• Journal of the Korean Chemical Society
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• v.13 no.2
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• pp.157-164
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• 1969

Aoolphane was treated with 30% Hydrochloric acid at $18^{\circ}C$ for two hows with stirring in order to obtain the insoluble form of SiO2 gel and to extract quantitatively both $Al_2O_3$as and $Fe_2O_3AlCl_3{\cdot}6H_2O Fe$ and $Cl_3{\cdot}6H_2O$ forms, respectively, at the same time. $SiO_2$ gel was filtered and to the filterate Ammonia was added to precipitate $Al(OH)_3[Fe(OH)_3 Contaminated ]$ The precipitate was separated by filteration and the filterate was recovered as the form of $NH_4Cl$. The precipitate was treated with 200g (NaOH)/l Concentration of NaOH a little excessively to the equivalent at $65~70^{\circ}C$ as $Fe(OH)_3$ formed was insoluble, it was filtered of and to the filterate containing $NaAl(OH)_4(OH_2)_2$Carbon dioxide gas was bubbled at $50^{\circ}C~90^{\circ}C$ to obtain the precipitate with excellent filterability and crystallinity. The product was certified to be Dawsonite $(NaAl(OH)_2CO_3)$ by X-Ray diffraction analysis at below $40^{\circ}C$, when $CO_2$ gas was bubbled into the relatively lower concentration of $NaAl(OH)_4(OH_2)_2$ solution, the precipitate of very fine particles was formed, which was hard to filter and with the Composition of $\alpha-Al_2O_3-H_2O$ (Boehmite).

• Korean Journal of Materials Research
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• v.16 no.3
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• pp.178-182
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• 2006

A single electro-discharge-sintering (EDS) pulse (1.0 kJ/0.7 g), from a $300{\mu}F$ capacitor, was applied to atomized spherical Ti-6Al-4V powder in a low vacuum to produce porous-surfaced implant compacts. A solid core surrounded by a porous layer was formed by a discharge in the middle of the compact. XPS (X-ray photoelectron spectroscopy) was used to study the surface characteristics of the implant material. C, O, and Ti were the main constituents, with smaller amounts of Al, V, and N. The implant surface was lightly oxidized and was primarily in the form of $TiO_2$ with a small amount of metallic Ti. A lightly etched EDS implant sample showed the surface form of metallic Ti, indicating that EDS breaks down the oxide film of the as-received Ti-6Al-4V powder during the discharge process. The EDS Ti-6Al-4V implant surface also contained small amounts of aluminum oxide in addition to $TiO_2$. However, V detected in the EDS Ti-6Al-4V implant surface, did not contribute to the formation of the oxide film..

• Design & Manufacturing
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• v.13 no.4
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• pp.23-27
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• 2019

People's interest in the environmental problems of the Earth is growing as they come to the modern world, and research is being actively conducted on how to protect the environment. As a result, the automobile industry, one of the causes of environmental pollution, is also affected. Therefore, research is being conducted to improve the fuel economy and light weight of cars, development of pollution-free cars such as electric cars, and aluminium materials that are lighter than ordinary steel sheets and easier to recycle are gaining attention. In this experiment, the material was formed to form a form of aluminium and the material reduction rate of the side wall of the foam was tested according to the amount of side wall. The material used in the experiment was A3003-O, which is less plastic than normal steel plates, but has excellent corrosion resistance, plasticity and weldability compared to aluminium materials, but has poor tensile strength. For tensile testing, a certain array of Forming Shapes was molded and the height of the Forming was set to 5mm, and the height of the Forming was 4.7mm, indicating that the difference between the first 5mm Forming and the height was not large. In addition, the material reduction rate was tested by giving 15, 0, and -0.15 teas, respectively, and was found to be valuable as a product only for -0.15.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.12
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• pp.1551-1561
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• 2012

Boat or yacht hulls are mainly built using FRP composite materials. FRP boat hull manufacturing has been restricted since 2000 under international regulations on ocean environment safety. FRP composite materials cannot be recycled and require more than 100 years to biodegrade. Therefore, alternatives to FRP have been proposed by many boat builders. Steel, aluminum, and FRP are commonly used as boat hull materials. Their design specifications are proposed as Korean register of shipping. However, the design specifications for inexpensive materials for a small boat have not yet been studied. Small shipbuilders manufacture and sell HDPE canoes or HDPE kayaks. In this study, a hull form was designed based on actual boats. The thickness of an HDPE boat hull was determined based on ISO 12215-5 structural design specifications.

• Structural Engineering and Mechanics
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• v.35 no.5
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• pp.571-592
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• 2010

An energy-based fatigue life prediction framework was previously developed by the authors for prediction of axial, bending and shear fatigue life at various stress ratios. The framework for the prediction of fatigue life via energy analysis was based on a new constitutive law, which states the following: the amount of energy required to fracture a material is constant. In the first part of this study, energy expressions that construct the constitutive law are equated in the form of total strain energy and the distortion energy dissipated in a fatigue cycle. The resulting equation is further evaluated to acquire the equivalent stress per cycle using energy based methodologies. The equivalent stress expressions are developed both for biaxial and multiaxial fatigue loads and are used to predict the number of cycles to failure based on previously developed prediction criterion. The equivalent stress expressions developed in this study are further used in a new finite element procedure to predict the fatigue life for two and three dimensional structures. In the second part of this study, a new Quadrilateral fatigue finite element is developed through integration of constitutive law into minimum potential energy formulation. This new QUAD-4 element is capable of simulating biaxial fatigue problems. The final output of this finite element analysis both using equivalent stress approach and using the new QUAD-4 fatigue element, is in the form of number of cycles to failure for each element on a scale in ascending or descending order. Therefore, the new finite element framework can provide the number of cycles to failure at each location in gas turbine engine structural components. In order to obtain experimental data for comparison, an Al6061-T6 plate is tested using a previously developed vibration based testing framework. The finite element analysis is performed for Al6061-T6 aluminum and the results are compared with experimental results.

• Proceedings of the KSME Conference
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• 2001.06c
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• pp.83-87
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• 2001

A 110 mm diameter aspheric metal secondary mirror for a test model of an earth observation satellite camera was fabricated by ultra-precision single point diamond turning (SPDT). Aluminum alloy for mirror substrates is known to be easily machinable, but not polishable due to its ductility. A harder material, Ni, is usually electrolessly coated on an Al substrate to increase the surface hardness for optical polishing. Aspheric metal secondary mirror without a conventional polishing process, the surface roughness of Ra=10nm, and the form error of $Ra={\lambda}/12({\lambda}=632nm)$ has been required. The purpose of this research is to find the optimum machining conditions for reflector cutting of electroless-Ni coated Al alloy and apply the SPDT technique to the manufacturing of ultra precision optical components of metal aspheric reflector.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2004.04a
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• pp.34-41
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• 2004

The purpose of this paper is to look at the characteristics of surface finishing which is one of the form accuracies and to obtain the fundamental technical data from the process of machining with diamond tool through experiment and theoretical analysis. The experiments were conducted with domestic made ultra-precision machine and MCD.PCD tool, with aluminum alloyed material and brass being used for the work pieces. The goal of the size accuracy was set to 100nm. The most suitable tool nose radius and machining conditions were selected, and the variations of the surface roughness were observed using SEM method while machining the distance of up to 500km. These data were evaluated and they examined the variation of the machined surfaces while cutting up to 500km of machining distance. At the same time, the state for the wear of diamond tool nose was analyzed and carefully examined through the newest measuring device. Additionally, the characteristics of ultra-precision machining technology were studied through visual analysis.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2007.11a
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• pp.565-573
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• 2007

This paper is concerned with the dynamic modeling, active vibration controller design and experiments for a cylindrical shell equipped with MFC actuators. The dynamic model was derived by using Rayleigh-Ritz method based on Donnel-Mushtari shell theory. The actuator and sensors for the MFC actuator equations were derived based on pin-force model. The equations of motion were then reduced to modal equations of motion by considering the modes of interest. The sensor equations were also converted to a reduced form. An aluminum shell was fabricated to demonstrate the effectiveness of modeling and control techniques. The boundary conditions at both ends of the shell were assumed to be shear diaphragm. Theoretical natural frequencies were calculated and compared to experimental result. It was observed that the theoretical result is in good agreement with experimental result for the first two modes. The multi-input and multi-output positive position feedback controller, which can cope with first two modes, was then designed based on the blockinverse theory and implemented using DSP. It was found from experiment that vibrations can be successfully suppressed.

• Bulletin of the Korean Space Science Society
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• 2011.04a
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• pp.31.4-32
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• 2011

The previous KRISS profilometer design used an aluminum profile structure to which a bar-type reference mirror subsystem and the measurement subsystem are mounted. The earlier design suffers from low stiffness as shown from the first resonance mode of 45.1 Hz. The improved mechanical design we describe in this study replaces the aluminium profile structure with a granite structure of $1340{\times}220{\times}230$ in dimension. The finite element analysis results for the revised design show 0.001 degree in probe contact angle variation. The first resonance mode was computed to 91.2 Hz that is much better than 45.1 Hz from the previous design. We describe the improved design, structural analysis results and how these results would satisfy the form accuracy requirement of 1 ${\mu}m$ PV.

• Journal of the Korean Institute of Navigation
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• v.9 no.2
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• pp.43-63
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• 1985

As a circular cylinder has a comparatively simple shape and becomes a basic problem for flows around other various shapes of bodies, the problem of two-dimensional viscous flow around the circular cylinder has been investigated, both theoretically and experimentally. But not a few problems are left unsolved. It is well known that the calculations are successfully made with the approximations of Stokes or Oseen for very low Reynolds numbers, but as Reynolds number is increased, Oseen's approximations as well as Stokes's ones become more and more remote from the exact solution of the Navier-Stokes equations. Therefore, in this paper, the authors transform the Navier-Stokes equations into the finite difference equations in the steady two-dimensional viscous flow at Reynolds number up to 45, and then solve the solution of the Navier-Stokes equations numerically. Also, the authors examine the accuracy of the solution by means of flow visualization with aluminum powder. The main results are as follows; (1) The critical Reynolds number at which twin vortices begin to form in the rear of the circular cylinder is found to be 6 in the experiment and 4 in the numerical solution. (2) As Reynolds number is increased, it is proved that the ratio of the length of the twin vortices to the diameter is grown almost linearly, both experimentally and numerically. (3) Separation angle is also increased according to reynolds number. But it is found that it would converge into 101.3 degrees, both experimentally and numerically.