• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1997년도 추계학술대회 논문집
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• pp.331-334
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• 1997

The electrical and physical charateristics of aluminum oxide and Pt thin films on it, deposited by reactive sputtering and DC magnetron sputtering, respectively, were analysed with increasing annealing temperature(400~80$0^{\circ}C$) by four point probe, SEM and XRD. Under $600^{\circ}C$ of annealing temperature, aluminum oxide had the properties of improving Pt adhesion to SiO$_2$and insulation without chemical reaction to Pt thin films and the resistivity of Pt thin finns was improved. But these properties of aluminum oxide and Pt thin finns on it were degraded over $700^{\circ}C$ of annealing temperature because aluminum oxide was changed into metal aluminum and then reacted to Pt thin films deposited on it. The thermal characteristics of Pt micro heater were analysed with Pt-RTD integrated on the same substrate. In the analysis of properties of Pt micro heater. active area was smaller size, Pt micro heater had better thermal characteristics. Temperature of Pt micro heater fabricated on membrane was up to 34$0^{\circ}C$ with 1.2watts of the heating power due to reduction of the external thermal loss.

• Environmental Engineering Research
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• 제10권3호
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• pp.131-137
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• 2005

The catalytic activity of precious metals(Rh, Pd, Pt) and nickel catalysts supported on ${\gamma}-Al_2O_3\;and\;CeO_2$ in the partial combustion of methane(PCM) to syngas was investigated based on the product distribution in a fixed bed now reactor under atmospheric condition and also on analysis results by SEM, XPS, TPD, BET, and XRD. The activity of the catalysts based on the syngas yield increased in the sequence $Rh(5)/CeO_2{\geq}Ni(5)/CeO_2>>Rh(5)/Al_2O_3>Pd(5)/Al_2O_3>Ni(5)/Al_2O_3$. Compared to the precious catalysts, the syngas yield and stability of the $Ni(5)/CeO_2$ catalyst were almost similar to $(5)/CeO_2$ catalyst, and superior to these of any other catalysts. The syngas yield of $Ni(5)/CeO_2$ catalyst was 90.66% at 1023 K. It could be suggested to be the redox cycle of the successive reaction and formation of active site, $Ni^{2-}$ and the lattice oxygen, $O^{2-}$ produced due to reduction of $Ce^{4-}$ to $Ce^{3-}$.

• 자원환경지질
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• 제31권3호
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• pp.223-233
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• 1998

The environments in the vicinity of the Dalseong mine has been much contaminated by heavy metals related to CuW ore deposit, which is of hydrothermal pipe type mineralized by quartz monzonite in the andesitic rocks. Chalcopyrite and wolframite are major ore minerals and sphalerite, galena and others are associated. To investigate the contamination of heavy metals in plants, samples of plants and soils were analysed by ICP for Fe, Mn, Cu, Pb, Zn, Ni, Co, Cd and Cr. Most of ore-related heavy metals are anomalously high in plants and soils, which were contaminated by the development of Taehan Tungsten Mining Company. The mine produced 48,704 tons (M/T) of 4 wt.% Cu and 1,620 tons (S/T) of 70 wt.% of $WO_3$ during active mining activity from 1961 to 1971 but was closed in 1975. Wild plants growing at the mine area may be used to remove heavy metals form soils, which cause contaminations of plants, stream waters and groundwaters in the vicinity of the mine.

• 공업화학
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• 제23권6호
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• pp.572-576
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• 2012

온실가스인 $CO_2$를 저감하기 위해 Pt계 촉매상 $CO_2$ methanation 반응에 관한 연구를 수행하였다. $Al_2O_3$의 전구체인 AlO(OH)를 열처리하여 지지체로 사용하였으며, 활성금속으로서 Pt를 사용하였다. XRD 분석결과, 활성금속인 Pt가 고르게 잘 분산되었음이 관찰되었으며, 지지체는 gamma phase의 $Al_2O_3$로 존재함을 확인할 수 있었다. 활성실험을 통해 $600^{\circ}C$로 열처리된 $Pt/Al_2O_3$ 촉매가 가장 우수한 전환율 및 선택도를 나타냄을 확인하였다.

• 한국표면공학회지
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• 제40권2호
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• pp.82-90
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• 2007

Crevice corrosion is the accelerated attack occurred in the occluded cell under a crevice on the metal surface. Crevice corrosion behaviors of nickel-based alloys such as Alloy 600 and Alloy 690 were investigated in acidic solution with different chloride ion concentrations. Tests were carried out using the specially designed crevice cell with a very narrow Luggin capillary assembly to measure the potential inside the crevice. It is believed that crevice corrosion in active/passive system like nickel-based alloys has much to do with the properties of passive film and its repassivation characteristics, investigated by the capacitance measurement and by the abrading electrode technique, respectively. An attempt was made to elucidate the relationship between crevice corrosion behaviors, properties of passive film and its repassivation kinetics. Results showed that repassivation rate parameter $n1{\leq}0.6$ and/or $n2{\leq}0.5$ indicated the possible occurrence of crevice corrosion.

• 마이크로전자및패키징학회지
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• 제26권3호
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• pp.15-22
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• 2019

In these days, importance of the power electronic devices and modules keeps increasing due to electric vehicles and energy saving requirements. However, current silicon-based power devices showed several limitations. Therefore, wide band gap (WBG) semiconductors such as SiC, GaN, and $Ga_2O_3$ have been developed to replace the silicon power devices. WBG devices show superior performances in terms of device operation in harsh environments such as higher temperatures, voltages and switching speed than silicon-based technology. In power devices, the reliability of the devices and module package is the critically important to guarantee the normal operation and lifetime of the devices. In this paper, we reviewed the recent trends of the power devices based on WBG semiconductors as well as expected future technology. We also presented an overview of the recent package module and fabrication technologies such as direct bonded copper and active metal brazing technology. In addition, the recent heat management technologies of the power modules, which should be improved due to the increased power density in high temperature environments, are described.

• Smart Structures and Systems
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• 제18권3호
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• pp.471-484
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• 2016

Optical fiber sensors have been proven that they have the potential to detect high-frequency ultrasonic signals, in structural health monitoring field which generally refers to acoustic emission signals from active structural damages and guided waves excited by ultrasonic actuators and propagating in waveguide. In this work, the sensing properties of optical fiber sensors based on Mach-Zehnder interferometer were investigated in the metal plate. Analytical formulas were conducted first to explore the parameters affecting its sensing performances. Due to the simple and definable frequency component, the Lamb wave excited by the piezoelectric wafer was employed to study the sensitivity of the proposed optical fiber sensors with respect to the frequency, rather than the acoustic emission signals. In the experiments, according to above investigations, spiral shape optical fiber sensors with different size were selected to increase their sensitivity. Lamb waves were excited by a circular piezoelectric wafer, while another piezoelectric wafer was used to compare their voltage responses. Furthermore, by changing the excitation frequency, the tuning frequency characteristic of the proposed optical fiber sensor was also investigated experimentally.

• 한국광학회지
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• 제14권3호
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• pp.327-330
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• 2003

본 논문에서는 도파로층이 1.3 $\mu\textrm{m}$ InGaAsP긴 파장 가변 BT(butt-coupled)-DBR(distributed bragg reflector)-LD(laser diode)를 제작하고, 특성을 측정하였다. Butt 결합 성장면의 성장조건을 건식식각과 선택식각 방법과 MOCVD(metal organic chemical vapor deposition)성장으로 최적화 한 후 활성층과 도파로층의 결합 효율을 측정한 결과 결합 효율이 85% 이상으로 나타났으며, 제작된 BT-DBR-LD에 연속전류를 인가 했을 때, 평균 임계전류는 약 21 ㎃, 최대 광출력이 25 ㎽ 이상으로 나타났다. 또한 위상제어 영역과 DBR영역에 각각 25㎃와 50 ㎃의 전류를 주입하여도 급격한 광출력 변화와 포화현상이 나타나지 않았다 이때 최대 파장 가변 폭은 7.4 nm, SMSR비는 40 ㏈이상으로 나타났다.

• 한국분말재료학회지
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• 제25권6호
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• pp.514-522
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• 2018

Layered-double hydroxide (LDH)-based nanostructures offer the two-fold advantage of being active catalysts with incredibly large specific surface areas. As such, they have been studied extensively over the last decade and applied in roles as diverse as light source, catalyst, energy storage mechanism, absorber, and anion exchanger. They exhibit a unique lamellar structure consisting of a wide variety of combinations of metal cations and various anions, which determine their physical and chemical performances, and make them a popular research topic. Many reviewed papers deal with these unique properties, synthetic methods, and applications. Most of them, however, are focused on the form-factor of nanopowder, as well as on the control of morphologies via one-step synthetic methods. LDH nanostructures need to be easy to control and fabricate on rigid substrates such as metals, semiconductors, oxides, and insulators, to facilitate more viable applications of these nanostructures to various solid-state devices. In this review, we explore ways to grow and control the various LDH nanostructures on rigid substrates.

• 한국수소및신에너지학회논문집
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• 제30권3호
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• pp.209-219
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• 2019

Methanol is a liquid fuel which could also be produced from renewable energy sources and has appreciably high energy density. In this work, we investigated the application of $Ce_{0.9}Gd_{0.1}O_{2-x}$ supported Cu and Ni catalysts for hydrogen production via methanol steam reforming. Catalysts were synthesized by solution combustion synthesis. The prepared catalysts with various active materials and Cu loading amounts were tested in a reactor at $200-300^{\circ}C$, 0-5 barg range and steam to methanol molar ratio was 1.5. The catalytic properties of Cu and Ni were compared, and the catalytic performance was shown to depend on the amounts of metal loading and operating conditions such as reaction temperature and pressure.