawamura, Masayoshi
    • Preventive Nutrition and Food Science
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    • v.7 no.1
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    • pp.5-11
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    • 2002
  • The comparison of the volatile flavor components from Korean and Japanese Satsuma mandarin (C. unshiu Marcov. forma Miyagawa-wase) peel oils, isolated by cold-pressing, was performed by gas chromatography, mass-spectrometry and gas chromatography-olfactometry (GC-O). Eighty-five volatile components were identified in each oil by GC and GC-MS. Forty-three components were detected in each oil by GC-O. The total amount of monoterpene hydrocarbons was 95.88% (Korean mandarin) and 95.29% (Japanese mandarin). Limonene, ${\gamma}$-terpinene, myrcene and $\alpha$-pinene were the main components of the cold-pressed oils from the both samples. The volatile composition of the Japanese mandarin was characterized by a higher content of sesquiterpene hydrocarbons, especially bicyclogermacrene, $\alpha$-humullene and valencene. The volatile composition of two samples can easily be distinguished by the percentages of aldehydes, ketones and esters, which were found at higher levels in the Japanese mandarin. The sweet and fruity flavor was stronger in the Korean mandarin oil while herbaceous flavor was stronger in Japanese sample. From GC-O data it is suggested that the sweet and fruity flavor of the Korean mandarin resulted from terpinolene and linalool, and the herbaceous note of the Japanese mandarin from $\alpha$-humullene, nepal, ι-carvone and perill aldehyde.

Phenol-Formaldehyde (PF) Resin Bonded Medium Density Fiberboard

  • Park, Byung-Dae;Riedl, Bernard;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.27 no.1
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    • pp.64-71
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    • 1999
  • This study was conducted to manufacture MDF panels bonded with PF resins which provide excellent durability and dimensional stability with panels, and to identify benefits and weaknesses of using PF resins for MDF panels that have been manufactured with urea-formaldehyde (UF) resins for interior applications due to its low dimensional stability under moisture conditions. The results showed that the performance of PF-bonded MDF panels satisfied the performance requirement. A six-cycle aging test also revealed that PF-bonded MDF panels had high durability. Thickness swelling after 24 hours submersion in cold water was less than 2 percent, showing good dimentioanl stability. The identified weaknesses of using PF resins were relatively high resin content and long hot-pressing time. An acceptable resin content appeared to be 8 percent which can increase the production cost of PF-bonded MDF panels. The hot-pressing time (7 minutes) used in this study is relatively long compared to that of UF-bonded MDF panels. This result also indicates that hot-pressing process has to be optimized to control various pressing variables.

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Water Soluble Type의 Cold Strip Rolling Oil

  • 김주항
    • Tribology and Lubricants
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    • v.5 no.2
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    • pp.21-31
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    • 1989
  • 최근 국내에서도 각종 공작기계 가공의 발전으로 말미암아 이에 쓰여지고 있는 윤활제의 이용범위도 점진적으로 확대되어 가고 있음은 물론 특히 Water계 윤활제의 요구성능은 점점 가혹하게 되어지고 있다. Water계 윤활제라고 하면 일반적으로 Cutting, Grinding, Drawing, Pressing, Heat Treating 등의 공작기계 계통의 Oil을 연상할 수 있겠지만 이들 이외에 각종 유압작동유를 비롯하여 Rolling Oil도 포함되고 있다. 따라서 본 논고에서는 근간 Crose up 되어지고 있는 Water계 윤활제 중 냉각압연유에 대하여 간략하게 기술하여 보고자 한다.

Effect of Cobalt to Bronze Ratio on Transverse Rupture Strength of Diamond Segments

  • Unal, Rahmi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1146-1147
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    • 2006
  • Diamond segments were fabricated by cold pressing and sintering under pressure at the temperature up to $750^{\circ}C$. Based on the results of this investigation, it can be concluded that the segments containing 39wt.% cobalt in the matrix material have the highest bending strength at a fracture probability of 50 % due to the weibull distribution method. According to the weibull statistics, it was also determined that the transverse rupture strength was the best for 39 wt.% cobalt ratio in the matrix material for the fracture probability when the other variables are the same.

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Fabrication of a Complex-Shaped Silicon Nitride Part with Aligned Whisker Seeds Using LOM Technique

  • Park, Dong-Soo;Cho, Byung-Wook
    • Journal of the Korean Ceramic Society
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    • v.40 no.10
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    • pp.931-935
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    • 2003
  • A complex-shaped part was successfully fabricated by Laminate Object Manufacturing (LOM) technique using silicon nitride tape with aligned silicon nitride whisker seeds. The ceramic tape was cut using a commercial cutting plotter according to the cross section drafts generated by slicing a 3-D model, and then the tapes were stacked sequentially. In order to improve adhesion between the tapes, stacking was performed under vacuum. After binder burnout, the part was encapsulated using latex emulsion and was cold isostaically pressed under 250 ㎫. It was sintered to 98.5% TD at 2148 K for 4 h under 2 ㎫ nitrogen pressure.

Numerical Simulation of Cold Compaction of 3D Granular Packings

  • Chen, Yuan;Imbault, Didier;Doremus, Pierre
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.189-190
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    • 2006
  • During cold compaction processes loose powder is pressed under tooling action in order to produce complex shaped engineering components. Here, the analysis of the plastic deformation of granular packings is of fundamental importance to the development of computer simulation models. Powders can be idealized by packing discrete particles, where each particle is a sphere meshed with finite elements. The pressing of a body centered cubic packing was compared with numerical prediction and experimental data. The global response was expressed in force-displacement curve, and the accuracy of the numerical models analyzed for high relative densities up to 0.95.

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Optimization of powder compaction parameters for the pressureless sintered ZTA (상압소결 ZTA의 분말 성형 공정 최적화)

  • 신동우;김경도;박삼식;임창성;이수완
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.2
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    • pp.356-364
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    • 1998
  • The dependence of green and sintered densities of Zirconia-Toughened Alumina ($ZTA:\;Al_2O_3/\;15\;vol{%}\;ZrO_2$) on the properties of spray-dried granules was studied thoroughly to establish the optimum compaction condition leading to high reproducibility in the light of sintered density. The sphericity, mean size, degree of hollow occurrence and moisture content of spray-dried granules were largely different in between the granule containing binder and the ones with no binder. The effect of these differences in the characteristic of granules on the compaction behavior was examined in terms of the compaction pressure from 80 MPa to 120 MPa 10 MPa increment and the compaction method, i.e., uniaxial and cold isostatic pressing. This work confirmed that the reproducibility of sintered density caused by the variation of granule property could be improved by the optimization of compaction process. The variation of sintered density was controlled within 1 % deviation by compacting the granules under a relatively low pressure of 80 MPa in an uniaxial forming and subsequent cold isostatic pressing at high pressure of 500 MPa.

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Importance of Green Density of Nanoparticle Precursor Film in Microstructural Development and Photovoltaic Properties of CuInSe2 Thin Films

  • Hwang, Yoonjung;Lim, Ye Seul;Lee, Byung-Seok;Park, Young-Il;Lee, Doh-Kwon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.471.2-471.2
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    • 2014
  • We demonstrate here that an improvement in precursor film density (green density) leads to a great enhancement in the photovoltaic performance of CuInSe2 (CISe) thin film solar cells fabricated with Cu-In nanoparticle precursor films via chemical solution deposition. A cold-isostatic pressing (CIP) technique was applied to uniformly compress the precursor film over the entire surface (measuring 3~4 cm2) and was found to increase its relative density (particle packing density) by ca. 20%, which resulted in an appreciable improvement in the microstructural features of the sintered CISe film in terms of lower porosity, reduced grain boundaries, and a more uniform surface morphology. The low-bandgap (Eg=1.0 eV) CISe PV devices with the CIP-treated film exhibited greatly enhanced open-circuit voltage (VOC, from 0.265 V to 0.413 V) and fill factor (FF, from 0.34 to 0.55), as compared to the control devices. As a consequence, an almost 3-fold increase in the average power conversion efficiency, 3.0 to 8.2% (with the highest value of 9.02%), was realized without an anti-reflection coating. A diode analysis revealed that the enhanced VOC and FF were essentially attributed to the reduced reverse saturation current density (j0) and diode ideality factor (n). This is associated with the suppressed recombination, likely due to the reduction in recombination sites such as grain/air surfaces (pores), inter-granular interfaces, and defective CISe/CdS junctions in the CIP-treated device. From the temperature dependences of VOC, it was confirmed that the CIP-treated devices suffer less from interface recombination.

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Antioxidant and Antimicrobial Activities of Camellia Oleifera Seed Oils

  • Zhou, Qing-Fen;Jia, Xue-Jing;Li, Qian-Qian;Yang, Rui-Wu;Zhang, Li;Zhou, Yong-Hong;Ding, Chun-Bang
    • Journal of Applied Biological Chemistry
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    • v.57 no.2
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    • pp.123-129
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    • 2014
  • The antioxidant and antimicrobial activities of Camellia oleifera seed oil were studied. Four kinds of seed oil samples were prepared, crude oil and refined oil, extracted by cold pressing method (CPC, CPR), and organic solvent extraction (OSC, OSR). Antioxidant activity analysis was measured in 2,2-azinobis (3-ethylbenzothiazoline-6-sulfonic acid)-diammonium salt, ferric reducing Ability of Plasma, and 2,2-diphenyl-1-picrylhydrazyl assays. Besides, the percentage of inhibition of red blood cells hemolysis induced by 2,2'-azobis(2-amidnopropane) dihydrochlorid, the lag time of LDL conjugated dienes formation in vitro, and the inhibitors of loss in tryptophan fluorescence were all used to estimate the antioxidant activity of the samples. The total phenolic contents (TPC) were detemined by Folin-Ciocalteu method. The TPC of the C. oleifera seed oils can be arranged in descending order: CPC ($1.9172{\mu}g/mL$) > OSC ($1.5218{\mu}g/mL$) > CPR ($1.0611{\mu}g/mL$) > OSR ($0.6782{\mu}g/mL$). And the oils were investigated for activity against Escherichia coli, Bacillus subtilis, Saccharomyces cerevisiae and Aspergillus niger. The results showed the antioxidant activity of crude oil by cold pressing method was stronger than others, and all oils did inhibit activity of the top three bacteria expert A. niger. The further significance of the study contributes to measure the antioxidant and antimicrobial activity of the potential health benefits by the different methods of preparation and the oil of C. oleifera seeds acting as free radical scavenger, pharmaceuticals and preservatives may offer some information in medicine and cosmetic not just in food field.