• 제목/요약/키워드: Adhesive Strength Test

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The Bending Strength and Adhesive Properties of PRF and MUF Glulam (PRF, MUF 집성재의 휨 강도와 접착 성능 평가)

  • Park Jun-Chul;Kim Keon-Ho;Hong Soon-Il
    • Journal of the Korea Furniture Society
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    • v.15 no.2
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    • pp.19-27
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    • 2004
  • As glulam is a woody material, it is necessary to be more careful in a gluing process. It takes 6-7 hours at $40-60^{\circ}C$ to harden PRF resin used in making structural glulam, and about 24 hours at room temperature. In the present process which can not use a press continuously, reducing the hardening time is necessary to increase production. The experiment was done to compare the adhesive properties of PRF resin and MUF resin through bending test, block shear strength test and water soaking test. In comparing the bending strength of prediction MOE is 1.2 times higher that actual MOE. PRF and MUF do not show significant difference in MOE and MOR, and in block shear strength test, such as shear strength and wood failure rate. However, in water soaking and boiling water soaking tests PRF and MUF show the significant difference in delamination rate.

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A STUDY ON THE ADHESIVENESS OF SILICONE AND POLYURETHANE SHEET IN MAXILLOFACIAL PROSTHESES (악안면 보철용 폴리우레탄과 실리콘의 접착도에 관한 실험적 연구)

  • Cho, Sang-Jun;Lim, Ju-Hwan;Cho, In-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.34 no.4
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    • pp.833-849
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    • 1996
  • The material of choice for functional and esthetic reconstruction of maxillofacial defects is silicone. Silicone has appropriate physical properties for maxillofacial prosthesis but it has weak edge strength. Therefore, a proper combination of silicone and polyurethane sheet is recommended to improve this weakness. Various primers are also used to enhance the adhesive strength between silicone and polyurethane sheet. The purpose of this study was to determine the adhesive strength of silicone and polyurethane sheet. Silicone elastomer mixture was made by admixing MDX4-4210 elastomer (40%) and Silastic Medical Adhesive Type A(60%). This silicone elastomer mixture was attached to polyurethane sheet, using one of three different primers(1205, S-2260, or A-304), treated for 1, 2, 4, 6, and 8 hours. These were then polymerized in room temperature, dry-heat oven or microwave oven. Six specimens per each group, a total of 270 specimens were prepared for final test. The differences of T-peel bonding strengths were then determined by a test. The differences of T-peel bonding strengths were then determined by a test method that was recommended by American Society for Testing and Materials C794-80. The results were statistically analyzed using the ANOVA and Mutiple Range Tests(Tukey' HSD). The reults were as follow. 1. Type of primer, primer reaction time, and methods of polymerization showed significant correlation on the T-peel bonding strengths in adhesiveness between silicone and polyurethane sheet. 2. A-304 primer showed statistically higher in T-peel bonding strength than otehr type of primers except for the polymerization in microwave oven with reaction times of 2, 6 hours(p<0.05). 3. No significant differences in T-peel bonding strength were observed among the polymerization methods. 4. The effect of reaction time by the primer type and polymerization method showed statistically significant differences in bonding strength among different reaction times. And in most cases, reaction time of 1 or 2 hours showed higher T-peel bonding strength.

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Effects of Artificial Saliva Contamination on the Bond Strength of Three Dentin Adhesives to Dentin of Primary Teeth (인공타액오염이 유치 상아질에서 3종 상아질 접착제의 결합 강도에 미치는 영향)

  • Bae, Youngeun;Kim, Shin;Jeong, Teasung;Kim, Jiyeon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.44 no.1
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    • pp.72-81
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    • 2017
  • The aim of this study was to evaluate the effectiveness of artificial saliva contamination and decontamination procedures at different stages of a bonding procedure on the microtensile bond strength (MTBS) of two one-step self-etch adhesives and a two-step total-etch adhesive to dentin of primary teeth. Forty-two extracted sound primary molars were randomly divided into three groups depending on three adhesives, Scotchbond Universal Adhesive (SBU), All-Bond Universal (ABU) and Prime & Bond NT (PNT). For each adhesive, the teeth were allocated into seven groups. Except for control group, group 1, the groups were contaminated with artificial saliva at three different stages: the groups 2 and 3 - before adhesive application; the groups 4 and 5 - before adhesive polymerization; the groups 6 and 7 - after adhesive polymerization. Decontaminating procedures were rinsing, air-drying (group 2, 4, 6) and air-drying (group 3, 5, 7). The specimens were restored with composite resin (Filtek, Z350) and microtensile bond strength was measured. The data was analyzed with one-way ANOVA and Tukey HSD test (p < 0.05). In the control group, using PNT resulted in significantly higher bond strength than when ABU and SBU were used (p < 0.001). For three adhesives, the groups 2, 4 and 6 had greater bond strength than the groups 3, 5 and 7. Also, when the artificial saliva was contaminated before adhesive polymerization (group 4, 5), it showed a significantly lower bond strength. Generally the two-step total-etch adhesive generated a higher bond strength than the one-step self-etch adhesive. Artificial saliva contamination before adhesive polymerization led to a drastic decrease in bond strength, and rinsing with water followed by air-drying could not recover the bond strength.

Adhesion Improvement for Copper Process in TFT-LCD

  • Tu, Kuo-Yuan;Tsai, Wen-Chin;Lai, Che-Yung;Gan, Feng-Yuan;Liau, Wei-Lung
    • 한국정보디스플레이학회:학술대회논문집
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    • 2006.08a
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    • pp.1640-1644
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    • 2006
  • The first issue that should be overcome in copper process is its poor adhesive strength between pure copper film and glass substrate. In this study, defining the adhesive strength of pure copper film on various substrates and clarifying the key deposition parameters are presented for the investigation of copper process. First, using different kinds of surface plasma treatments were studied and the results showed that the adhesive strength was not improved even though the roughness of glass substrate surface was increased. Second, adding an adhesive layer between glass substrate and pure copper film was used to enhance the adhesion. Based on the data in the present paper, adopting copper alloy film as an adhesive layer can have capability preventing peeling problem in copper process. Besides, Cu/Cu alloy structure could be etched with the same etchant with better taper angle than the one with single layer of Cu. Unlike Cu/Mo structure, there is no residual problem for Cu/Cu alloy structure during etching process. Finally, this structure was examined in electrical test without significant difference in comparison with the conventional metal process.

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Pullout Test of Retrofit Anchors using Deformed Reinforcement and Adhesive

  • Choi, Dong-Uk;Kim, Yon-Gon
    • KCI Concrete Journal
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    • v.11 no.3
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    • pp.201-210
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    • 1999
  • An experimental study was carried out to determine pullout behavior of a new type of anchor bolt that used deformed reinforcement and a commercial adhesive. Concrete slabs and columns with about 20-MPa compressive strength were used for 136 pullout tests performed. Test variables included anchor diameter (10 mm ~ 32 mm). embedment depth (10$\Phi$ or 15$\Phi$), edge effect. and Presence of transverse reinforcement in existing concrete. In Tyre-S test. where the edge or reinforcing steel effect was not included, the anchor Pullout strengths increased with increasing anchor diameters. Anchors with 15$\Phi$ embedment depth had higher Pullout strengths than those with 100 embedment depth The largest average Pullout load of 208 kN was determined for anchors made with D25 reinforcement and with 15$\Phi$ embedment depth. In Type-E tests, where the anchors were installed close to the edge of existing concrete, there were reductions in pullout strengths when compared to those determined in Type-S tests. In Type-ER tests, influence of the reinforcement in existing concrete on the anchor pullout strengths was examined using reinforced concrete and plain concrete columns Test results indicated that existing transverse reinforcement (column ties) did not help increase the pullout strength. The overall pullout test results revealed that the new anchor bolt can develop large pullout strengths while the anchors can be made of materials that are readily available in the market.

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Failure Analysis of PSA applied electronics in home appliances (전자제품 적용 감압성 점착제(PSA)의 고장분석)

  • Kim, So-Yeon;In, Tae-Kyung;Kim, Jin-Woo;Kim, Myung-Su
    • Journal of Applied Reliability
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    • v.9 no.4
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    • pp.331-341
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    • 2009
  • PSA (Pressure Sensitive Adhesive) is used for various purposes in electronic appliances such as double-sided tape for fitting parts, product's name plate, and surface protecting film, and so forth. In several kinds of PSAs, this paper dealt with the failure analysis of PET (Polyethylene Terephthalate) acrylic adhesive tapes. The causes of interface failure were investigated through the test of adhesive strength, thickness, and structure. And test standard methods to prevent recurrences were established.

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Shear Bond Strength Between Zirconia and Porcelain (지르코니아와 포세린의 전단결합강도)

  • Kim, Sa-Hak
    • Journal of Technologic Dentistry
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    • v.33 no.1
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    • pp.1-6
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    • 2011
  • Purpose: To examine the shear bond strengths of zirconia and veneering ceramic according to their surface processing. Methods: The test samples were divided into three groups: one without zirconia surface processing, one sandblasted, and one sandblasted then 3% etched. Then veneering ceramic was fired on all test samples, and their shear bond strengths were measured. Results: The test samples of the control group (Z1) showed the lowest shear bond strengths of $21.82{\pm}1.02$ MPa. The shear bond strengths of Z2 and Z3 ($28.25{\pm}0.72$ and $26.23{\pm}0.82$ MPa, respectively) were relatively higher than those of the control group. The fracture surface of the control group showed adhesive fractures while the test groups had relatively large numbers of cohesive fractures. Conclusion: The shear bond strength was high in the test groups with surface processing while the fracture surfaces showed compound fractures of adhesive and cohesive fractures.

Utilization of Pyrolysis Oil from Pine Wood as Thermosetting Wood Adhesive Resins

  • Kim, Jae-Woo;Myers, Deland J.;Brown, Robert C.;Kuo, Monlin
    • Journal of the Korean Wood Science and Technology
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    • v.35 no.2
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    • pp.51-60
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    • 2007
  • In this study, the possibility of using pyrolysis oil as wood adhesives was explored. Especially, adhesives were formulated by reacting pyrolysis oil and formaldehyde and also partially replacing phenol with pyrolysis oil in phenol-formaldehyde (PF) adhesive and soy hydrolizate/PF adhesive formulation. The pine wood was fast pyrolyized and the oils were obtained from a series of condensers in the pyrolysis system. The oils from each condenser were first reacted with formaldehyde to explore potential use of the oil itself as adhesive. The lap-shear bond strength test results indicated that the oil itself could be polymerized and form bonds between wood adherends. The oils from each condenser were then mixed together and used as partial replacement of phenol (25, 33, and 50% by weight) in phenol-formaldehyde adhesive. The bond strength of the oil containing PF adhesives was decreased as percent phenol replacement level increased. However, no significant difference was found between 25 and 33% of phenol replacement level. The oil-contained PF resins at 25, 33, and 50% phenol replacement level with different NaOH/Phenol (Pyrolysis oil) molar ratio were further formulated with soy hydrolizate to make soy hydrolizate/pyrolysis oil-phenol formaldehyde adhesive at 6:4 weight (wt) ratio and used for fiberboard manufacturing. Surface internal bond strength (IB) of the boards bonded with 33% replacement at 0.3 NaOH/Phenol (Pyrolysis oil) molar ratio performed better than other replacement levels and molar ratios. Thickness swelling after 24 hr cold water soaking and after 2 hr in boiling water was increased as % replacement of pyrolysis oil increased.

Mechanical Properties of Metal/Ceramic FGM made by Thermal Spraying Method (용사법에 의해 제작된 금속/세라믹 경사기능 재료의 기계적 특성)

  • Kim, Y.S.;Nam, K.W.;Kim, H.S.;Oh, M.S.;Kim, K.S.
    • Journal of Power System Engineering
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    • v.2 no.3
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    • pp.41-48
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    • 1998
  • This study was aimed at development of fabrication process of functionally graded materials(FGM), consisting of metal and ceramic by thermal spraying method. NiCrAIY/$Al_2O_3$ FGM were made by using plasma spraying onto the SS400 carbon steel substrate. And mechanical properties such as microhardness, thermal shock resistance and adhesive strength of the coating layer were investigated. Adhesive strength was evaluated by acoustic emission method. It was resulted that NiCrAIY/$Al_2O_3$ FGM made by thermal spraying method showed excellent thermal shock resistance and adhesive strength compared to the other lamellar structures of sprayed coatings and that AE is useful tool to evaluate the defect of thermal sprayed coating layer.

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Manufacture Technology Development of Paper Mending Tape for Conservation of Archive Document (종이 기록물 보수용 안전 테이프 시제품 제조 기술 연구)

  • Shin, Joung-Soon;Yoo, Sun-Kyun
    • Journal of the Korean Graphic Arts Communication Society
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    • v.29 no.3
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    • pp.41-53
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    • 2011
  • For manufacturing the tape for repairing archival documents, we tested ten carrier candidates for selecting best material. The tensile strength, transmissivity, stability of deterioration, and processability were determined. Physical-chemical characteristics and stability of deterioration was best to the Hanji. Tensile strength and transmissivity was best in tracing paper, but was low in oil paper, white sketch paper, lyon coat paper. Synthetic carrier to tensile strength showed higher than paper carrier and to the transmissivity showed 2-8 times higher than paper carriers. The tracing paper to the transmissivity was 10 times higher than others. To determine characteristic of conservation to the selected carriers, stability of deterioration was examined at conditions of $90^{\circ}C$ for 15 days. Oil paper and white sketch paper turned strongly yellowish. Cellulopane, Felt, and Cpp film showed stable stability of deterioration, but deformation like wrinkles. PET film and Syntheletic film showed excellent conservation characteristics without any change of exterior. Test of adhesive uniform between carriers and adhesive processability was performed. PET film > Syntheletic film > Tracing Paper in order were determined. Ununiformal adhesive characteristics appeared to Hangi. Accordingly, we thought that Hanji as carrier material might be unsuitable because of low adhesive processability.