• Title/Summary/Keyword: Adhesive method

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Preparation and Properties of Water-based Adhesive Using Gemini Type Nonionic Reactive Surfactants (제미니형 비이온 반응성 계면활성제를 이용한 수성접착제의 제조 및 특성)

  • Shin, Hye-Lin;Jeong, Noh-Hee
    • Applied Chemistry for Engineering
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    • v.30 no.5
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    • pp.597-605
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    • 2019
  • In order to improve the adhesion of water-based adhesive, gemini type nonionic reactive surfactants were synthesized and applied to water-based adhesives. The surfactants were synthesized by using maleic acid and polyoxyethylene cetyl ether having different length of ethylene oxide and confirmed by FT-IR and $^1H-NMR$. Their appearance was light yellow wax. The cloud point of the compound was more than $78^{\circ}C$. The measured critical micelle concentration (c.m.c) was $1.0{\times}10^{-4}{\sim}7.0{\times}10^{-4}mol/L$ and surface tension at c.m.c was 25.9~32.0 mN/m. As the number of ethylene oxide increased, the emulsifying power was improved. The foaming height of each compound by Ross-Miles method was 1.4~4.5 cm. The synthesized surfactants was then used as an emulsifier in emulsion polymerization of water-based adhesives and its physical properties were evaluated. The solid contents of prepared adhesives was 59%. The average particle size and initial tackiness of the prepared adhesives were 164~297 nm and ball no. of 20~32, respectively. The peel strength was $1.8{\sim}2.1kg_f/mm$. The retention rate of adhesives viscosity was evaluated to 99% during 30 days. Therefore, synthesized gemini type nonionic reactive surfactants are expected to be applied as an emulsifier for the high adhesive force.

A study on the distribution of latent fingerprints on paper knife sheaths (간이 칼집에서의 잠재지문 분포에 관한 연구)

  • Kim, Hyo-Mi;Park, Gi-Hyun;Lee, Su-Bhin;Yu, Je-Seol
    • Analytical Science and Technology
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    • v.34 no.6
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    • pp.251-258
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    • 2021
  • Knives are most frequently used as weapons in violent crimes. Criminals leave behind knife sheaths made of paper and tape at crime scenes. It is difficult to develop fingerprints using tape attached to a porous surface, resulting in the need to explore effective techniques for identifying fingerprints as well as the distribution of fingerprints on each surface, when evidence such as paper knife sheaths are found. In this study, 50 knife sheaths were prepared. The cyanoacrylate fuming (CA fuming) method was applied to develop fingerprints on the non-adhesive side of the tape, and a dual-purpose 1,2-indanedione/Zn (1,2-IND/Zn) reagent was used to separate tape from paper while simultaneously developing fingerprints on the paper. The fingerprints on the adhesive side of the tape were developed using Wet Powder Black®. Using the R statistical analysis program (The R Foundation for Statistical Computing), we used a heat map to indicate the location of fingerprints developed from each surface. More fingerprints were detected at the ends than in the center of the adhesive side of the tape, and although the non-adhesive sides of tape and paper did not present clear distribution patterns, many fingerprints were developed that had sufficient clarity for personal identification. The results of this study may be applicable for processing evidence when paper sheaths are found at crime scenes.

Manufacturing technology of two-layer self bonding insulating tape (이중절연 자기융착테이프 제조기술)

  • 조용석;이철호;심대섭
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.890-893
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    • 2001
  • Two-layer self bonding insulating tape consists of butyl rubber(IIR ; Isobutylene-isoprene rubber) adhesive layer and polyethylene protective film. Butyl rubber have inherent characteristics such as resistance to corrosion and water, low temperature flexibility, excellent electrical insulating properties also resistance to environmental effect such as ozone and ultraviolet. Polyethylene film was used for the purpose of good insulating properties and resistance to ozone and ultraviolet. The tape was manufactured using extrusion and calender method.

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교정용 브라켓의 간접 접착법

  • Cha, Bong-Geun
    • The Journal of the Korean dental association
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    • v.37 no.7 s.362
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    • pp.530-535
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    • 1999
  • Detailed finishing of the occlusion is a clinical skill that has become difficult with the development of fixed appliances. Accuracy of bracket placement definitely improves with indirect technique, Several methods for the placement of orthodontic brackets on dental casts are currently used in the indirect bonding technique. These include attachment by means of bonding resins, adhesive tapes or sticky wax. This article presents the indirect procedures of our clinic, which use paste-paste chemically cured composites. Detailed laboratory and clinical procedure for dual tray method and other application of indirect bonding will be presented.

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Evaluation Method of Bonded Strength Considering Stress Singularity in Adhesively Bonded Joints (응력특이성을 고려한 접착이음의 강도평가 방법)

  • 정남용
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.7 no.1
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    • pp.58-68
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    • 1998
  • Advantages of adhesively bonded joints and techniques of weight reduction have led to increasing use of structural adhesives such as LSI(large scale integration) package, automobile, aircraft in the various industries. In spite of such wide applications of adhesively bonded joints, the evaluation method of bonding strength has not been established. Stress singularity occurs at the interface edges of adhesively bonded joints and it is required to analyze it. In this paper, the stress singularity using 2-dimensional elastic boundary element method (BEM) with the changes of the lap length and adhesive for single lap joint was analyzed, and experiments of strength evaluation were carried out. As the results, the evaluating method of bonding strength considering stress singularity at interface edges of adhesively bonded joints and stress intensity factor of interface crack have been proposed in static and fatigue test.

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Characterization of Carbon Nanotube Cathodes with Surface Treatment by Polymer-Based Organic Materials

  • An, Young-Je;Lee, Ji-Eon;Kim, Kye-Sung;Cheon, Ko-Eun;Karim, Md. Anwarul;Cho, Young-Rae
    • 한국정보디스플레이학회:학술대회논문집
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    • 2006.08a
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    • pp.1210-1213
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    • 2006
  • The effect of surface treatment on CNT cathodes used in field emission displays was investigated. A liquid method using a polymer-based organic solution and a mechanical method were applied. The liquid method, using PVA(polyvinyl alcohol) showed high potential compared to the mechanical adhesive taping and rolling method used in the fabrication of CNT cathodes for large-sized field emission displays with high emission uniformity and a low cost.

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Topology Optimization of Connection Component System Using Density Distribution Method (밀도분포법을 이용한 부재의 연결구조 최적화)

  • 한석영;유재원
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.12 no.4
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    • pp.50-56
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    • 2003
  • Most engineering products contain more than one component. Failure occurs either at the connection itself or in the component at the point of attachment of the connection in many engineering structures. The allocation and design of connections such as bolts, spot-welds, adhesive etc. usually play an important role in the structure of multi-components. Topology optimization of connection component provides more practical solution in design of multi-component connection system. In this study, a topology optimization based on density distribution approach has been applied to optimal location of fasteners such as T-shape, L-shape and multi-component connection system. From the results, it was verified that the number of iteration was reduced, and the optimal topology was obtained very similarly comparing with ESO method. Therefore, it can be concluded that the density distribution method is very suitable for topology optimization of multi-component structures.

Topology Design of Connection Component System Using Density Distribution Method (밀도분포법을 이용한 부재의 연결구조 최적화)

  • 한석영;유재원;박재용
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2003.04a
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    • pp.15-20
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    • 2003
  • Most engineering products contain more than one component. Failure occurs either at the connection itself or in the component at the point of attachment of the connection in many engineering structures. The allocation and design of connections such as bolts, spot-welds, adhesive etc. usually play an important role in the structure of multi-components. Topology optimization of connection component provides more practical solution in design of multi-component connection system. In this study, a topology optimization based on density distribution approach has been applied to optimal location of fasteners such as T-shape, L-shape and multi-component connection system. From the results, it was verified that the number of iteration was reduced, and the optimal topology was obtained very similarly comparing with ESO method. Therefore, it can be concluded that the density distribution method is very suitable for topology optimization of multi-component structures.

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Optimization of the Plasma Spray Coating Parameters of Ni-5%Al Alloy Powder Using the Taguchi Experimental Method (다꾸찌방법에 의한 Ni-5%Al 합금 분말의 플라즈마 용사코팅 조건의 최적화)

  • 이형근
    • Journal of Welding and Joining
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    • v.20 no.5
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    • pp.120-126
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    • 2002
  • Ni-5%Al alloy powder is widely used as the bond coating powder to improve the adhesive strength between the substrate and coating. The important properties in the bond coating are the deposition efficiency and surface roughness. In this study, it was tried to optimize the plasma spray parameters to maximize the deposition efficiency and surface roughness. In the first step, spray current and hydrogen gas flow rate were optimized in order to increase the deposition efficiency. In the next step, the seven plasma spray variables were selected and optimized to improve both the deposition efficiency and surface roughness using the Taguchi experimental method. By these optimization, the deposition efficiency was improved from about 10 % at the frist time to 51.2 % by the optimization of spray current and hydrogen gas flow rate and finally to 65.2 % by the Taguchi experimental method. The average surface roughness was increased from about $12.9\mu\textrm{m}$ to $15.4\mu\textrm{m}$.

Effect of Different Types of Bonding Agent and Application Methods on Shear Bond Strength of Orthodontic Bracket (Bonding agent의 종류 및 적용 방법에 따른 교정용 브라켓의 전단결합강도에 관한 연구)

  • Lee, Jaehee;Kim, Jongsoo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.44 no.4
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    • pp.419-426
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    • 2017
  • Attachment of the orthodontic bracket conducted during the window opening procedure can result in failure due to various adverse conditions such as blood or saliva contamination, or other wet conditions. For the success of the bracket attachment, reduction of total operation time is crucial. The purpose of this literature is to evaluate the differences between the final resultant shear bond strength of the conventional method of using phosphoric acid and self-etching primer, and that of the operation time-reduced method in which the curing step is omitted subsequent to the primer application. A total of 40 human maxillary incisors were prepared. Group I(control group) and II were etched with 37% phosphoric acid and Group III and IV were conditioned with self-etching primer. Attachment of the group I and III was conducted by manufacturer's instructions. The operation time of Group II and IV was reduced by eliminating the curing step after the primer application. The resultant shear bond strength of each group was measured and an adhesive remnant index (ARI) was recorded. The mean shear bond strength of group I, II, III, and IV were 14.16 MPa, 8.33 MPa, 8.29 MPa, and 6.48 MPa respectively. Significant differences could only be found between the control group and the experimental groups (p < 0.05). The ARI indicated no significant difference among all groups.