• 한국세라믹학회지
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• 제48권2호
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• pp.168-172
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• 2011

Alumina powder was added in a general porcelain (Backja) with clay, feldspar and quartz contents to promote the mullite ($3Al_2O_3{\cdot}2SiO_2$) generation in the porcelain. Low melting materials ($B_2O_3(450^{\circ}C)$, $MnO_3(940^{\circ}C)$, CuO($1080^{\circ}C$)) were doped at ~3 wt% to modify the sinterability of porcelain with a high alumina contents and promote the mullite generation. Green body was made by slip casting method with blended slurry and then, they were fired at $1280^{\circ}C$ for 1hr by a $2^{\circ}C/min$. Densifications of samples with high alumina contents (20~30 wt%) were impeded. As the doping contents of low melting materilas increased, the sinterability of samples was improved. The shrinkage rate and bulk density of samples were improved by doping with low melting materials. Mullite phase increased with increasing the low melting contents in the phase analyses. This means lots of alumina and quartz were transformed into mullite phase by low melting contents doping. In the results, high bending strength of samples with high alumina contents was accomplished by improving the densification and mullite generation in the porcelain.

• 대한기계학회논문집
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• 제10권5호
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• pp.713-723
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• 1986

본 논문에서는 비금속성 재질(SiO$_{2}$)로 만든 윅의 열전달 특성을 실험적 해석적 방법으로 연구했다. 먼저 비금속 윅을 단독으로만 실험하여 해석해와의 일치 성을 밝히고, 윅의 성능 개선을 위해 결합재의 첨가가 히이트파이프 증발부의 열전달 에 미치는 영향을 ADI해석 해법으로 예측하였다. 따라서 고온용 히이트파이프 뿐만 아니라 ,저온용에서도 비금속윅의 사용을 위한 가치 판단을 하고 비금속성 재질(SiO S12 등)이 윅으로서 넓게 이용 될수 있다는 가능성을 제시하는데 그 목적이 있다.

• 대한기계학회논문집B
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• 제21권9호
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• pp.1105-1114
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• 1997

The heat transfer characteristics of free surface water jet impinging normally against a flat uniform heat flux surface were investigated. This deals with the effect of three nozzle configurations (Cone type, Reverse cone type, Vertical circular type) on the local and the average heat transfer. Heat transfer measurements were made for water jet issuing from a nozzle of which exit diameter 8 mm. The experimental conditions investigated are Reynolds number range of 27000 ~ 70000( $V_{O}$=3 ~ 8 m/s), nozzle-to-target plate distances H/D=2 ~ 10, and radial distance from the stagnation point r/D ~ = 0 ~ 7.42. For all jet velocities of H/D=2, the local Nusselt number decreased monotonically with increasing radial distance. However, for H/D from 4 to 10, and for the jet velocity $V_{O}$.geq.7 m/s for Cone type nozzle and $V_{O}$.geq.6 m/s for the other type nozzles, the Nusselt number distributions exhibited secondary peaks at r/D=3 ~ 3.5. For Reverse cone type nozzle and Vertical circular nozzle, the maximum stagnation point heat transfer and the maximum average heat transfer occurs at H/D=8. But for the Cone type nozzle, the maximum stagnation and average heat transfer occurs at H/D=10, 4, respectively. From the optimum nozzle-to-target plate distance, the stagnation and the average heat transfer reveal the following ranking: Reverse cone type nozzle, Vertical circular type nozzle, Cone type nozzle.ozzle.

• Progress in Superconductivity
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• 제3권1호
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• pp.78-82
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• 2001

The spatial resolution of $high-T_{c}$ scanning SQUID microscope is limited by the washer size of SQUID and the gap distance between SQUID sensor and the sample. In this work, we tried to improve the spatial resolution of scanning SQUID microscope by reducing the size of SQUID sensor fabricated with $YBa_2$$Cu_3$$O_{7}$ thin film. Outer dimensions of the SQUiDs we tested are 24 $\mu\textrm{m}$ $\times$ $ 28\mu\textrm{m}$, $12 \mu\textrm{m}$ $\times$ $16\mu\textrm{m}$, $12\mu\textrm{m}$ x $12\mu\textrm{m}$, $10 \mu\textrm{m}$ $\times$ $10 \mu\textrm{m}$ each. To operate them in the flux-locked loop scheme, we used a direct-coupled electronics instead of using conventional electronics involving a modulation scheme. Since the direct-coupled feedback scheme does not require modulation current adjustment that poses as a practical difficulty in the SQUID operation in modulation-scheme, the direct feedback operation is rather simpler than the conventional modulation method. The resulting noise features were dominated by the noise of preamp in FLL electronics except that of the largest SQUID. The noise levels of SQUIDs are expected below 1$\times$$10^{-5}$ $\Phi_{0}$H $z^{1}$2/ (at 300 Hz), that is a typical noise level for SQUID made of $YBa_2$C $u_3$$O_{7}$ thin film. The data acquisition and motion-controlling parts were also improved, resulting in faster data acquisition rate and less vibration of the system.m.

• 한국결정학회지
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• 제5권2호
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• pp.93-99
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• 1994

K2O/3MOOS/0.SBB03 융제를 사용하여 TSSG 법으로 육성한 Md:Yal3(BO3)4 (NYAB) 단결정의 결정외형 및 표면형상을 연구하였다. <100>과 <120> 종자정을 사용한 경우는 서로 다른 크기의 프리즘 면들과 (101) 면들이 발달하였고 <001> 종자정을 사용하였을 때는 (001) 면이 함께 발달하였다. 종자정의 방향이 <100>또는 <120> 일때 프리즘 면 위에 성장구룽이 많이 형성되었으나, <001> 일때는 이웃하는 (101) 면에 평행한 줄무늬가 형성 되었다. (101) 면은 이차원 핵생성에 의한 성장이 지배적이고, <001> 종지정을 사용할 때 발달하는 (001) 면은 나선형 전위에 의한 성장이 지배적이었다. 종자정의 방향은 성장외형을 변화시키고 성장외형과 결정의 질을 결정하는 중요한 성장변수로 작용하였다.

• 한국결정성장학회지
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• 제12권6호
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• pp.288-291
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• 2002

We developed a new RF indirect-heating LPE furnace. The thermal gradient of our newly developed furnace is less than that of direct heating, and is as gentle as that of the resistance-heating LPE furnace. With this new furnace, the heating and/or cooling is faster than that of the resistance-heating furnace. Impurity-doped YIG film was grown from a $PbO-B_{2}O_{3}$, based flux on a (111) GGG substrate. To study the effect of the impurities on the MSSW threshold power and the saturation response time, we used two microstrip lines to excite and propagate the MSSW at 1.9 GHz. The MSSW threshold power and saturation response time was found to be related to the $\Delta$H.

• Journal of Advanced Marine Engineering and Technology
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• 제23권2호
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• pp.140-149
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• 1999

This study is on the development of the computer program that calculates a 3-D hull temperadistribution and analyzes BOR(Boil off rate) to be important to the heat design of a membrane type LNG carrier. The quarter of a tank is taken as an calculation model. And the thermal conductivity of insulation is assumed to be the function of a temperature. In the present steady state calculation, the temperature of LNG in a cargo tank is assumed to be -$162^{\circ}C$ and the air temperature of a cofferdam, to be +$5^{\circ}C$. The lowest air temperature in compartments is calculated as $21.39^{\circ}C$ under the USCG condition ($T_{air}=-18^{\circ}C,\;T_{sw}=O^{\circ}C)$ and B.O.R value is O.0977%/day under the maximum boil-off condition, IMO IGC ($T_{air}=45^{\circ}C,\;T_{sw}=32^{\circ}C$), which satisfies the requirement by KOGAS. The calculated temperature distribution over tank panels at each condition is maximum 3% less than GTT's results. From the results of this study, it can be concluded that the present design of LNG cargo tank satisfies the requirement by KOGAS.

• 한국세라믹학회지
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• 제26권4호
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• pp.459-470
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• 1989

Single crystals of rare-earth iron garnets were grown from solutions of molten lead oxide, lead fluoride, baric oxide, iron oxide, and the oxides of yttrium, samarium orgadolinium. The crystals were grown by slow cooling technique. A convenient composition was 41.8mol% PbO, 20.59mol% PbF2, 8.23mol% B2O3, 20.00mol% Fe2O3 and 10.00mol% R2O3 where R is Y, Sm or Gd. For this experiment, platinum crucibles of size 20, 30cc and a vertical siliconit tube furnace were used. The precipitation temperature of YIG was observed in the range of 115$0^{\circ}C$-112$0^{\circ}C$ and the optimum growth conditions in this experiment were determined. The nucleation rate was controlled by the holding time after the fast colling, the growth rate by the slow cooling conditiions. The form of the grown YIG crystals showed a combination of {110} and {211}, and the size of the crystals grown in this experiment was up to about 9mm under the conditions of holding time 16hour, cooling rate 2$^{\circ}C$/hr. and temperature range 115$0^{\circ}C$-90$0^{\circ}C$. The precipitatin temperature of SmIG was observed in the range of 105$0^{\circ}C$-98$0^{\circ}C$ and the size of the crystals grown in this experiment was up to about 5mm under the conditiions of holding time 16hours, cooling rate 2$^{\circ}C$/hr. and temperature range 100$0^{\circ}C$-80$0^{\circ}C$.

• Progress in Superconductivity
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• 제10권2호
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• pp.87-91
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• 2009

Fluorine-doped $SmFeAsO_{1-x}F_x$ single crystals with the nominal value of x=0.2 were grown at $1350-1450^{\circ}C$ under the pressure of 3.3 GPa by using the self-flux method. Plate-shaped single crystals in the range of a few-150 ${\mu}m$ in their lateral size were obtained. The detailed crystal structure was analyzed by using the x-ray diffractometry. Superconducting transition temperature, determined by the resistive transition, of a single crystal was about 49 K with a narrow resistive transition width of ${\sim}1$ K. A relatively sharp transition, a low residual resistivity, and a large residual resistivity ratio compared with those reported for $REFeAsO_{1-x}F_x$(RE=Sm, Nd) single crystals indicate the high quality of our single crystals.

• 한국재료학회지
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• 제25권12호
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• pp.694-702
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• 2015

Nd-Fe-B permanent magnets have been used in a wide variety of applications because of their high magnetic flux density. So, demand for neodymium has been increasing in worldwide. In this study, an electrowinning process was performed in $LiF-NdF_3-Nd_2O_3$ high temperature molten salts. However, a corrosion resistant material for use in the molten salt must be found for stable operation because of the harsh corrosion environment of the electrowinning process. Therefore, for this paper, boron nitride(BN), aluminum nitride(AlN), and silicon nitride($Si_3N_4$) were selected as protective and structural materials in the high temperature electrolyte. To investigate the characteristics of BN, AlN, and $Si_3N_4$, in molten salts, materials were immersed in the molten salts for 24, 72, 120, and 192 hours. Also, surface condition and stability were investigated by SEM and EDS and corrosion products were calculated by HSC chemistry. As a result, among BN, AlN, and $Si_3N_4$, AlN was found to show the best protective material properties.