• Title/Summary/Keyword: 4-ball test

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Evaluation of Pull Strengths and Fracture Modes of Solder Joino by Modified Ball Pull Testing with Protrusion Jaw (Protrusion Jaw가 적용된 볼 당김시험을 이용한 솔더 접합부의 강도와 파괴 메커니즘 분석에 관한 연구)

  • Kim Hyoung-Il;Han Sung-Won;Kim Jong-Min;Choi Myung-Ki;Shin Young-Eul
    • Journal of Welding and Joining
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    • v.23 no.4
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    • pp.34-40
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    • 2005
  • There have been numerous approaches to examine the bonding strengths of solder joints. However, despite the technical and practical limitations, the precedent test methods such as the ball shear and ball pull tests are being used in industrial applications. In this study, the optimum jaw pressure with the modified protrusion jaw was introduced in order to obtain higher successful rate f3r ball pull testing. Furthermore, the pull strengths and fracture modes of Sn-8Zn-3Bi, Sn-4Ag-0.7Cu, and Sn-37Pb eutectic solder after isothermal aging tests ($100^{\circ}C,\;150^{\circ}C$), were evaluated with the protrusion jaw. The pull strength-displacement hysteresis curves and fracture surfaces were carefully investigated to evaluate the correlation between the pull strengths and the fracture modes of each solder. In conclusion, it is verified that Au-Zn IMCs (Intermetallic Compounds) have a detrimental effect on the pull strengths and changed fracture modes of Sn-8Zn-3Bi solder. Meanwhile, the microstructure transformation influences the degradation of pull strengths of Sn-4Ag-0.7Cu and Sn-37Pb solders.

Synthese and Anti-wear Properties of Diol Derivatives Containing Dithiophosphate Group-effect on Main Alkyl Chain and Side Alkyl Chain (Dithiophosphate Group을 함유한 디올유도체의 합성 및 내마모성-말단 알킬기 및 몸체 알킬기의 탄소사슬에 따른 영향)

  • Ko, Kyung-Min;Han, Hye-Rim;Kim, Young-Wun;Kang, Ho-Cheol;Jeong, Noh-Hee
    • Applied Chemistry for Engineering
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    • v.29 no.4
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    • pp.405-412
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    • 2018
  • Three types of bis[3-(dialkyloxylphosphorothionyl) thio-2-methylpropanyloxy]alkane (BAPA) drived from alkane diol were synthesized. The principal chain of each BAPA had a different carbon number, i.e., 6, 9, and 11. The three types of synthesized BAPA were compared to zinc dialkyl dithiophosphates (ZDDPs) in terms of abrasion resistance. A four-ball test was conducted to evaluate the anti-abrasion performance of the synthesized BAPA according to the length of the principal carbon chain. Each product was added to an additive at a concentration of 1% of the base oil weight, and the wear scar diameter (WSD) was measured as 0.472, 0.459, and 0.480 mm, respectively. Among the BAPA compounds, dialkyl dithiophosphoric acid (DDP), which is the side chain of bis[methacryloyloxy] nonane (BMOO9), was synthesized by varying the carbon number, i.e., 4, 8, and 12, and subsequently the 4-ball test was carried out. The WSD was determined as 0.537, 0.459, and 0.531 mm, respectively. As a result, it was found that when a side chain is short, a thin film is formed. In contrast, a long side chain hindered the formation of a film, and hence the best result was achieved when the carbon number was 8. As for the ZDDPs, the WSD was determined to be 0.563 mm, when measured under the same conditions. The measurements confirm that the synthesized BAPA compounds are superior to the ZDDPs as abrasion resistance additives.

Synthesis of Nanosized Cu/Zn Particles in the Base Oil Phase by Hydrothermal Method and Their Abrasion Resistance (기유 내에서 수열합성법에 의한 나노크기의 구리/아연 입자 합성 및 윤활 특성)

  • Kim, Young-Seok;Lee, Ju-Dong;Lee, Man-Sig
    • Journal of the Korean institute of surface engineering
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    • v.40 no.1
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    • pp.11-15
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    • 2007
  • Stable metallic Cu/Zn nanoparticles were prepared in the base oil phase by hydrothermal method. The physical properties, such as crystal structure, crystallite size and crystallinity according to synthesis conditions have been investigated by XRD, FT-IR and TEM. In addition, 4-ball test has been performed in order to investigate the frictional wear properties of prepared nanosized Cu/Zn particles. The peaks of the X-ray diffraction pattern indicate that the particle size was very small and crystallinity of Cu/Zn particles was good. The micrographs of TEM showed that nanosized Cu/Zn particles possessed a spherical morphology with a narrow size distribution. The crystallite size of the Cu/Zn particles synthesized in base oils was 23-30 nm. It was found that the antiwear capacity increases with increasing Cu/Zn concentration. When the concentration of Cu/Zn was 5.0 wt%, the wear scar diameters was 0.38 mm.

Synthesis and Lubricating Properties of Succinic Acid Alkyl Ester Derivatives (숙신산 알킬 에스테르 유도체의 합성 및 윤활특성)

  • Baek, Seung-Yeob;Kim, Young-Wun;Chung, Keun-Wo;Yoo, Seung-Hyun;Park, Su-Jin
    • Applied Chemistry for Engineering
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    • v.22 no.2
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    • pp.196-202
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    • 2011
  • In this paper, a series of alkyl succinic acid esters for base oil were synthesized by condensation reaction of succinic anhydride and fatty alcohol. The structures of the synthesized esters were confirmed by $^1H-NMR$, FT-IR spectrum and GC analysis. Basic properties of esters such as kinematic viscosity (KV), refractive index (RI), total acid number (TAN) and pour points were measured and lubricating properties such as SRV wear scar diameter (SRV WSD), fraction coefficient (COF) and 4-ball wear (4-ball WSD) were also evaluated. As the results of basic properties, KV, RI and pour point of synthetic esters increased as the carbon chain of the esters increased. Measurement value of total acid number (TAN) was indicated between 0.2~4 mgKOH/g, and that metal working fluids and pressure working oils are acceptable to use as base oil. Also, lubricating properties of the esters showed as follows: 0.391~0.689 mm of SRV WSD, 0.110~0.138 of SRV COF and 0.49~0.55 mm of 4-ball WSD depended on the structure of the esters. In a comparison on the lubrication capacity of the SRV test based on polyester TMPTO, SRV WSD result showed that a better performance caused by the alkyl group. On the other hand, SRV COF test was not influenced of the alkyl group which the capacity of the lubricant was sightly diminished than the comparison material, regardless of the alkyl group.

EFFECTS OF AGING AND THERMAL CYCLING ON THE BIAXIAL FLEXURE STRENGTH OF VENEERING RESIN COMPOSITES FOR CROWN (시효처리와 thermal cycling이 치관전장용 복합레진의 2축굽힘강도에 미치는 영향)

  • Jeong, Gwan-Ho;Ha, Il-Soo;Song, Kwang-Yeob
    • The Journal of Korean Academy of Prosthodontics
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    • v.37 no.5
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    • pp.597-606
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    • 1999
  • This study was performed to evaluate the effect of aging and thermal cycling on the biaxial flexure strength of low commercially available veneering resin composites for crown(Dentacolor : DC, Artglass : AG, Esternia : ET and Targis : TG). Disc specimens were fabricated in a teflon mold giving 12mm in diameter and 1mm in thickness. All samples were divided into 4 groups. Group 1 was dried in a dessicator at $25^{\circ}C$ for 30 days. Group 2 was immersed in distilled water at $37^{\circ}C$ for 30 days. Group 3 was immersed in distilled water at $65^{\circ}C$ for 30 days. Group 4 was subjected to 10,000 thermal cycles between $5^{\circ}C\;and\;55^{\circ}C$, and the immersion time in each bath was 15 seconds per cycle. Biaxial flexure test was conducted using the ball-on-three-ball method at the cross head speed of 0.5mm/min and fracture surfaces were observed with scanning electoron microscope. The results obtained were summarized as follows; 1. Weibull modulus values, except for the AG group, decreased after thermal cycling treatment. 2. Biaxial flexure strength values of aging group at $37^{\circ}C$ were the lowest in all sample groups. Except for the DC group, strength values were significantly decreased for the drying group. 3. After thermal cycling test, the highest value of biaxial flexure strength of 188.8 MPa was observed in the ET group and the lowest value of 73.2 MPa was observed in the DC group. The strength values showed the significant differences in each group (p<0.05). 4. Observation of surfaces after thermal cycling test revealed the ditching in the part of surrounding large fillers.

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Effect of lumbar stabilizing exercise using the gym ball on psychosocial status in elderly women with chronic low back pain (짐볼을 이용한 요부안정화 운동이 만성요통 여성노인의 정신사회적 건강수준에 미치는 영향)

  • Park, Jae-Young;Shin, Hyung-Soo;Seo, Byoung-Do
    • PNF and Movement
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    • v.7 no.4
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    • pp.9-16
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    • 2009
  • Objective : The purpose of this study was to analyze the effect on psychosocial status in elderly women with chronic low back pain after practicing lumbar stabilizing exercise using the gym ball, and to developed and activated on exercise program for healthy senile life. Methods : The subjects were 23 elderly women with chronic low back pain. Mean age of subjects was $67{\pm}13$ years. The lumbar stabilizing exercise using the gym ball was performed 3 times a week during the 8 weeks study period. The research tool were ODI(Oswestry Disability Index), VAS(Visual Analogue Scale), SES(Self-esteem Scale), GDSSF-K(Geriatric Depression Scale Short Form Korea Version), PSS (perceived stress scale), Life satisfaction, and MMSE-K. The analysis of data was processed by the statistical program SPSS 12.0 and paired t-test and frequency analysis were used to compare psychosocial status between the pretest and post tests. Result : The lumbar stabilizing exercise using the gym ball increased significantly SES and Life satisfaction of subjects, and ODI, VAS(trunk flexion & trunk extention), GDSSF-K, and PSS were decreased significantly(p<.05). While VAS(trunk rotation) were not significantly. Conclusion : The lumbar stabilizing exercise using the gym ball improved psychosocial status in elderly women with chronic low back pain.

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The Effects of Ball-Based Squats and Narrow Squats on Muscle Thickness, Q Angle and Gap between the Knees in Adults with Genu Varum (볼을 이용한 스쿼트와 내로우 스쿼트가 안굽이 무릎을 가진 성인의 근 두께, Q각 및 무릎 사이 간격에 미치는 영향)

  • Min-Kyu Kim;Hoe-Song Yang;Chan-Joo Jeong;Young-Dae Yoo;Hyo-Jeong Kang
    • Journal of The Korean Society of Integrative Medicine
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    • v.11 no.1
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    • pp.149-157
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    • 2023
  • Purpose : Genu varum is a condition characterized by a wider than normal gap between. This may be due to muscle weakness caused by poor posture, lifestyle, or lack of exercise. This study aimed to compare the effects of ball-based squats and narrow squats on muscle thickness, Q-angle, and the gap between the knees, in order to assess the potential for improving this condition. Methods : Twenty six adult participants with genu varum were randomly assigned to either a ball-based squat group (n=13) or a narrow squats group (n=13). Both groups performed their respective exercises three times weekly for 4 weeks. The data was analyzed using paired t-tests to compare pre- and post- intervention measurements within each group, and independent t-test was used to compare the two groups. Results : Both groups showed significant improvement in the thickness of the vastus lateralis and medialis, and rectus femoris muscles, as well as a significant decrease in the gap between the knees (p<.05). However, there was no significant difference in Q-angle variation between the two group. Furthermore, there was no significant differences in the Q-angle, gap between the knees, and muscle thickness variation between both groups. Conclusion : The results suggest that both ball-based squats and narrow squats are effective in improving muscle thickness and reducing the gap between the knees in adults with genu varum. However, there was no significant difference between the two types of squats in terms of their effects on the Q-angle. These findings highlight the potential for exercise interventions to address this common postural issue.

A Study on the Wear Performances of Dibutyl 3,5-di-t-Butyl 4-Hydroxy Benzyl Phosphonate under Sliding and Rolling Contacts (미끄럼 및 구름접촉하에서 Dibutyl 3,5-di-t-Butyl 4-Hydroxy Benzyl Phosphonate의 마모성는에 관한 연구)

  • 최웅수;한흥구;권오관
    • Tribology and Lubricants
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    • v.7 no.1
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    • pp.40-45
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    • 1991
  • Wear performances for dibutyl 3,5-di-t-butyl 4-hydroxy benzyl phosphonate (DBP) were invesitigated using the four ball test machine under sliding and also rolling contact conditions, and compared with ZDDP. DBP showed excellent antiwear performace compared with ZDDP under severe sliding contact. Also, DBP achieved a longer fatigue life than ZDDP under rolling contact conditions. The surface of the worn balls was observed using an optical microscope, and the wear derbis generated was measured using the Particle Quantifier (PQ).

An Experimental Study on the Engineering Properties of Concrete using Fine Aggregate of PS ball Slag (풍쇄슬래그 잔골재를 사용한 콘크리트의 공학적 특성에 관한 실험적 연구)

  • Lee Sang-Soo;Song Ha-Young;Kim Eul-Yong
    • Journal of the Korea Institute of Building Construction
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    • v.6 no.3 s.21
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    • pp.107-114
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    • 2006
  • In this study, the experiment was carried out to investigate and analyze the engineering properties of concrete using fine aggregate of PS bal slagl. The main experimental variables were water/cement ratio 30, 40, 50(%), water content $170kg/m^3$, replacement ratio of slag fine aggregate 0, 25, 50, 75(%) in experiment I and water/cement ratio 30, 40, 50(%), water content 165, 170, 175($kg/m^3$), replacement ratio of fine aggregate of PS ball 0, 50 in experiment II. According to the test results, the principle conclusions are summarized as follows (1) The workability of slag fine aggregate-mixed concrete tends to improve, as the replacement rate increases. (2) The air content of slag fine aggregate-mixed concrete tends to decrease, as the replacement rate increases. (3) The unit volume weight of slag fine aggregate-mixed concrete tends to significantly increase, as the replacement rate increases. (4) The compressive strength of slag fine aggregate-mixed concrete tends to show more increasing propensity, in case the curing period is relatively long, as the replacement rate increases.

Damage Mechanism of Particle Impact in a $Cr_2O_3$ Plasma Coated Soda-lime Glass ($Cr_2O_3$ 플라스마 용사 코팅된 유리의 입자충격에 의한 손상기구)

  • Suh, Chang-Min;Lee, Moon-Whan;Kim, Sung-Ho;Jang, Jong-Yun
    • Journal of Ocean Engineering and Technology
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    • v.12 no.3 s.29
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    • pp.49-59
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    • 1998
  • The damage mechanism of $Cr_2O_3$ plasma coated soda-lime glass and uncoated glass by steel ball particle impact was analyzed in this study. And the shape variation of the cracks was investigated by stereo-microscope according to the impact velocity and steel ball diameter. In order to improve the damage reduction effect by $Cr_2O_3$ coating layer, crack size was measured and surface erosion state was observed for both of two kinds of specimen after impact experiment. And the results were compared with each other. The 4-point bending test was performed according to ASTM D790 testing method to evaluate the effect of coating layer for bending strength variation. As a result, it was found that the crack size of $Cr_2O_3$ coated specimen was smaller than that of uncoated one, because of the impact absorption by interior pores in the coating layer and the load dispersion by the structural characteristic of the coating layer. For the specimens subjected to the steel ball impact, the bending strength of coated specimen was higher than that of uncoated specimen.

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