Synthesis of the Ultrafine $BaTiO_3$ power by hydrothermal Process

  • Bae, Dong-Sik (Division of Ceramics, Korea Institute of Science & Technology) ;
  • Han, Kyong-Sop (Division of Ceramics, Korea Institute of Science & Technology) ;
  • Park, Sang-Heul (Department of Inorg. Mater. Engineering, Hanyang University)
  • Published : 1997.10.01

Abstract

The BaTiO$_3$ fine powder was prepared by hydrthermal method using titanium tetrahydoxide (Ti(OH)$_4$) and barium dihydroxide (Ba(OH)$_2$.8$H_2O$) as raw materials. The fine powder was obtained at temperatures as low as 160 to 185$^{\circ}C$. The properties of the BaTiO$_3$ powder were studied as a function of various parameters (reaction temperature, reaction time, Ba/Ti=ratio, etc). The average particle size of the BaTiO$_3$ increased with increasing reaction temperature. After hydrothermal treatment at 17$0^{\circ}C$ for 8 h, the average particle size of the BaTiO$_3$ powder was about 30 nm and the particle size distribution was narrow.

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