• 제목/요약/키워드: Acid washing

검색결과 382건 처리시간 0.022초

발효주정 첨가 저염 미더덕(Styela clava) 양념젓갈의 제조 및 품질 (Processing and Quality Analysis of Seasoned Low-salt Fermented Styela clava Supplemented with Fermentation Alcohol for Extended Shelf-life)

  • 황영숙;이현진;황석민;오광수
    • 한국수산과학회지
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    • 제54권1호
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    • pp.1-8
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    • 2021
  • In order to develop value-added low-salt fermented seafood with a long shelf-life, we prepared seasoned low-salt fermented Mideoduck (Styela clava) supplemented with fermentation alcohol (SME). The SME was produced by washing and dewatering shelled Mideoduck, followed by cutting and salting for 24 h at 0℃. The salted Mideoduck was seasoned and fermented with ingredients, including garlic, ginger, monosodium glutamate, red pepper, sesame, sorbitol and sugar, for 7-8 days at 0℃. After adding 3-5% fermentation alcohol, the Mideoduck was packed in a polyester container. The salinity, volatile basic nitrogen, and amino nitrogen content of the SME was 4.5%, 20.9 mg/100 g and 92.0 mg/100 g, respectively. In comparison with the control, the addition of 3-5% fermentation alcohol showed inhibitory effects of decreased freshness, texture degradation, and growth of residual bacteria. Additionally, the SME had good storage stability and organoleptic qualities when stored at 4±1℃ for 40 days. Therefore, it is suitable for commercialization as a seasoned low-salt fermented product with a long shelf-life. The total amino acid content of the SME was 11,774.5 mg/100 g, majorly comprising glutamic acid, aspartic acid, lysine, arginine, and leucine, and the free amino acid content was 506.4 mg/100 g, majorly comprising hydroxyproline, taurine, and glutamic acid.

국내산 참나무속 수종 잎의 추출성분 (Chemical Constituents of Domestic Quercus spp. Leaves)

  • 김진규;배영수
    • Journal of the Korean Wood Science and Technology
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    • 제34권6호
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    • pp.61-71
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    • 2006
  • 국내산 주요 참나무류인 신갈나무, 상수리나무, 떡갈나무, 졸참나무, 갈참나무 및 상수리나무 잎의 추출성분의 구조를 규명하고 수종 상호간의 성분의 특성 및 상호 연관성 등을 조사하였다. 신갈나무에서는 gallic acid, (+)-catechin, (-)-epicatechin, (+)-gallocatechin, kaempferol, a stragalin, astragalin-6"-O-gallate, isoquercirin, isoquercitrin-6"-O-gallate 및 myricetin 등 10종의 화합물이 단리되었고 상수리나무에서는 gallic acid, kaempferol과 quercetin이 떡갈나무에서는 gallic acid, (+)-catechin, (-)-epicatechin, (+)-galocatechin, (-)-epigallocatechin, kaempferol, quercetin, guajaverin 및 tamarixin 등 9종의 화합물이 단리되었으며 갈참나무에서는 gallic acid, caffeic acid, astragalin, quercetin과 isoquercitrin이 졸참나무에서는 gallic acid, (+)-catechin, (-)-epicatechin, kaempferol, quercitrin, isoquercitrin 및 myricetin 등 7종의 화합물이 단리되었고 굴참나무에서는 gallic acid, (+)-catechin, astragalin, astagalin-6"-O-gallate와 isoquercitrin 등 5종의 화합물이 단리되었다. Gallic aicd는 모든 수종에서 단리되어 참나무류 잎 추출성분의 지표 화합물로 이용될 수 있다.

Quantification of Karanjin, Tannin and Trypsin Inhibitors in Raw and Detoxified Expeller and Solvent Extracted Karanj (Pongamia glabra) Cake

  • Panda, A.K.;Sastry, V.R.B.;Kumar, A.;Saha, S.K.
    • Asian-Australasian Journal of Animal Sciences
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    • 제19권12호
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    • pp.1776-1783
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    • 2006
  • Despite being a rich source of protein (28-34%), karanj (Pongamia glabra) cake is found to be bitter in taste and toxic in nature owing to the presence of flavonoid (karanjin), tannin and trypsin inhibitor, thereby restricting its safe inclusion in poultry rations. Feeding of karanj cake at higher levels (>10%) adversely affected the growth performance of poultry due to the presence of these toxic factors. Therefore, efforts were made to detoxify karanj cake by various physico-chemical methods such as dry heat, water washing, pressure cooking, alkali and acid treatments and microbiological treatment with Sacchraromyces cerevisiae (strain S-49). The level of residual karanjin in raw and variously processed cake was quantified by high performance liquid chromatography and tannin and trypsin inhibitor was quantified by titrametric and colorimetric methods, respectively. The karanjin, tannin and trypsin inhibitor levels in such solvent and expeller pressed karanj cake were 0.132, 3.766 and 6.550 and 0.324, 3.172 and 8.513%, respectively. Pressure-cooking of solvent extracted karanj cake (SKC) substantially reduced the karanjin content at a cake:water ratio of 1:0.5 with 30-minute cooking. Among chemical methods, 1.5% (w/w) NaOH was very effective in reducing the karanjin content. $Ca(OH)_2$ treatment was also equally effective in karanjin reduction, but at a higher concentration of 3.0% (w/w). A similar trend was noticed with respect to treatment of expeller pressed karanj cake (EKC). Pressure cooking of EKC was effective in reducing the karanjin level of the cake. Among chemical methods alkali treatment [2% (w/w) NaOH] substantially reduced the karanjin levels of the cake. Other methods such as water washing, dry heat, HCl, glacial acetic acid, urea-ammoniation, combined acid and alkali, and microbiological treatments marginally reduced the karanjin concentration of SKC and EKC. Treatment of both SKC and EKC with 1.5% and 2.0% NaOH (w/w) was the most effective method in reducing the tannin content. Among the various methods of detoxification, dry heat, pressure cooking and microbiological treatment with Saccharomyces cerevisiae were substantially effective in reducing the trypsin inhibitor activity in both SKC and EKC. Based on reduction in karanjin, in addition to tannin and trypsin inhibitor activity, detoxification of SKC with either 1.5% NaOH or 3% $Ca(OH)_2$, w/w) and with 2% NaOH were more effective. Despite the effectiveness of pressure cooking in reducing the karanjin content, it could not be recommended for detoxification because of the practical difficulties in adopting the technology as well as for economic considerations.

김 양식망의 파래류 제거 및 세척 효과 증대를 위한 공기방울처리장치의 활용 (Utilization of air bubble device to improve removal Ulva linza and cleaning effects from Pyropia nets)

  • 이학증;김영희;남지연;김찬송;허진석
    • 환경생물
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    • 제41권4호
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    • pp.706-711
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    • 2023
  • 본 연구에서는 김활성처리제와 부가장치인 공기방울처리장치의 효과를 검증하고자 양식현장에서 잎파래 제거와 부착 이물질 세척 효과를 조사하였다. 그 결과 김활성처리제만 처리하였을 때보다 물리적 처리방법인 공기방울처리장치를 혼합하여 처리하였을 때 잎파래 제거에 유의적인 영향을 미치지는 않았으나 김 양식망의 이물질 세척 효과는 향상되었다. 이러한 연구 결과를 통해 공기방울처리장치를 혼합 사용한다면 김활성처리제의 사용량을 줄일 수 있으며 친환경적으로 이물질을 제거하여 김의 생산성과 품질을 향상시킬 수 있을 것으로 판단된다.

BTCA처리 면직물의 질소계양이온화제 첨가에 의한 염색성 향상에 관한 연구 (A study on Improving the Dyeability of BTCA treated Cotton Fabrics Containing Nitrogenous Cationic Additives)

  • 박은경;유효선
    • 한국의류학회지
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    • 제24권6호
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    • pp.819-827
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    • 2000
  • The purpose of this study is to produce cotton fabric having improved dyeability and colorfastness as well as retaining the desirable durable press property. When cotton fabric was treated with additives, nitrogen content was increased as the additive concentration was increased. DP ratings and wrinkle recovery properties of BTCA treated cotton fabrics were greatly increased. But DP rating was lowered slightly by adding additives and wrinkle recovery property was decreased with the increase of additive concentration. Tensile strength was decreased by BTCA treatment but increased as additive concentration was increased. Various BTCA/additive treatments produced great affinity for reactive and acid dyes when dyebaths were adjusted at pH 3. It was showed that dyeability was increased as additive concentration was increased. The most effective additive for improving the dyeing properties of the crosslinked cotton was TEAㆍHCl. In case of reactive dye, there was almost no improvement on the dyeability of finished cotton by adding salt. Color fastness to washing and light of finished and dyed cotton were low except for the washfastness of reactive dye. Dyeing the BTCA/additive treated cotton fabrics with reactive dye had no effect on the physical properties.

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Quantitative Assay for the Binding of Jun-Fos Dimer and Activator Protein-1 Site

  • Lee, Sang-Kyou;Park, Se-Yeon;Jun, Gyo;Hahm, Eun-Ryeong;Lee, Dug-Keun;Yang, Chul-Hak
    • BMB Reports
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    • 제32권6호
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    • pp.594-598
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    • 1999
  • The Jun and Fos families of eukaryotic transcription factors form heterodimers capable of binding to their cognate DNA enhancer elements. We are interested in searching for inhibitors or antagonists of the binding of the Jun-Fos heterodimer to the activator protein-1 (AP-1) site. The basic-region leucine zipper (bZIP) domain of c-Fos was expressed as a fusion protein with glutathione S-transferase, and allowed to form a heterodimer with the bZIP domain of c-Jun. The heterodimer was bound to glutathione-agarose, to which were added radiolabeled AP-1 nucleotides. After thorough washing, the gel-bound radioactivity was counted. The assay is faster than the coventional electrophoretic mobility shift assay because the gel electrophoresis step and the autoradiography step are eliminated. Moreover, the assay is very sensitive, allowing the detection of picomolar quantities of nucleotides, and is not affected by up to 50% dimethylsulfoxide, a solvent for hydrophobic inhibitors. Curcumin and dihydroguaiaretic acid, recently known inhibitors of Jun-Fos-DNA complex formation, were applied to this Jun-GST-fused Fos system and revealed to decrease the dimer-DNA binding.

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아민기를 도입한 면직물의 염색성에 관한 연구 (A Study on the Dyeability of the Aminized Cotton Fabrics)

  • 최연주;유효선
    • 한국의류학회지
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    • 제19권1호
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    • pp.51-56
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    • 1995
  • Cotton fabric was treated with acrylonitrile in t-butyl alcohol and then aminized by reduction of the resultant cyanoethyl cellulose with LiAIH4, under various temperatures and times. Aminized cotton fabric toras dyed with acid and reactive dye. Dyeability as to temperatures, pH, and color fastness were compared to the amiRe group content of treated cotton fabrics. The results of this study were as follow: 1. D.S of cyanoethyl cellulose has been increased by increasing treating temperatures and times. Maximum D.S of cyanoethyl cellulose was 1.45. By SEM and the tensile strength, the damage of the treated cotton was not observed. 2. Since aminized cotton has greater affinity on acid dye than untreated cotton, dyeability increased with the increase of amino group content, and the lower pH, $60^{\circ}C$. 3. Since amino group in aminized cotton changes surface charge of cotton, dyeability for reactive dye increased by increasing the amino group content. Optimum dyeability was obtained at pH 5-7, $40^{\circ}C$. And dyeability of the amine treated cotton increased with the NaCl conc. 4. Color fastness to washing & light of the amine treated cotton was very low except for the wash fastness of the reactive dye.

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수용액 중 극미량 니켈(II)과 아연(II)의 흡착농축 및 ICP-AES 정량에 관한 연구 (Adsorptive Preconcentration and ICP-AES Determination for Trace Amount of Ni(II) and Zn(II) in Aqueous Solution)

  • 최종문;최선도
    • 한국환경보건학회지
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    • 제31권1호
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    • pp.73-78
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    • 2005
  • A determination method of trace Ni(II) and Zn(II) in aqueous solution was studied and developed by adsorbing on titanium dioxide. For this purpose, several conditions were optimized such as the pH of sample solution, adsorption time, the types and concentration acid, and desorption time. The titanium dioxide was added in sample solution which was pH adjusted. Then, the sample solution was stirred for 5 minutes. This mixture was stored in room temperature for 30 minutes to allow adsorption. After filtering and washing the titanium dioxide, the analytes were dissolved from the titanium dioxide on membrane filter by an ultrasonic vibration for 10 minutes in 1.0 M $HNO_3$ solution. Then, this sample solution was analysed using ICP-AES. The adsorption equilibrium was achieved in 30 minutes. The desorption was the most of effective with 1.0 M(mol/l) nitric acid solution, and desorption time was 10 minutes. This procedure was applied for the analysis of two real samples, i.e., brown seaweed and tangle. The recoveries of Ni(II) and Zn(II) in spiked samples were 89.4${\sim}$98.9% for analytes.

유색배수 처리를 위한 고분자흡착제의 개발과 그 응용(III) ―디에틸아미노에틸화 셀룰로오스계 흡착제― (Development of Polymeric Adsorbents for the Treatment of Colored Waste Waters and It's Applications ―Diethylaminoethylated Cellulosic Adsorbents―)

  • Choe, Ji Eun;Sung, Woo Kyung;Lee, Mee Kyung;Park, Soo Min
    • 한국염색가공학회지
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    • 제5권4호
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    • pp.42-48
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    • 1993
  • In the present work, decoloring of acid dye solution by the diethylaminoethylated cellulosic adsorbents($CA_{DASE}$) was studied with the aim of developing polymeric adsorbents for the treatment of colored wastewaters. To prepare the cellulosic adsorbents, the $CA_{DASE}$ cellulose and polyvinyl alcohol mixture(80 wt% cellulose content) were crosslinked by tryacryloyl hexahydro-s-tryazine(TAHHT), ammonium phosphate and then treated with solutions containing sodium hydroxide and 2-diethylaminoethyl chloride. Batch and flow method were employed to determine decoloring capacity of C $A_{DEAE}$ for C.I.acid yellow 49. $CA_{DASE}$ exhibited much better desorption capacity than activated carbon. Furthermore, the exhausted $$CA{DASE} could be readily regenerated by washing with dilute sodium hydroxide.

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A Pre-treatment Process for Natural Dyeing of Wool to Impar t Durable Antimicrobial Efficacy

  • Raja, A.S.M.;Thilagavathi, G.
    • 한국염색가공학회지
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    • 제23권2호
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    • pp.69-75
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    • 2011
  • A pre-treatment process has been developed for natural dyeing of wool by which the dyed materials have been imparted antimicrobial efficacy against both gram-positive and gram-negative bacteria durable up to 20 washes. In this process, wool fabrics were treated with citric acid under oxidizing condition prior to dyeing. The treated fabrics were then dyed with four different types of natural dye powders obtained from leaves of silver oak, wattle, tanner's senna and flame of forest. All the natural dyes produced yellowish brown colour on wool fabrics. The washing and light fastness properties of the fabrics subjected to pre-treatment were one grade higher compared to those of the dyed fabrics without pre-treatment. The pre-treated wool fabrics showed antimicrobial efficacy against both gram-positive bacteria (Staphylococcus aureus) and gram-negative bacteria (Escherichia coli). The fabrics dyed without pre-treatment showed antimicrobial efficacy against gram-positive bacteria (Staphylococcus aureus) only. The durability of antimicrobial efficacy was higher in pre-treated and dyed wool fabrics compared to the dyed fabrics without pre-treatment.