• Journal of the Korean Ceramic Society
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• v.40 no.12
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• pp.1189-1196
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• 2003

Ferroelectric B $i_{3.25}$L $a_{0.75}$ $Ti_3$ $O_{12}$ (BLT) solution was synthesized by sol-gel process. BLT thin films were deposited on Pt/Ti $O_2$/ $SiO_2$/Si substrates by spin-coating. In this experiments, Bi(TMHD)$_3$, La(III)2-Methoxyethoxide, and Ti(IV) i-propoxide were used as starting materials, which were dissolved in 2-Methoxyethanol. Rapid Thermal Annealing (RTA) was used to promote crystallization of BLT thin films. The thin films with RTA process were compared with those with non-RTA process on electrical properties. After RTA process, the remanent polarization value (2Pr) of BLT thin films annealed at 72$0^{\circ}C$ was 20.46 $\mu$C/$\textrm{cm}^2$ which was approximately 27% higher than that of non-RTA process at 5 V.

• Transactions of Materials Processing
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• v.8 no.6
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• pp.541-553
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• 1999

Cold forging is a special type of forging process in which metal is forced to flow plastically under compressive force into a variety of shapes in room temperature. Gear blank, which is produced by cold forging, is concerned with the production method of transmission gear. Based on the results of simulation of the current four-stage process, the gear blank forging process for improving the conventional process sequence is designed. The rigid plastic finite element analysis for improving the conventional process. The new process consists of three stage operations with one annealing treatment after first operation. Based on the results of simulation of the proposed process, a required equipment could be selected. The new designed process appears to be more economical in producing the gear blank.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.19 no.7
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• pp.42-49
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• 2018

In steel industries, cold-rolled sheet manufacturing is one of the links between the front and rear important industries for national competitiveness and high value-added production. In particular, in small and medium-sized enterprises, one of the major problems is the carbonization phenomenon of the steel sheet during the annealing process. Carbonization occurring on the surface of the coil help reduce steel production. After conducting various experiments to identify the cause of carbonization on the surface of a cold-rolled steel, the following results were obtained: (1) An analysis of the rolling oil, which is used in the field, revealed it to contain approximately 40 ppm carbonized material. (2) A comparison of the thermal denaturation characteristics of the fresh rolling oil and using rolling oil by FT-IR analysis showed that thermal denaturation had occurred, as shown by the significant decrease in the relative intensity of the 2900 and $1750cm^{-1}$ peaks. (3) The thermal decomposition of the rolling oil took place for the rolling oil at approximately $220^{\circ}C$. Furthermore, annealing experiments at $200^{\circ}C$ showed that the carbonization phenomenon of the sample was not observed. On the other hand, carbonization was observed at temperatures higher than $240^{\circ}C$.

• Journal of Korean Vacuum Science & Technology
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• v.6 no.2
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• pp.84-87
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• 2002

The Si$_{1-x}$ Gex/Si surface alloy (x = 0.3, 0.4 and 0.5), which are prepared by solid source MBE and have the SiGe epilayer thickness of 50$\AA$, are annealed with different parameters. The surface structure analyses of the heterostructure samples are made on a triple-axis X-ray diffractometer in grazing incidence X-ray diffraction (GIXRD) geometry. It has been found that with different annealing time (1.5h, 18h, 64h) and annealing temperature (550 $^{\circ}C$, 750 $^{\circ}C$), the SiGe epilayer experienced different strain relaxation process, which was deduced from the GIXRD measurements of the in-plane (220) diffraction peak of Si(001) substrate and the relevant (220) surface diffraction of SiGe epilayer. The results show that the stress relieving and the lateral strain relaxation in the SiGe/Si heterostructure can be promoted by correct annealing, which is very helpful for the preparation of SiGe/Si strained superlattice with fine strain crystallization..

• Bulletin of the Korean Chemical Society
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• v.33 no.2
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• pp.398-402
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• 2012

ZnSe/$SiO_2$ coaxial nanowires were synthesized by a two-step process: thermal evaporation of ZnSe powders and sputter-deposition of $SiO_2$. Two different types of nanowires are observed: thin rod-like ones with a few to a few tens of nanometers in diameter and up to a few hundred of micrometers in length and wide belt-like ones with a few micrometers in width. Room-temperature photoluminescence (PL) measurement showed that ZnSe/$SiO_2$ coaxial nanowires had an orange emission band centered at approximately 610 nm. The intensity of the orange emission from the $SiO_2$-sheathed ZnSe nanowires was enhanced significantly by annealing in a reducing atmosphere whereas it was degraded by annealing in an oxidizing atmosphere. The origins of the PL changes by annealing are discussed based on the energy-dispersive X-ray spectroscopy analysis results.

• Applied Microscopy
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• v.45 no.1
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• pp.16-22
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• 2015

The reaction kinetics of the growth of Ni germanide in the Ni/Zr-interlayer/Ge system was investigated using isothermal in situ annealing at three different temperatures in a transmission electron microscope. The growth rate of Ni germanide in the Ni/Zr-interlayer/Ge system was determined to be diffusion controlled and depended on the square root of the time, with the activation energy of $1.04P{\pm}0.04eV$. For the Ni/Zr-interlayer/Ge system, no intermediate or intermixing layer between the Zr-interlayer and Ge substrate was formed, and thus the Ni germanide was formed and grew uniformly due to Ni diffusion through the diffusion path created in the amorphous Zr-interlayer during the annealing process in the absence of any intermetallic compounds. The reaction kinetics in the Ni/Zr-interlayer/Ge system was affected only by the Zr-interlayer.

• Journal of Surface Science and Engineering
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• v.38 no.1
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• pp.44-48
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• 2005

We prepared nickel silicide layers from p-Si(l00)/SiO₂(2000 Å)/poly-Si(700 Å)/Ni(400 Å) structures, feasible for gates in MOSFETs, by annealing them from 500℃～900℃ for 30 minutes. We measured the color coordination in visible range, cross sectional micro-structure, and surface topology with annealing temperature by an UV-VIS-IR spectrometer, field effect scanning electron microscope(FE-SEM), and scanning probe micro-scope respectively. We conclude that we may identify the nickel silicide by color difference of 0.90 and predict the silicide process reliability by color coordination measurement. The nickel silicide layers showed similar thickness while the columnar grains size and surface roughness increased as annealing temperature increased.

• ETRI Journal
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• v.36 no.1
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• pp.159-162
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• 2014

In this letter, we present low-temperature grown GaAs (LTG-GaAs)-based photoconductive antennas for the generation and detection of terahertz (THz) waves. The growth of LTG-GaAs and the annealing temperatures are systematically discussed based on the material characteristics and the properties of THz emission and detection. The optimum annealing temperature depends on the growth temperature, which turns out to be $540^{\circ}C$ to $580^{\circ}C$ for the initial excess arsenic density of $2{\times}10^{19}/cm^3$ to $8{\times}10^{19}/cm^3$.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.6
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• pp.1827-1835
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• 1996

This paper addresses the problem of a torch path generation for the 2D laser cutting of a stock plate nested with resular or irregular parts. Under the constaint of the relative positions of parts enforced by nesting, the developed torch path algorithm generate feasible cutting path. In this paper, the basic object is a polygon( a many-slide figure) with holes. A part may be represented as a number of line segments connected end-to-end in counterclockwise order, and formed a closed contour as requied for cutting paths. The objective is to tranverse this cutting contours with a minimum path length. This paper proposes a simulated annealing based dtorch path algorithm, that is an improved version of previously suggested TSP models. Since everypiercing point of parts is not fixed in advance, the algorithm solves as relazed optimization problem for the constraint, thich is one of the main features of the proposed algorithm. For aolving the torch path optimization problem, an efficient generation mechanism of neighborhood structure and as annealing shedule were introduced. In this way, a global solution can be obtained in a reasonable time. Seveeral examples are represented to ilustrate the method.

• Industrial Engineering and Management Systems
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• v.10 no.2
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• pp.134-139
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• 2011

The problem of scheduling in permutation flowshops has been extensively investigated by many researchers. Recently, attempts are being made to consider more than one objective simultaneously and develop algorithms to obtain a set of Pareto-optimal solutions. Varadharajan et al. (2005) presented a multi-objective simulated-annealing algorithm (MOSA) for the problem of permutation-flowshop scheduling with the objectives of minimizing the makespan and the total flowtime of jobs. The MOSA uses two initial sequences obtained using heuristics, and seeks to obtain non-dominated solutions through the implementation of a probability function, which probabilistically selects the objective of minimizing either the makespan or the total flowtime of jobs. In this paper, the same problem of heuristically developing non-dominated sequences is considered. We propose an effective heuristics based on simulated annealing (SA), in which the weighted sum of the makespan and the total flowtime is used. The essences of the heuristics are in selecting the initial sequence, setting the weight and generating a solution in the search process. Using a benchmark problem provided by Taillard (1993), which was used in the MOSA, these conditions are extracted in a large-scale experiment. The non-dominated sets obtained from the existing algorithms and the proposed heuristics are compared. It was found that the proposed heuristics drastically improved the performance of finding the non-dominated frontier.