• Title/Summary/Keyword: Analytical mode

검색결과 933건 처리시간 0.027초

A comparative study of ultra-trace-level uranium by thermal ionization mass spectrometry with continuous heating: Static and peak-jumping modes

  • Lee, Chi-Gyu;Park, Ranhee;Park, Jinkyu;Lim, Sang Ho
    • Nuclear Engineering and Technology
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    • 제52권7호
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    • pp.1532-1536
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    • 2020
  • For ensuring nuclear safeguards, we report the analytical signal-detection performance of thermal ionization mass spectrometry (TIMS) with continuous heating for the measurement of isotopic ratios in samples containing ultra-trace amounts of uranium. As methods for detecting uranium signals, peak-jumping mode using a single detector and static mode using multiple detectors were examined with U100 (10% 235U-enriched) uranium standard samples in the femtogram-to-picogram range. Uranium isotope ratios, n(235U)/n(238U), were measured down to levels of 1 fg and 3 fg in static and peak-jumping modes, respectively, while n(234U)/n(238U) and n(236U)/n(238U) values were measured down to levels of 100 fg in both modes. In addition, the dependency of the 238U signal intensity on sample quantity exhibited similar tendencies in both modes. The precisions of the isotope ratios obtained in the static mode over all sample ranges used in this study were overall slightly higher than those obtained in peak-jumping mode. These results indicate that isotope ratio measurements by TIMS with continuous heating are almost independent of the detection method, i.e., peak-jumping mode or static mode, which is characteristic of isotope-ratio measurements using the TIMS method with continuous heating. TIMS with continuous heating is advantageous as it exhibits the properties of multiple detectors within a single detector, and is expected to be used in various fields in addition to ensuring nuclear safeguards.

단일모드 구간해법을 이용한 보강토옹벽 설계의 신뢰성해석 (Reliability Analysis in Designing of Reinforced Soil Structures using Uni-Modal Bounds)

  • 김현기;이성혁;최찬용
    • 한국지반신소재학회논문집
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    • 제9권4호
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    • pp.17-25
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    • 2010
  • 전통적인 보강토옹벽 설계에서의 안정성 검토는 내적 외적 안정으로 구분하여 평가하며, 내적 안정은 보강재의 인발, 파단를 대상으로 하고 외적 안정은 구조체의 침하, 전도, 활동을 대상으로 한다. 최근 지반물성과 해석모델이 갖는 고유 불확실성을 최소화하기 위하여 신뢰성해석이 개발되어져 왔다. 본 연구에서는 내적 외적 안정이라고 정의되는 다양한 파괴모드에 대한 동시 파괴확률의 산정할 수 있도록 체계 신뢰성해석을 제안하였다. 단일구간 모드해법을 적용함에 의해 여러 안정해석에 대한 파괴모드를 통합하여 보강토옹벽 전체 시스템의 안정성을 평가할 수 있도록 하였다. 동시 파괴확률을 이용하면 대상으로 하는 안정해석모델과 파괴형상 및 파괴확률을 복합적으로 고려할 수 있기 때문에 개선된 안전성을 확보할 수 있을 것으로 판단되며, 안정해석모델별로 여러 지표를 이용하여 평가되었던 보강토옹벽의 설계를 대표 지표를 통하여 평가할 수 있다.

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LC/MS를 이용한 식육중 잔류 벤지미다졸계 구충제 분석법 연구 (Study on analytical method of residual benzimidazole anthelmintics in meat by LC/MS)

  • 최은영;서형석;백귀정;허부홍;서이원;정동석
    • 한국동물위생학회지
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    • 제28권1호
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    • pp.81-89
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    • 2005
  • Recently, mass spectrometry coupled with liquid chromatography (LC/MS) has been a preferred technique for determination of organic compounds in complex matrixes. LC/MS provides a high degree sensitivity and specificity of the compounds of interest. The purpose of this study was to confirm analytical method of residual 6 benzimidazoles (thiabendazole, oxfendazole, mebendazole, albendazole, flubendazole and fenbendazole) in meat by LC/MS. Benzimidazoles were analyzed by LC/MS on XTerra $C_{18}$ column with 0.01% trifluoroacetic acid-acetonitrile (TFA) in a gradient mode as mobile phase, and that were identified by electrospray ionization with selected ion recording mode at 150-350 amu mass range. Residual benzimidazoles were extracted from tissue with ethylacetate, and elute benzimidazoles with $50\%$ acetonitrile. In the LC/MS analysis of benzimidazoles, signal to noise ratio was showed relatively high in the positive mode and special ion in the quality analysis was determined via $[M+H]^+$ and Fragment ions. A spectrum of benzimidazoles was showed from all 6 benzimidazoles

Differential transform method and numerical assembly technique for free vibration analysis of the axial-loaded Timoshenko multiple-step beam carrying a number of intermediate lumped masses and rotary inertias

  • Yesilce, Yusuf
    • Structural Engineering and Mechanics
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    • 제53권3호
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    • pp.537-573
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    • 2015
  • Multiple-step beams carrying intermediate lumped masses with/without rotary inertias are widely used in engineering applications, but in the literature for free vibration analysis of such structural systems; Bernoulli-Euler Beam Theory (BEBT) without axial force effect is used. The literature regarding the free vibration analysis of Bernoulli-Euler single-span beams carrying a number of spring-mass systems, Bernoulli-Euler multiple-step and multi-span beams carrying multiple spring-mass systems and multiple point masses are plenty, but that of Timoshenko multiple-step beams carrying intermediate lumped masses and/or rotary inertias with axial force effect is fewer. The purpose of this paper is to utilize Numerical Assembly Technique (NAT) and Differential Transform Method (DTM) to determine the exact natural frequencies and mode shapes of the axial-loaded Timoshenko multiple-step beam carrying a number of intermediate lumped masses and/or rotary inertias. The model allows analyzing the influence of the shear and axial force effects, intermediate lumped masses and rotary inertias on the free vibration analysis of the multiple-step beams by using Timoshenko Beam Theory (TBT). At first, the coefficient matrices for the intermediate lumped mass with rotary inertia, the step change in cross-section, left-end support and right-end support of the multiple-step Timoshenko beam are derived from the analytical solution. After the derivation of the coefficient matrices, NAT is used to establish the overall coefficient matrix for the whole vibrating system. Finally, equating the overall coefficient matrix to zero one determines the natural frequencies of the vibrating system and substituting the corresponding values of integration constants into the related eigenfunctions one determines the associated mode shapes. After the analytical solution, an efficient and easy mathematical technique called DTM is used to solve the differential equations of the motion. The calculated natural frequencies of Timoshenko multiple-step beam carrying intermediate lumped masses and/or rotary inertias for the different values of axial force are given in tables. The first five mode shapes are presented in graphs. The effects of axial force, intermediate lumped masses and rotary inertias on the free vibration analysis of Timoshenko multiple-step beam are investigated.

Free vibration of a rectangular plate with an attached three-degree-of-freedom spring-mass system

  • Febbo, M.;Bambill, D.V.;Rossi, R.E.
    • Structural Engineering and Mechanics
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    • 제40권5호
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    • pp.637-654
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    • 2011
  • The present paper studies the variation of the natural frequencies and mode shapes of rectangular plates carrying a three degree-of-freedom spring-mass system (subsystem), when the subsystem changes (stiffness, mass, moment of inertia, location). An analytical approach based on Lagrange multipliers as well as a finite element formulation are employed and compared. Numerically reliable results are presented for the first time, illustrating the convenience of using the present analytical method which requires only the solution of a linear eigenvalue problem. Results obtained through the variation of the mass, stiffness and moment of inertia of the 3-DOF system can be understood under the effective mass concept or Rayleigh's statement. The analysis of frequency values of the whole system, when the 3-DOF system approaches or moves away from the center, shows that the variations depend on each particular mode of vibration. When the 3-DOF system is placed in the center of the plate, "new" modes are found to be a combination of the subsystem's modes (two rotations, traslation) and the bare plate's modes that possess the same symmetry. This situation no longer exists as the 3-DOF system moves away from the center of the plate, since different bare plate's modes enable distinct motions of the 3-DOF system contributing differently to the "new' modes as its location is modified. Also the natural frequencies of the compound system are nearly uncoupled have been calculated by means of a first order eigenvalue perturbation analysis.

Assumed Mode Method에 의한 부가물(附加物)을 갖는 임의(任意) 사각형(四角形) 평판(平板)의 진동해석(振動解析) (Vibration Analysis of Quadrangular Plate having Attachments by the Assumed Mode Method)

  • 한성용;허영철
    • 대한조선학회논문집
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    • 제32권3호
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    • pp.116-125
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    • 1995
  • 선체(船體) 해양구조물(海洋構造物)과 같은 대형(大型) 구조물(構造物)은 대부분 판(板) 구조물(構造物)로 이루어져 있으며, 이에 각종(各種) 기기류(機器類), cable류(類). Pillar, 탄성지지(彈性支待)된 장비(裝備) 등과 같이 집중질량(集中質量), 분포질량(分布質量), 지지(支持)스프링 , 질량(質量)-스프링 계(系) 등이 부가(附加)되는 경우가 많다. 이러한 판(板) 구조물(構造物)의 진동해석(振動解析) 방법(方法)으로 매우 단순(單純)한 경우를 제외하고는 엄밀해(嚴密解)를 얻기 어렵기 때문에 Rayleigh-Ritz방법(方法), assumed mode method와 같은 해석적(解析的) 방법(方法)이 주로 적용(適用)되고 있다. 국부(局部) 팬널의 형상(形狀)은 직사각형(直四角形) 뿐만 아니라 사다리꼴, 삼각형(三角形) 등 매우 다양(多樣)한데 상기(上記) 해석적(解析的) 방법(方法)을 적용한 연구(硏究)는 대부분 직사각형(直四角形)인 경우에 대하여 이루어졌다. 따라서 본(本) 연구(硏究)에서는 임의(任意) 사각형(四角形) 형상(形狀) 평판(平板)에 집중질량(集中質量), Pillar와 같은 지지(支持)스프링, 질량(質量)-스프링 계(系) 등이 부가(附加)된 전체계(全體系)의 진동해석(振動解析)을 효율적(效率的)으로 수행(遂行)하는 방법으로서 임의(任意) 사각형(四角形) 형상(形狀)을 효과적(效果的)으로 취급하기 위해 특성좌표계(特性座標系)를 활용하고 assumed mode method을 적용하는 정식화(定式化)를 제시하였다. 질량(質量)-스프링 계(系)가 부가(附加)된 사다리꼴 평판(平板)을 대상(對象)으로 일련의 수치(數値) 계산(計算)을 수행(遂行)하고 유한요소법(有限要素法)에 의한 결과(結果)와 비교(比較) 검토(檢討)하므로써 본(本) 연구(硏究)에서 제시한 방법(方法)의 타당성(妥當性)을 입증하였다.

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A Unified Analytical One-Dimensional Surface Potential Model for Partially Depleted (PD) and Fully Depleted (FD) SOI MOSFETs

  • Pandey, Rahul;Dutta, Aloke K.
    • JSTS:Journal of Semiconductor Technology and Science
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    • 제11권4호
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    • pp.262-271
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    • 2011
  • In this work, we present a unified analytical surface potential model, valid for both PD and FD SOI MOSFETs. Our model is based on a simplified one dimensional and purely analytical approach, and builds upon an existing model, proposed by Yu et al. [4], which is one of the most recent compact analytical surface potential models for SOI MOSFETs available in the literature, to improve its accuracy and remove its inconsistencies, thereby adding to its robustness. The model given by Yu et al. [4] fails entirely in modeling the variation of the front surface potential with respect to the changes in the substrate voltage, which has been corrected in our modified model. Also, [4] produces self-inconsistent results due to misinterpretation of the operating mode of an SOI device. The source of this error has been traced in our work and a criterion has been postulated so as to avoid any such error in future. Additionally, a completely new expression relating the front and back surface potentials of an FD SOI film has been proposed in our model, which unlike other models in the literature, takes into account for the first time in analytical one dimensional modeling of SOI MOSFETs, the contribution of the increasing inversion charge concentration in the silicon film, with increasing gate voltage, in the strong inversion region. With this refinement, the maximum percent error of our model in the prediction of the back surface potential of the SOI film amounts to only 3.8% as compared to an error of about 10% produced by the model of Yu et al. [4], both with respect to MEDICI simulation results.

소형 MR감쇠기의 성능 실험에 기초한 준능동 제어 시스템 (Semi-Active Control System Based on the Experimental Results of the Performance of a Small Scale MR Damper)

  • 민경원
    • 한국전산구조공학회논문집
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    • 제19권3호
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    • pp.233-238
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    • 2006
  • 이 논문에서는 소형 다층 구조물의 진동제어에 적용하기 위한 복합모드의 자기유변유체(MR) 감쇠기를 개발하였다. 우선, 도식적으로 전단, 유동, 복합모드 MR감쇠기의 형태를 설계조건과 함께 표현하였고, 각각의 모드에 대하여 자기장에 따른 감쇠력을 예측하기 위한 해석모델을 유도하였다. 다음으로 적당한 크기의 복합모드 MR감쇠기를 제작하고 자기장에 따른 감쇠특성을 시간영역에서 평가하였다. 마지막으로 지진하중을 받는 소형구조물에 제작된 MR감쇠기가 준능동 제어기로 제어하였을 때의 성능을 수치적으로 평가하였다.

Design Optimization of Double-array Bolted Joints in Cylindrical Composite Structures

  • Kim, Myungjun;Kim, Yongha;Kim, Pyeunghwa;Park, Jungsun
    • International Journal of Aeronautical and Space Sciences
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    • 제17권3호
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    • pp.332-340
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    • 2016
  • A design optimization is performed for the double-bolted joint in cylindrical composite structures by using a simplified analytical method. This method uses failure criteria for the major failure modes of the bolted composite joint. For the double-bolted joint with a zigzag arrangement, it is necessary to consider an interaction effect between the bolt arrays. This paper proposes another failure mode which is determined by angle and distance between two bolts in different arrays and define a failure criterion for the failure mode. The optimal design for the double-bolted joint is carried out by considering the interactive net-tension failure mode. The genetic algorithm (GA) is adopted to determine the optimized parameters; bolt spacing, edge distance, and stacking sequence of the composite laminate. A purpose of the design optimization is to maximize the burst pressure of the cylindrical structures by ensuring structural integrity. Also, a progressive failure analysis (PFA) is performed to verify the results of the optimal design for the double-bolted joint. In PFA, Hashin 3D failure criterion is used to determine the ply that would fail. A stiffness reduction model is then used to reduce the stiffness of the failed ply for the corresponding failure mode.

Free vibration analysis of cracked Timoshenko beams carrying spring-mass systems

  • Tan, Guojin;Shan, Jinghui;Wu, Chunli;Wang, Wensheng
    • Structural Engineering and Mechanics
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    • 제63권4호
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    • pp.551-565
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    • 2017
  • In this paper, an analytical approach is proposed for determining vibration characteristics of cracked non-uniform continuous Timoshenko beam carrying an arbitrary number of spring-mass systems. This method is based on the Timoshenko beam theory, transfer matrix method and numerical assembly method to obtain natural frequencies and mode shapes. Firstly, the beam is considered to be divided into several segments by spring-mass systems and support points, and four undetermined coefficients of vibration modal function are contained in each sub-segment. The undetermined coefficient matrices at spring-mass systems and pinned supports are obtained by using equilibrium and continuity conditions. Then, the overall matrix of undetermined coefficients for the whole vibration system is obtained by the numerical assembly technique. The natural frequencies and mode shapes of a cracked non-uniform continuous Timoshenko beam carrying an arbitrary number of spring-mass systems are obtained from the overall matrix combined with half-interval method and Runge-Kutta method. Finally, two numerical examples are used to verify the validity and reliability of this method, and the effects of cracks on the transverse vibration mode shapes and the rotational mode shapes are compared. The influences of the crack location, depth, position of spring-mass system and other parameters on natural frequencies of non-uniform continuous Timoshenko beam are discussed.