• Composites Research
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• 제32권5호
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• pp.216-221
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• 2019

Piecewise Integrated Composite (PIC) 보는 하중 유형에 따라 구간을 나누어, 각 구간마다 하중 유형에 강한 복합재료의 적층 순서를 배열한 보이다. 본 연구에서는 보의 거동을 고려하여 PIC 보의 구간을 머신 러닝을 통해 나누어 기존에 제시되었던 PIC 보에 비해 우수한 굽힘 특성을 갖게 하는 것이 목적이다. FE 모델의 240개 요소가 참조점으로 선택되었다. 선행 유한요소해석은 머신 러닝의 학습데이터 생성을 위하여 규칙적으로 분포된 참조점에서 3축 특성 값(Triaxiality)으로 나타냈다. 3축 특성 값은 인장, 압축 그리고 전단의 하중유형을 나타낸다. 머신 러닝 모델은 하이퍼파라미터(Hyperparameter)와 학습데이터로 구성되었으며, 하이퍼파라미터 튜닝을 통해 적절한 하중 충실도를 도출하였지만, 거동이 큰 보의 옆면에서는 적절하지 않은 하중 충실도가 도출되었다. 이를 해결하기 위하여 고르게 배치한 참조점을 보의 거동에 따라 배치하여 학습 데이터를 얻었고, 머신 러닝 모델이 생성되었다. 앞서 생성된 머신 러닝 모델을 통하여 보가 매핑 되었고, PIC 보에 대하여 유한요소 해석을 진행한 결과, 기존에 제시되었던 PIC 보에 비해 최대하중과 흡수 에너지가 커지는 특성이 나타났다.

• 한국콘텐츠학회논문지
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• 제21권3호
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• pp.602-608
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• 2021

임상에서 사용되는 Co-Cr 합금과 도재 간의 접착 강도를 비교하기 위해 대조군으로 전통적인 주조(Casting) 방법, 실험군으로 Milling(Milling group), SLM(3d printing group) 시편을 제작하여 금속과 도재(ceramic) 간의 접착 강도를 비교 하였다. 합금과 도재간의 접착강도를 측정하기 위해 universal testing machine를 이용하여 3점 굴곡 시험을 시행하고, 결합강도 측정 후 금속-도재간의 계면을 관찰하였다. 금속-도재(ceramic) 간의 실험 결과 casting group 53.59 MPa, milling group 45.90 MPa, 3d printing group 58.34 MPa의 결과값을 보였고, 통계적으로 유의성은 없었다. 파절양상은 두 집단 시편의 대부분이 복합 파절양상(mixed failure)을 보였다. 본 연구는 3D 프린팅로 제작된 합금으로 합금-도재의 결합 강도값을 측정하였을 때 임상적으로 적용 가능한 수치를 보여 주었다.

• The Journal of Advanced Prosthodontics
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• 제14권6호
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• pp.360-368
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• 2022

PURPOSE. This study assessed the physical and mechanical properties of interim crown materials fabricated using various digital techniques after accelerated aging. MATERIALS AND METHODS. Three groups of interim dental restorative materials (N = 20) were tested. The first group (CO) was fabricated using a conventional manual method. The second group (ML) was prepared from prefabricated resin blocks for the milling method and cut into specimen sizes using a cutting disc. The third group (3D) was additively manufactured using a digital light-processing (DLP) 3D printer. Aging acceleration treatments using toothbrushing and thermocycling simulators were applied to half of the specimens corresponding to three years of usage in the oral environment (N = 10). Surface roughness (Ra), Vickers microhardness, 3-point bending, sorption, and solubility tests were performed. A 2-way analysis of variance (ANOVA) and Fisher's multiple comparison test were used to compare the results among the groups. RESULTS. The mean surface roughness (Ra) of the resin after accelerated aging was significantly higher in the CO and ML groups than that before aging, but not in the 3D group. All groups showed reduced hardness after accelerated aging. The flexural strength values were highest in the 3D group, followed by the ML and CO groups after accelerated aging. Accelerated aging significantly reduced water sorption in the ML group. CONCLUSION. According to the tested material and 3D printer type, both 3D-printed and milled interim restoration resins showed higher flexural strength and modulus, and lower surface roughness than those prepared by the conventional method after accelerated aging.

• 한국운동역학회지
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• 제17권1호
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• pp.145-153
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• 2007

The purpose of this study is to compare and analyze the phase-by-phase elapsed time, the COG, the body joint angle changes and the angular velocities of each phase of Handspring Salto Forward Piked performed by 4 college gymnasts through 3D movement analysis program. 1. The average elapsed time for each phase was .13sec for Phase 1, .18sec for Phase 2, .4sec for Phase 3, and .3sec for Phase 5. The elapsed time for Phase 1 to Phase 3 handspring was .35sec on average and the elapsed time for Phase 4 to Phase 5 handspring salto forward piked was .7sec on average. And so it showed that the whole elapsed time was 1.44sec. 2. The average horizontal changes of COG were 93.2 cm at E1, 138. 5 cm at E2, 215.7 cm at E3, 369.2 cm at E4, 450.7 cm at E5, and 553.1 cm at E6. The average vertical changes of COG were 83.1 cm at E1, 71.3 cm at E2, 78.9 cm at E3, 93.7 cm at E4, 150.8 cm at E5, and 97.2 cm at E6. 3. The average shoulder joint angles at each phase were 131.6 deg at E1, 153.5 deg at E2, 135.4 deg at E3, 113.4 deg at E4, 39.6 deg at E5, and 67.5 deg at E6. And the average hip joint angles at each phase were 82.2 deg at E1, 60 deg at E2, 101.9 deg at E3, 161.2 deg at E4, 97.7 deg at E5, and 167 deg at E6. 4. The average shoulder joint angular velocities at each phase were 130.9deg/s E1, 73.1 deg/s at E2, -133.9 deg/s at E3, -194.4 deg/s at E4, 29.4 deg/s at E5, and -50.1 deg/s at E6. And the average hip joint angular velocities at each phase were -154.7 deg/s E1, -96.5 deg/s at E2, 495.9 deg/s at E3, 281.5 deg/s at E4, 90.3 deg/s at E5, and 181.7 deg/s at E6. The results shows that, as for the performance of handspring salto forward piked, it is important to move in short time and horizontally from the hop step to the point to place the hands on the floor and jump, and to stretch the hip joints as much as possible after the displacement of the hands and to keep the hip joints stretched and high in the vertical position at the takeoff. And it is also important to bend the shoulder joints and the hip joints fast and spin as much as possible after the takeoff, and to decrease the speed of spinning by bending he shoulder joints and the hip joints quickly after the highest point of COG and make a stable landing.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2004년도 학술대회지
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• pp.347-351
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• 2004

[ $Si_3N_4$ ] composites have been extensively studied for engineering ceramics, because it has excellent room and high temperature strength, wear resistance properties, good resistance to oxidation, and good thermal and chemical stability. In the present work, carbon short fiber reinforced $Si_3N_4$ ceramics were fabricated by hot press method in $N_2$ atmosphere at $1800^{\circ}C$ using $Al_2O_3\;and\;Y_2O_3$ as sintering additives. Content of carbon short fiber was $0\%,\;0.1\%\;and\;0.3\%$. The composites were evaluated in terms of density, flexural strength and elastic modulus through the 3-point bending test at room temperature. Also, The wear behavior was determined by the pin on disk wear tester using silicon nitride ball. Experimental density and flexural strength decreased with increasing content of carbon fiber. But specific modulus increased with increasing content of carbon fiber. In addition, friction coefficient and specific wear loss decreased with increasing content of carbon short fiber by reason of interfacial defects between matrix and fiber.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2003년도 춘계학술발표강연 및 논문개요집
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• pp.222-222
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• 2003

나노크기 금속입자가 분산된 세라믹 나노복합재료는 향상된 기계적 특성과 함께 독특한 전기적, 자기적 특성을 보여주어 새로운 기능성 재료로의 응용가능성을 갖고 있다. 그러나 소결 중의 반응이나 입자성장 등으로 형성된 반응상 또는 조대한 입자상이 세라믹 기지의 입계 등에 존재한다면, 나노크기 금속상 분산에 의한 기계적 특성의 향상과 독특한 기능성 부여라는 장점들이 없어지게 된다. 따라서 요구되는 특성을 구현할 수 있는 금속분산 나노복합재료의 제조를 위해서는 미세조직 제어를 위한 최적의 제조공정 확립과 미세조직과 특성 등의 관계에 대한 연구가 요구된다. 본 연구에서는 기지상으로 A1$_2$O$_3$를, 분산상으로는 저융점 금속이며 일반적인 A1$_2$O$_3$의 가압소결시에 (약 140$0^{\circ}C$) 액상으로 존재하는 금속 Cu를 선택하여 조성이 5 vol% Cu가 되도록 복합재료를 제조하였다. $Al_2$O$_3$와 CuO 원료분말들은 습식 및 건식 볼 밀링을 통하여 균일한 분말혼합체로 제조되었다. 혼합분말은 열간가압소결기 내에 장입한 후 35$0^{\circ}C$에서 30분 동안 H$_2$가스를 흘려주며 CuO를 Cu로 환원 처리하였다. 계속해서 H$_2$분위기를 유지하며 승온한 후, 각각 1000-145$0^{\circ}C$에서 분위기를 Ar 으로 치환하였다. 소결은 145$0^{\circ}C$에서 30 ㎫의 압력으로 1시간동안 행하였다 소결한 시편들은 직사각형 형태로 가공하였으며 표면은 0.5$\mu\textrm{m}$의 다이아몬드 입자로 연마하였다. XRD, SEM 및 TEM을 이용하여 상분석 및 미세조직관찰을 행하였다. 파괴강도는 3중점 굽힘 법으로 (3-point bending test) 측정하였다. 이때 시편 하부의 지지 점간의 거리는 30mm, cross-head 속도는 0.5 mm/min으로 하였고 5개의 시편을 측정하여 평균값을 구하였다.

• Journal of Welding and Joining
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• 제30권3호
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• pp.26-31
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• 2012

Three-dimensional integrated circuit (3D IC) technology has become increasingly important due to the demand for high system performance and functionality. We have evaluated the effect of Buffered oxide etch (BOE) on the interfacial bonding strength of Cu-Cu pattern direct bonding. X-ray photoelectron spectroscopy (XPS) analysis of Cu surface revealed that Cu surface oxide layer was partially removed by BOE 2min. Two 8-inch Cu pattern wafers were bonded at $400^{\circ}C$ via the thermo-compression method. The interfacial adhesion energy of Cu-Cu bonding was quantitatively measured by the four-point bending method. After BOE 2min wet etching, the measured interfacial adhesion energies of pattern density for 0.06, 0.09, and 0.23 were $4.52J/m^2$, $5.06J/m^2$ and $3.42J/m^2$, respectively, which were lower than $5J/m^2$. Therefore, the effective removal of Cu surface oxide is critical to have reliable bonding quality of Cu pattern direct bonds.

• Composites Research
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• 제35권6호
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• pp.463-468
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• 2022

상용 FFF (Fused filament fabrication) 3D 프린터로 제조된 탄소 단섬유강화 나일론 복합재료 구조의 내부 채움 패턴(Infill pattern)의 높은 공극률은 프린팅 된 구조의 기계적 성능을 결정한다. 본 연구는 프린팅 된 구조의 내부 채움 패턴의 공극률을 줄여서 기계적 특성을 개선하기 위해 사각형 내부 채움 구조로 제작된 Onyx 복합 재료 시편의 열압밀 조건에 따른 시편의 기계적 성능을 실험적으로 평가하고, 가장 우수한 기계적 물성을 유도하는 열압밀 공정 조건(145℃, 4 MPa, 12 min)을 찾았다. 현미경 관찰결과 열압밀 후처리를 겪은 복합재료 시편의 내부 채움 공극률이 효과적으로 줄어듦을 확인하였다. 후처리된 시편의 기계적 성능을 확인하기 위해, 후처리를 하지 않은 대조군 시편과, 후처리 후 밀도와 치수를 동일하게 설정하여 출력한 시편과 함께 인장시험 및 3점 굽힘시험을 수행하여 기계적 물성을 비교한 결과 열압밀 후처리를 수행한 경우 기계적 물성이 효과적으로 개선되는 것을 확인하였다.

• 한국해양공학회지
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• 제25권3호
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• pp.28-33
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• 2011

The thermal shock properties of SiC materials were investigated for high temperature applications. In particular, the effect of thermal shock temperature on the flexural strength of SiC materials was evaluated, in conjunction with a detailed analysis of their microstructures. The efficiency of a nondestructive technique using ultrasonic waves was also examined for the characterization of SiC materials suffering from a cyclic thermal shock history. SiC materials were fabricated by a liquid phase sintering process (LPS) associated with hot pressing, using a commercial submicron SiC powder. In the materials, a complex mixture of $Al_2O_3$ and $Y_2O_3$ powders was used as a sintering additive for the densification of the microstructure. Both the microstructure and mechanical properties of the sintered SiC materials were investigated using SEM, XRD, and a three point bending test. The SiC materials had a high density of about 3.12 Mg/m3 and an excellent flexural strength of about 700 MPa, accompanying the creation of a secondary phase in the microstructure. The SiC materials exhibited a rapid propagation of cracks with an increase in the thermal shock temperature. The flexural strength of the SiC materials was greatly decreased at thermal shock temperatures higher than $700^{\circ}C$, due to the creation of microcracks and their propagation. In addition, the SiC materials had a clear tendency for a variation in the attenuation coefficient in ultrasonic waves with an increase in thermal shock cycles.

• 한국세라믹학회지
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• 제48권5호
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• pp.384-389
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• 2011

Gas pressure sintering (GPS) of reaction bonded silicon nitride (RBSN) was performed using $Lu_2O_3-SiO_2$ additive and the properties were compared with those of specimens prepared using high purity $Si_3N_4$ powder. The relative density of RBSN and compacted $Si_3N_4$ powder were 68.9 and 47.1%, and total linear shrinkage after sintering at $1900^{\circ}C$ were 14.8 and 42.9%, respectively. High nitrogen partial pressure (5MPa) was required during sintering at $1900^{\circ}C$ in order to prevent the decomposition of the nitride and to promote the formation of SiC. The relative density and 4-point bending strength of RBSN and $Si_3N_4$ powder compact were 97.7%, 954MPa and 98.2%, 792MPa, respectively, after sintering at $1900^{\circ}C$. The sintered RBSN also showed high fracture toughness of 9.2MPam$^{1/2}$.