• Title/Summary/Keyword: BA treatment time

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Synthesis and characterization of $BaTiO_3$ fine particles by hydrothermal process (수열합성법에 의한 미립의 $BaTiO_3$ 분말합성 및 특성)

  • 배동식;주기태;한경섭;최상흘
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.563-566
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    • 1998
  • $BaTiO_3$ fine particles were prepared by hydrothermal process from titanium tetra-isoproproxide ($Ti(OiPr)_4$) and barium hexa-hydroxide ($Ba(OH)_2{cdot}8H_2O$) as raw materials. The fine particles were obtained at the temperature range of 160 to $185^{\circ}C$. The properties of $BaTiO_3$ particles were studied as a function of various parameters such as reaction temperature, reaction time and Ba/Ti ratio, etc. The average particle size of $BaTiO_3$ increased with increasing reaction temperature and time. After hydrothermal treatment at $170^{\circ}C$ for 8 h, the average particle size of $BaTiO_3$ was about 30 nm and the particle size distribution was narrow.

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Effects of GA3, BA, Zeatin and Kinetin on Flowering of Oncidium 'Aloha' (온시디움 'Aloha'의 개화에 미치는 GA3, BA, Zeatin 및 Kinetin의 영향)

  • Lee, Jong-Suk;Park, Byoung-Mo;Park, Hark-Bong
    • Horticultural Science & Technology
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    • v.17 no.2
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    • pp.134-135
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    • 1999
  • In order to improve quality and to accelerate blooming time in potted Oncidium 'Aloha', foliar spray of $GA_3$, BA, zeatin, and kinetin were applied on June 1 and June 15. The plant growth regulators did affect the improvement of number of peduncles, pedicels and florets, and shortened flowering time. Especially, number of peduncles and of florets were remarkably increased by foliar application of BA solution. And the flower opening time were shortened 26 days by 100mg/L BA treatment compare with control.

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Synthesis of the Ultrafine $BaTiO_3$ power by hydrothermal Process

  • Bae, Dong-Sik;Han, Kyong-Sop;Park, Sang-Heul
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1997.10a
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    • pp.87-89
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    • 1997
  • The BaTiO$_3$ fine powder was prepared by hydrthermal method using titanium tetrahydoxide (Ti(OH)$_4$) and barium dihydroxide (Ba(OH)$_2$.8$H_2O$) as raw materials. The fine powder was obtained at temperatures as low as 160 to 185$^{\circ}C$. The properties of the BaTiO$_3$ powder were studied as a function of various parameters (reaction temperature, reaction time, Ba/Ti=ratio, etc). The average particle size of the BaTiO$_3$ increased with increasing reaction temperature. After hydrothermal treatment at 17$0^{\circ}C$ for 8 h, the average particle size of the BaTiO$_3$ powder was about 30 nm and the particle size distribution was narrow.

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In vitro Shoot Proliferation by Pulse Treatment from Shoot Cultures of Q. acutissima and Ex vitro Root Induction Using Peat Plug Systems in Quercus spp. (상수리나무 기내배양(器內培養)에서의 Pulse처리(處理)에 의한 줄기증식(增殖) 및 Peat Plug를 이용(利用)한 참나무류(類) 기내줄기의 기외삽목(器外揷木))

  • Moon, Heung Kyu;Youn, Yang;Son, Sung Ho;Lee, Suk Koo;Yi, Jae Seon
    • Journal of Korean Society of Forest Science
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    • v.82 no.3
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    • pp.221-226
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    • 1993
  • Methods for shoot proliferation via pulse treatment onto the microshoots of Quercus acutissima, and ex vitro root induction using peat plug systems of the microshoots of 4 oak trees were described. Pulsing solution was prepared by the addition of BA and/or BA plus zeatin onto the aqueous WPM and sterilized distilled water. Using the solution, pulsing time was adjusted at different levels(0. 1, 2, 5. 9, and 24 hours). Although the effect of pulsing solution prepared by the addition of cytokinins onto the sterilized distilled water was slightly lower in shoot proliferation rate, a little higher in shoot elongation was observed compared with that of aqueous WPM. One hour of pulse treatment revealed best in shoot proliferation and its elongation, whereas the increment of pulsing time slightly suppressed the response. In addition, prolonged pulse time resulted high frequency of hyperhydric shoot appearance. Single treatment of BA was better in shoot proliferation than that of BA combination with zeatin, whereas the latter treatment usually showed rapid and healthy shoot growth. For ex vitro root induction using peat plug systems, black oaks(Q. acutissima and Q. variabilis) revealed excellent rootability compared with white oaks(Q. serrata and Q. mongolica). Shoot-tip necrosis of white oaks eras one of the big problems for survival. In this study, we discribed the effect of pulse treatment, successful ex vitro rooting system by the incorporation of peat plug, and the possibilities for the overcoming the obstacles on micropropagation of oaks.

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Nd1+XBa2-XCu3O7-δ Bulk Superconductor by Zone-melt Process

  • Soh, Dea-Wha;Guo, Fan-Zhan
    • Transactions on Electrical and Electronic Materials
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    • v.3 no.3
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    • pp.21-24
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    • 2002
  • Two kinds of $Nd_{1+X}Ba_{2-X}Cu_3O_{7-{\delta}}$, the sintering samples and zone melting samples, were heat-treated under pure Ar at 950$^{circ}C$. The substitution of Nd ion for Ba ion in the $Nd_{1+X}Ba_{2-X}Cu_3O_{7-{\delta}}$ before and after the heat treatment was investigated by XRD. In order to confirm the effects of the heat treatment, the Tc and Jc of samples with/without the heat treatment under Ar were comparatively studied. $Nd_{1+X}Ba_{2-X}Cu_3O_{7-{\delta}}$ samples were oxygenated under pure oxygen at $300^{circ}C$. From the XRD pattern it was found that the sample with x<0.4 was transferred from tetragonal phase to orthorhombic phase after the oxygenation, while the sample with x>0.4 did not show the phase transition even after a long time oxygenation. Therefore, the low oxygen partial pressure (Ar+1 % O$_2$) was used for the ambient atmosphere of the zone-melting samples, which could reduce the melting temperature and depress the substitution of Nd for Ba. After the improvement in the zone-melting process, the Jc value was increased to 2 x $10^4$A/$cm^2$ (0 T, 78 K). The particle orientation and the structure of zone-melted NdBaCuO were studied by the XRD and SEM analysis.

The Synthesis Mechanism of BaTiO3 Nano Particle at Low Temperature by Hydrate Salt Method (Hydrate Salt법을 이용한 Nano BaTiO3 저온합성 메커니즘)

  • Lee, Chang-Hyun;Shin, Hyo-Soon;Yeo, Dong-Hun;Ha, Gook-Hyun;Nahm, Sahn
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.12
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    • pp.852-856
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    • 2014
  • $BaTiO_3$ nano powder can be synthesized by hydrate salt method at $120^{\circ}C$ in air. Decreasing the thickness of thick film, the nano dielectric particle is needed in electronic ceramics. However, the synthesis of $BaTiO_3$ nano particle at low temperature in air and their mechanism were not reported enough. And ultrasonic treatment can be tried because of low temperature process in air. Therefore, in this study, the $BaTiO_3$ nano powder was synthesised with the synthesis time and ultrasonic treatment at $120^{\circ}C$ in air. In the synthesis process, the effects of process were evaluated. From the experimental observation, the synthesis mechanism was proposed. The homogeneous $BaTiO_3$ particle was synthesised by KOH salt solution at $120^{\circ}C$ for 1hour. It was conformed that the ultrasonic treatment effected on the increase of synthesis rate. After cutting the salt powder using FIB, $BaTiO_3$ nano particles observed homogeneously in the cross-section of the salt particle.

A Numerical Analysis of Heat Transfer in Bright Annealing Furnace of Stainless Steel Strip (Strainless steel strip 광휘어닐링로 내의 열전달 해석)

  • Ryou, H.S.;Jeong, Y.T.;Jang, B.L.
    • Journal of the Korean Society for Heat Treatment
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    • v.22 no.4
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    • pp.228-233
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    • 2009
  • In order to predict the temperature distribution of stainless steel strip in Bright Annealing (BA) furnace, we performed the analysis of heat transfer and fluid flow using STAR-CCM+. The analysis model included unsteady fluid flow, heat transfer with radiation and moving grid. Two kinds of radiative properties, emissivity and reflectivity, were applied to the stainless steel strip, one is constant and the other is variable with time. As we call, the BA furnaces of stainless steel strip have two different types, muffle and no-muffle. The using of muffle type has been faced with some problems such as rising in material price and shortening of life cycle, etc. So the development of no-muffle type BA furnace is very important in order to save energy cost, lower environmental load and increase the productivity. The designed (or expected) temperature of stainless steel strip coming out of BA furnace was about $1065^{\circ}C$ while the environment temperature maintains around $1100^{\circ}C$. The result of our calculation was very close (or similar) to design temperature, and the application of radiative properties variable with time produced more accurate result than applying constant ones.

Effects of Foliar-Sprayed Benzyladenine and Diphenylurea on Leaf Senescence, Grain Yield and Some Characters Related to Grain Quality of Rice (벼에서 Benzyladenine과 Diphenylurea의 엽면살포가 잎의 노화, 수량 및 미질관련형질에 미치는 영향)

  • 이변우;명을재;남택수;이정양
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.39 no.4
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    • pp.323-330
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    • 1994
  • Benzyladenine(BA) and Diphenylurea(DPU) at 10ppm level were foliar-applied one to three times at an interval of 10 days from heading stage of rice variety, Dongjinbyeo. One time treatment of both cytokinins did not delayed leaf senescence substantially, but consecutive treatments of two to three times markedly retarded leaf senescence. Leaf senescence retarding effects were greater in BA than DPU. Ripened grain ratio, grain weight and grain yield were not improved by the treatments. BA treatments increased the percentage of green and white belly kernels with no effects on opaque and white core kernels. BA and DPU treatments did not altered amylose content, but BA treatments significantly decreased protein content of polished rice. Consecutive treatments of BA and DPU twice or three times at an interval of 10 days from heading increased oil content by 30 to 78% as compared to non-treated control, but one time treatment at any stage did not enhance it of polished rice. Fatty acid composition was slightly altered in favor of unsaturated fatty acid by BA and DPU treatments.

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Synthesis of Nanocrystalline BaTiO3 Powder by the Combination of High Energy Ball Milling of BaCO3-TiO2 Mixture and Solid-State Reaction (고에너지 볼밀링된 BaCO3와 TiO2 혼합분말의 고상반응에 의한 나노결정 BaTiO3 분말 합성)

  • Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.310-316
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    • 2012
  • Nanocrystalline $BaTiO_3$ powder could be synthesized by solid-state reaction using the mixture which was prepared by a high energy milling process in a bead mill for $BaCO_3$ and nanocrystalline $TiO_2$ powders mixture. Effect of the milling time on the powder characteristic of the synthesized $BaTiO_3$ powder was investigated. Nanocrystalline $BaTiO_3$ with a particle size of 50 nm was obtained at $800^{\circ}C$. High tetragonal $BaTiO_3$ powder with a tetragonality(=c/a) of 1.009 and a specific surface area of $7.6m^2/g$ was acquired after heat-treatment at $950^{\circ}C$ for 2 h. High energy ball milling was effective in decreasing the reaction temperature and increasing the tetragonality.

Effects of reflector, surface treatment, and length of scintillation crystal on the performance of TOF-DOI PET detector with dual-ended readout

  • Jin Ho Jung;Yong Choi;Johyeon Yun;Jiwoong Jung;Sangwon Lee
    • Nuclear Engineering and Technology
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    • v.56 no.7
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    • pp.2633-2640
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    • 2024
  • The purpose of this study was to investigate the effect of the reflector, surface treatment, and length of scintillation crystals on the performance of a time-of-flight and depth-of-interaction (TOF-DOI) PET detector with a dual-ended readout and to determine the best reflector and surface treatment. Various types of crystal arrays with three different reflectors (ESR, BaSO4, and Toray), three different lateral surface treatments (all-polished (AP), all-roughened (AR), and partially roughened (PR, three sides polished, and one side roughened)), and two different lengths (20 and 15 mm) were fabricated. The highest light collection efficiency and best energy resolution were achieved using a crystal with a diffuse reflector (BaSO4 for AP and Toray for AR). In contrast, the best coincidence timing resolution (CTR) was achieved using an AR crystal with a specular reflector (ESR). The best DOI resolution was achieved using an AR crystal with BaSO4. Moreover, the results measured with the 20 mm long crystals were similar to those measured with the 15 mm long crystals. Therefore, we concluded that the dual-ended readout PET detector employing the crystal with AR lateral surface treatment and ESR was a good candidate for TOF-DOI PET because it provided excellent CTR and adequate DOI resolution.