• Title/Summary/Keyword: Bond strengths

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Evaluation of shear bond strength of repair acrylic resin to Co-Cr alloy

  • Kulunk, Safak;Kulunk, Tolga;Sarac, Duygu;Cengiz, Seda;Baba, Seniha
    • The Journal of Advanced Prosthodontics
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    • v.6 no.4
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    • pp.272-277
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    • 2014
  • PURPOSE. The purpose of this study was to investigate the impact of different surface treatment methods and thermal ageing on the bond strength of autopolymerizing acrylic resin to Co-Cr. MATERIALS AND METHODS. Co-Cr alloy specimens were divided into five groups according to the surface conditioning methods. C: No treatment; SP: flamed with the Silano-Pen device; K: airborne particle abrasion with $Al_2O_3$; Co: airborne particle abrasion with silica-coated $Al_2O_3$; KSP: flamed with the Silano-Pen device after the group K experimental protocol. Then, autopolymerized acrylic resin was applied to the treated specimen surfaces. All the groups were divided into two subgroups with the thermal cycle and water storage to determine the durability of the bond. The bond strength test was applied in an universal test machine and treated Co-Cr alloys were analyzed by scanning electron microscope (SEM). Two-way analysis of variance (ANOVA) was used to determine the significant differences among surface treatments and thermocycling. Their interactons were followed by a multiple comparison' test performed uing a post hoc Tukey HSD test (${\alpha}=.05$). RESULTS. Surface treatments significantly increased repair strengths of repair resin to Co-Cr alloy. The repair strengths of Group K, and Co significantly decreased after 6,000 cycles (P<.001). CONCLUSION. Thermocycling lead to a significant decrease in shear bond strength for air abrasion with silica-coated aluminum oxide particles. On the contrary, flaming with Silano-Pen did not cause a significant reduction in adhesion after thermocycling.

Tensile bond strength between auto-polymerized acrylic resin and acrylic denture teeth treated with MF-MA solution

  • Thongrakard, Ticha;Wiwatwarrapan, Chairat
    • The Journal of Advanced Prosthodontics
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    • v.8 no.4
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    • pp.285-289
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    • 2016
  • PURPOSE. This study evaluated the effect of chemical surface treatment using methyl formate-methyl acetate (MF-MA) solution on the tensile bond strength between acrylic denture teeth and auto-polymerized acrylic resin. MATERIALS AND METHODS. Seventy maxillary central incisor acrylic denture teeth for each of three different brands (Yamahachi New Ace; Major Dent; Cosmo HXL) were embedded with incisal edge downwards in auto-polymerized resin in polyethylene pipes and ground with silicone carbide paper on their ridge lap surfaces. The teeth of each brand were divided into seven groups (n=10): no surface treatment (control group), MF-MA solution at a ratio of 25:75 (v/v) for 15 seconds, 30 seconds, 60 seconds, 120 seconds, 180 seconds, and MMA for 180 seconds. Auto-polymerized acrylic resin (Unifast Trad) was applied to the ground surface and polymerized in a pressure cooker. A tensile strength test was performed with a universal testing machine. Statistical analysis of the results was performed using two-way analysis of variance (ANOVA) and post-hoc Dunnett T3 test (${\alpha}$=.05). RESULTS. The surface treatment groups had significantly higher mean tensile bond strengths compared with the control group (P<.05) when compared within the same brand. Among the surface treatment groups of each brand, there were no significantly different tensile bond strengths between the MF-MA groups and the MMA 180 second group (P>.05), except for the Yamahachi New Ace MF-MA 180-second group (P<.05). CONCLUSION. 15-second MF-MA solution can be an alternative chemical surface treatment for repairing a denture base and rebonding acrylic denture teeth with auto-polymerized acrylic resin, for both conventional and cross-linked teeth.

Bracket bonding to polymethylmethacrylate-based materials for computer-aided design/manufacture of temporary restorations: Influence of mechanical treatment and chemical treatment with universal adhesives

  • Goracci, Cecilia;Ozcan, Mutlu;Franchi, Lorenzo;Di Bello, Giuseppe;Louca, Chris;Vichi, Alessandro
    • The korean journal of orthodontics
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    • v.49 no.6
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    • pp.404-412
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    • 2019
  • Objective: To assess shear bond strength and failure mode (Adhesive Remnant Index, ARI) of orthodontic brackets bonded to polymethylmethacrylate (PMMA) blocks for computer-aided design/manufacture (CAD/CAM) fabrication of temporary restorations, following substrate chemical or mechanical treatment. Methods: Two types of PMMA blocks were tested: $CAD-Temp^{(R)}$ (VITA) and $Telio^{(R)}$ CAD (Ivoclar-Vivadent). The substrate was roughened with 320-grit sandpaper, simulating a fine-grit diamond bur. Two universal adhesives, Scotchbond Universal Adhesive (SU) and Assure Plus (AP), and a conventional adhesive, Transbond XT Primer (XTP; control), were used in combination with Transbond XT Paste to bond the brackets. Six experimental groups were formed: (1) $CAD-Temp^{(R)}/SU$; (2) $CAD-Temp^{(R)}/AP$; (3) $CAD-Temp^{(R)}/XTP$; (4) $Telio^{(R)}$ CAD/SU; (5) $Telio^{(R)}$ CAD/AP; (6) $Telio^{(R)}$ CAD/XTP. Shear bond strength and ARI were assessed. On 1 extra block for each PMMA-based material surfaces were roughened with 180-grit sandpaper, simulating a normal/medium-grit ($100{\mu}m$) diamond bur, and brackets were bonded. Shear bond strengths and ARI scores were compared with those of groups 3, 6. Results: On $CAD-Temp^{(R)}$ significantly higher bracket bond strengths than on $Telio^{(R)}$ CAD were recorded. With XTP significantly lower levels of adhesion were reached than using SU or AP. Roughening with a coarser bur resulted in a significant increase in adhesion. Conclusions: Bracket bonding to CAD/CAM PMMA can be promoted by grinding the substrate with a normal/medium-grit bur or by coating the intact surface with universal adhesives. With appropriate pretreatments, bracket adhesion to CAD/CAM PMMA temporary restorations can be enhanced to clinically satisfactory levels.

Shear Bond Strength of Resin Cements on the IPS e.max Press (IPS e.max Press에 대한 수종 레진 시멘트의 전단결합강도에 관한 연구)

  • Lee, Kyung-Eun;Kim, Yu-Lee;Shin, Chang-Yong;Dong, Jin-Keun
    • Journal of Dental Rehabilitation and Applied Science
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    • v.26 no.3
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    • pp.311-322
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    • 2010
  • The purpose of this study was to evaluate the bond strengths between IPS e.max Press and four different types of resin cements that often used for esthetic restoration. Disc shaped IPS e.max Press blocks(N=40, diameter: 12mm, thickness: 3mm) were fabricated according to the manufacture's instruction and cleaned with ultrasonic cleaner. They were embedded into an autopolymerizing acrylic resin. Fourty cylinder shaped resin block(Filtek Z350, diameter: 4.5mm, thickness: 3mm) were fabricated using a plastic tube. Each specimens were randomly divided into 4 experimental group and bonded each other using 4 different resin cements(Variolink II(light-cure), Variolink II(dual-cure), Calibra, Super-Bond C&B) according to the manufactures' recommendations. All the specimens were stored in normal saline at $37^{\circ}C$ for 24 hours before test. Universal testing machine at a crosshead speed of 1mm/min was used to evaluate the shear bond strength. The data were statistically analyzed using one-way ANOVA(P<.01). Multiple comparison was done by the Tukey HSD test. The shear bond strength of Super-Bond C&B to e.max was significantly lower than those of Calibra, Variolink II(light-cure), Variolink II(dual-cure) (P<.01). The shear bond strength of Calibra, Variolink II(light-cure), Variolink II(dual-cure) to e.max were not significantly different. The shear bond strengths of light-cure/dual-cure cement were higher than that of self-cure cement.

Development and Splice Lengths of FRP Bars with Splitting Failures (쪼갬파괴에 의한 FRP 보강근의 정착길이와 이음길이)

  • Chun, Sung-Chul;Choi, Dong-Uk
    • Journal of the Korea Concrete Institute
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    • v.22 no.4
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    • pp.519-525
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    • 2010
  • Data from beam-based bond tests for FRP bars in the literature were collected and regression analyses were conducted for the data of splitting failure. Average bond strengths obtained from splice tests were found to be lower and more affected by C/$d_b$ values than average bond strengths from anchorage tests, indicating needs of new design equation for the splice length of FRP bars based on the data of splice tests only. In addition, the variation of bond strengths was greater than that of tensile strengths of FRP bars and, therefore, a new safety factor should be involved for the design equation. Five percent fractile coefficients were used to develop the design equations based on the assumption that load and resistance factors for FRP reinforced concrete structures are same to the factors for steel reinforced concrete structures. The proposed design equations give economical and reliable lengths for development and splice of FRP bars. The proposed equation for splice provides shorter lengths than the ACI 440 equation in case of C/$d_b$ of 3.0 or greater. Because FRP bars are expected to be used in slabs and walls exposed to weather with thick cover and large spacing between bars, the proposed equation gives optimal splice lengths.

Flexural behavior and durability evaluation of flexural members manufactured using prepacked DFRCC material (Prepacked DFRCC 재료로 제작된 휨 부재의 휨 거동 및 내구성 평가)

  • Kim, Jang-Ho;Lim, Yoon-Mook;Hong, Jong-Seok;Lee, Kyung-Min;Kim, Yoon-Ho
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05b
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    • pp.57-60
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    • 2006
  • The purpose of this study is to assess performance of prepacked DFRCC material compared with the DFRCC material which is made by using general mixing method. From 4r-point bending test, bond strength test and chlorine ion penetration test, flexural stress, -deflection relations, bond strengths, and durability assessment have been obtained. From the experiments, premixed DFRCC shows relatively good performance.

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THE EFFECT OF Ti ON THE SHEARBONDING STRENGTH BEWEEN DENTAL PORCELAIN AND Ni-Cr NONPRECIOUS ALLOY (Ti가 치과용 도재와 Ni-Cr 비귀금속 합금의 결합에 미치는 영향)

  • Cho, Sung-Am
    • The Journal of Korean Academy of Prosthodontics
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    • v.35 no.2
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    • pp.413-416
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    • 1997
  • A study of the shear bond strength between dental porcelain and alloy on Ti depostion effect was conducted by Instron universal testing machine. The obtained result was as follows ; The shear bond strengths of Ti-depostion group and acid-etched group were statistically significantly greater than that of untreated control group (p<0.01)

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Microshearbond strength to different surfaces of dentin under simulated pulpal pressure

  • Song, Yoon-Jung;Park, Sung-Ho
    • Proceedings of the KACD Conference
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    • 2003.11a
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    • pp.566-566
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    • 2003
  • The purpose of this in vitro study was to measure and compare the in vitro micro shear bond strengths of the following dentin bonding systems to different dentin surfaces under simulated pulpal pressure. Occlusal surfaces of 180 extracted human molars were prepared to expose the dentin surface in perpendicular to axis of tooth. Teeth were randomly assigned to 3 equal groups and subdivided into 4 equal groups. 4 adhesive systems(All Bond 2, SEbond, AdheSE, Prompt L-Pop) were used in this study.(omitted)

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Studies on Fracture Toughness in Internal Bond and Tension of Particleboard (파티클보드의 박리(剝離) 및 인장(引張)에 있어서의 파괴인성치(破壞靭性値)에 관(關)한 연구(硏究))

  • Kim, Han-Seok;Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.18 no.3
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    • pp.6-16
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    • 1990
  • The objectives of this study were to investigate the relative effects of specific gravity and particle size on internal bond and tensile strengths and fracture toughness of particleboard and to compare mechanical strength with fracture toughness. The particleboard was manufactured with three different particle sizes at specific gravity levels of 0.6, 0.7, and 0.8 with a resin content of 10% based on oven dry weight. The results were summarized as follows: 1. Internal bond strength. fracture toughness in internal bond test. maximum tensile strength, and fracture toughness in tension test increased with the increase of specific gravity of particleboard. 2. As partcle size increased, internal bond strength, fracture toughness. maximum tensile strength. and fracture toughness in tension test increased. 3. The maximum tensile strength and fracture toughness appeared to be in a direct relationship, and then maximum tensile strength could be used for predicition of fracture toughness for tension test. 4. The fracture toughness in internal bond test was somewhat independent on induced crack length.

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Bond-Strengthening Hooks for RC Members with High Strength Spirals

  • Kim Kil-Hee;Sato Yuichi
    • Journal of the Korea Concrete Institute
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    • v.17 no.5 s.89
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    • pp.835-842
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    • 2005
  • This paper presents an experimental investigation of bond-strengthening hooks as a new method to increase bond strength along flexural reinforcing bars in reinforced concrete (RC) beams and columns. The RC members, which consisted of 1,300 MPa-class spirals as shear reinforcement, often suffered from bond splitting failure. The proposed method attempts to increase confining stiffness around the flexural bars by placing U-shaped hooks and to prevent premature bond splitting failure. Twelve specimens with varied amounts and sizes of the hooks were prepared to verify the strengthening effectiveness under monotonic and cyclic loading conditions. The test result indicated that the hooks increased the bond strength along the flexural bars although the strengthening effectiveness was limited by effective reinforcement ratio $P_{be}$. This limit is determined by size of stress-transmitting zones of concrete around anchors of the hooks. Anchors of the hooks are recommended to be longer than twelve times the hook diameter and inserted deeper than a quarter of the member depth (D/4). Proposed design equations provide modest estimates of the shear strengths.