• 제목/요약/키워드: Adhesion control

검색결과 661건 처리시간 0.031초

FTS형 이온 플레이팅의 특성 및 박막 형성에 관한 연구 (A Study on the Characteristics of FTS Type Ion Plating System and Thin film Deposition)

  • 성열문;이창영;신중홍;김규섭;조정수;박정후
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1994년도 하계학술대회 논문집 C
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    • pp.1589-1592
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    • 1994
  • We developed the ion plating system, consisted of the Facing Target Magnetron Sputtering System and the r.f, electrode of the coil type, which was available to control the reactive and the adhesion between thin film and substrate, and studied about the discharge characteristics and the optimum condition in order to form the high quality thin film. The characteristics of discharge and plasma was measured as Double Probe and Electrostatic Retarding Grid Analyzer. The incident ion energy on the substrate was increased as the increasing r.f power, bias voltage. By the r.f electrode, the ionization rate of the sputtered particles was about 75%, and the mean incident ion energy depend on the value which was difference between the plasma potential and biased substrate potential.

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자장을 이용한 이온화율 증대형 삼극형 BARE에서 이온화율의 증대경향과 QMS를 이용한 이온의 에너지 분포 측정 (Measurement of Ion Energy Distribution using QMS & Ionization Enhancement by usign Magnetic Field in Triod BARE)

  • 김익현;주정훈;한봉희
    • 한국표면공학회지
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    • 제24권3호
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    • pp.119-124
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    • 1991
  • Recently, the trend of research in hard coating is concentrate on developing the process of ionization rate under low operating pressure, to get the thin film with high adhesion and dense microstructures. In this study ionization rate enhancement type PVD process using permanent magnet is developed, which enhances the ionization rate by confining the plasma suppressing the wall loss of electron. By the result to investigate the characteristic of glow discharge, the ionization rate of this process is enhanced about twice as high as that of triod BARE process (about 26%), and more dense TiN microstructures are obtained in this process. Cylindrical ion energy analyzer is made and attached in front of a quadrupole mass filter for the analysis of the energy distribution of reactive gas and activated gas ions from the plasma zone. To analyze the operation mechanism of ion energy analyzer, computer simulation is performed by calculation the electric field environment using finite element method. By these analyses of ion energy distribution of outcoming ions from the plasma zone, it is found that magnetic field enhances ion kinetic energy as well as ionization rate. The other results of this study is that the foundation of feed-back system is constructed, which automatically control the partial pressure of reactive gas. In can be possible by recording the data of mass spectrum and ion energy analysis using A-D converter.

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Nanotube shape on the Ti-29Nb-xHf alloys with applied potentials

  • Park, Seon-Yeong;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2016년도 추계학술대회 논문집
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    • pp.119-119
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    • 2016
  • Over the last years the anodic formation of ordered $TiO_2$ nanotube layers has created significant scientific interest. Titanium oxide nanotube formation on the titanium or titanium alloy surface is expected to be important to improve cell adhesion and proliferation under clinical conditions. It should be possible to control the nanotube size and morphology for biomedical implant use by controlling the applied voltage, alloying element, current density, anodization time, and electrolyte. $TiO_2$ nanotubes show excellent biocompatibility, and the open volume in the tubes may be exploited as a drug release platform and so on. Therefore, in this study, Nanotube shape on the Ti-29Nb-xHf alloys with applied potentials was reserched. $TiO_2$ nanotube formation on Ti-29Nb-xHf alloys was carried out using anodization technique as a function of applied DC potential (10 V to 30 V and 30 V to 10 V) and anodization time for 60~120 min in $1MH_3PO_4$ with small additions of (0.8 wt. %, to 1.2 wt. %) NaF. The morphology change of anodized Ti-29Nb-xHf alloys was determined by FE-SEM, XRD, and EDS.

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A review on the medicinal potentials of ginseng and ginsenosides on cardiovascular diseases

  • Lee, Chang Ho;Kim, Jong-Hoon
    • Journal of Ginseng Research
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    • 제38권3호
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    • pp.161-166
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    • 2014
  • Ginseng is widely used for its promising healing and restorative properties as well as for its possible tonic effect in traditional medicine. Nowadays, many studies focus on purified individual ginsenoside, an important constituent in ginseng, and study its specific mechanism of action instead of whole-plant extracts on cardiovascular diseases (CVDs). Of the various ginsenosides, purified ginsenosides such as Rb1, Rg1, Rg3, Rh1, Re, and Rd are the most frequently studied. Although there are many reports on the molecular mechanisms and medical applications of ginsenosides in the treatment of CVDs, many concerns exist in their application. This review discusses current works on the countless pharmacological functions and the potential benefits of ginseng in the area of CVDs. Results: Both in vitro and in vivo results indicate that ginseng has potentially positive effects on heart disease through its various properties including antioxidation, reduced platelet adhesion, vasomotor regulation, improving lipid profiles, and influencing various ion channels. To date, approximately 40 ginsenosides have been identified, and each has a different mechanism of action owing to the differences in chemical structure. This review aims to present comprehensive information on the traditional uses, phytochemistry, and pharmacology of ginseng, especially in the control of hypertension and cardiovascular function. In addition, the review also provides an insight into the opportunities for future research and development on the biological activities of ginseng.

Cohesive Interface Model on Concrete Materials

  • Rhee In-Kyu;Roh Young-Sook
    • 콘크리트학회논문집
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    • 제17권6호
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    • pp.1053-1064
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    • 2005
  • The mechanical damage of concrete is normally attributed to the formation of microcracks and their propagation and coalescence into macroscopic cracks. This physical degradation is caused from progressive and hierarchical damage of the microstructure due to debonding and slip along bimaterial interfaces at the mesoscale. Their growth and coalescence leads to initiation of hairline discrete cracks at the mesoscale. Eventually, single or multiple major discrete cracks develop at the macroscale. In this paper, from this conceptual model of mechanical damage in concrete, the computational efforts were made in order to characterize physical cracks and how to quantify the damage of concrete materials within the laws of thermodynamics with the aid of interface element in traditional finite element methodology. One dimensional effective traction/jump constitutive interface law is introduced in order to accommodate the normal opening and tangential slips on the interfaces between different materials(adhesion) or similar materials(cohesion) in two and three dimensional problems. Mode I failure and mixed mode failure of various geometries and boundary conditions are discussed in the sense of crack propagation and their spent of fracture energy under monotonic displacement control.

부유선별법을 적용한 탈묵공정의 계면화학적 및 수력학적 원리(II) -수력학적 원리를 중심으로- (Interface Chemical and Hydrodynamic Aspects of Deinking Process Using Flotation for Waste paper Recycling(II))

  • Sun-Young Park
    • 자원리싸이클링
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    • 제5권4호
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    • pp.11-16
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    • 1996
  • 부유선별법에 의한 탈묵공정에서 잉크입자와 기포의 부착은 상호간의 충돌에 의한 것인데, 충돌의 가능성은 주로 수력학적 조건에 지배된다. 따라서, 부유선별법에서 미세입자의 제거효율이 낮은 이유는 수력학적 영향에 의해 입자가 기포주위의 수층유선을 따라 흘러내리는 경향이 있으므로 기포와의 충돌이 어렵기 때문이라고 해석되어 진다. 또한, 크고 무거운 잉크입자의 경우에는 기포에 의한 부상과정에서 중력과 점성력 등의 영향을 크게 받으므로 부유선별에 의한 제거가 어렵다고 간주되어 진다. 따라서, 부유선별의 실제공정에서는 계면화학적 측면에서의 조건선정 뿐만 아니라, 잉크입자와 기포의 크기를 조절하는 수력학적 관점에서의 조절이 또한 중요하다.

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MOCVD 방법으로 증착된 TaN와 무전해도금된 Cu박막 계면의 열적 안정성 연구 (Thermal Stability of the Interface between TaN Deposited by MOCVD and Electroless-plated Cu Film)

  • 이은주;황응림;오재응;김정식
    • 한국전기전자재료학회논문지
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    • 제11권12호
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    • pp.1091-1098
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    • 1998
  • Thermal stability of the electroless deposited Cu thin film was investigated. Cu/TaN/Si multilayer was fabricated by electroless-depositing Cu thin layer on TaN diffusion barrier layer which was deposited by MOCVD on the Si substrate, and was annealed in $H_2$ ambient to investigate the microstructure of Cu film with a post heat-treatment. Cu thin film with good adhesion was successfully deposited on the surface of the TaN film by electroless deposition with a proper activation treatment and solution control. Microstructural property of the electroless-deposited Cu layer was improved by a post-annealing in the reduced atmosphere of $H_2$ gas up to $600^{\circ}C$. Thermal stability of Cu/TaN/Si system was maintained up to $600^{\circ}C$ annealing temperature, but the intermediate compounds of Cu-Si were formed above $650^{\circ}C$ because Cu element passed through the TaN layer. On the other hand, thermal stability of the Cu/TaN/Si system in Ar ambient was maintained below $550^{\circ}C$ annealing temperature due to the minimal impurity of $O_2$ in Ar gas.

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Electrical Properties of Organic/Inorganic Hybrid Composites for Insulation Materials

  • Kim, Sang-Cheol;Ok, Jeong-Bin;Aho, Myeong-Jin;Park, Do-Hyun;Lee, Gun-Joo
    • Transactions on Electrical and Electronic Materials
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    • 제3권1호
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    • pp.9-13
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    • 2002
  • In this work, the surface of inorganic fillers were modified with some functional groups such as stearic acid, aliphatic long chain, vinylsilane and aminosilane to control the interaction between inorganic fillers and polymer matrix. Ethylene-vinyl acetate copolymers (EVA) with various amount of vinyl-acetate and copolyether-ester elastomer were used as polymer matrix. The addition of inorganic fillers increases flame retardancy, but results in steep drop of electrical and mechanical properties, which may be caused by the defects in the interface between organic/inorganic hybrid composites. The hybrid composites are found to show better mechanical properties and higher volume resistivities as inorganic fillers are well dispersed and have good adhesion with polymer matrix. Also, the most effective type of functional group coated on fillers depends on the chemical structure of polymer.

수열합성법에 의한 3차원 ZnO 나노구조체 합성 (Synthesis of 3D Nanostructured Flower-like ZnO Architecture on ZnO Thin-film by Hydrothermal Process)

  • 유범근;박용욱;강종윤;김진상;윤석진
    • 한국전기전자재료학회논문지
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    • 제22권10호
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    • pp.884-889
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    • 2009
  • Recently, the control of size, morphology and dimensionality in inorganic materials has been rapidly developed into a promising field in materials chemistry. 3D nanostructured flower-like ZnO architecture with different size and shapes have been simply synthesized by hydrothermal process, using zinc acetate and ammonium hydroxide as reactants. In this study, the ZnO thin-films were deposited by RF magnetron sputtering in other to get high adhesion and uniformity of 3D nanostructured flower-like ZnO architecture on a $SiO_2$ substrate. The XRD patterns identified that the obtained the nanocrystallized ZnO architecture exhibited a wurtzite structure. SEM images illustrated that the flower-like ZnO bundles consisted of flower-like or chestnut bur, which were characterized by polycrystalline and (002) preferential orientation.

Effect of CrN barrier on fuel-clad chemical interaction

  • Kim, Dongkyu;Lee, Kangsoo;Yoon, Young Soo
    • Nuclear Engineering and Technology
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    • 제50권5호
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    • pp.724-730
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    • 2018
  • Chromium and chromium nitride were selected as potential barriers to prevent fuel-clad chemical interaction (FCCI) between the cladding and the fuel material. In this study, ferritic/martensitic HT-9 steel and misch metal were used to simulate the reaction between the cladding and fuel fission product, respectively. Radio frequency magnetron sputtering was used to deposit Cr and CrN films onto the cladding, and the gas flow rates of argon and nitrogen were fixed at certain values for each sample to control the deposition rate and the crystal structure of the films. The samples were heated for 24 h at 933 K through the diffusion couple test, and considerable amount of interdiffusion (max. thickness: $550{\mu}m$) occurred at the interface between HT-9 and misch metal when the argon and nitrogen were used individually. The elemental contents of misch metal were detected at the HT-9 through energy dispersive X-ray spectroscopy due to the interdiffusion. However, the specimens that were sputtered by mixed gases (Ar and $N_2$) exhibited excellent resistance to FCCI. The thickness of these CrN films were only $4{\mu}m$, but these films effectively prevented the FCCI due to their high adhesion strength (frictional force ${\geq}1,200{\mu}m$) and dense columnar microstructures.