• Journal of the Korean Ceramic Society
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• v.44 no.7
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• pp.343-348
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• 2007

Alumina/silver nanocomposites were fabricated using a soaking method through a sol-gel route to construct an intra-type nanostructure. The pulse electric-current sintering (PECS) technique was used to sinter the nanocomposites. Several specimens were annealed after sintering. The microstructure, mechanical properties, critical frontal process zone (FPZ) size, and thermo-mechanical properties of the nanocomposites were estimated. The relative densities of the specimens sintered at 1350 and $1450^{\circ}C$ were 95% and 99%, respectively. The maximum value of the three-point bending strength was found to be 780 MPa for the $2{\times}2{\times}10 mm$ specimen sintered at $1350^{\circ}C$. The fracture toughness of the specimen sintered at $1350^{\circ}C$ was measured to be $3.60 MPa{\cdot}m^{1/2}$ using the single-edge V-notched beam (SEVNB) technique. The fracture mode of the nanocomposites was transgranular, in contrast to the intergranular mode of monolithic alumina. The fracture morphology suggested that dislocations were generated around the silver nanoparticles dispersed within the alumina matrix. The specimens sintered at $1350^{\circ}C$ were annealed at $800^{\circ}C$ for 5 min, following which the maximum fracture strength became 810 MPa and the fracture toughness improved to $4.21 MPam^{1/2}$. The critical FPZ size was the largest for the specimen annealed at $800^{\circ}C$ for 5 min. Thermal conductivity of the alumina/silver nanocomposites sintered at $1350^{\circ}C$ was 38 W/mK at room temperature, which was higher than the value obtained with the law of mixture.

• International Journal of Highway Engineering
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• v.3 no.1 s.7
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• pp.185-197
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• 2001

This paper dealt with modification of effective crack length model (ECM) by adding Poisson's ratio term to evaluate fracture toughness of asphalt concrete which varies its material property by temperature. The original ECM model was developed for solid materials, such as cement concrete, and Poisson's ratio of materials was not considered. However, since asphalt concrete is sensitive to temperature variation and changes its Poisson's ratio by temperature, it should be taken into consideration to know exact fracture property under various temperatures. Four binders, including 3 polymer-modified asphalt (PMA) binders, were used to make a dense-grade asphalt mixture and 3-point bending test was peformed on notched beam at low temperatures, from -5oC to 35oC. Elastic modulus, flexural strength and fracture toughness were obtained from the test. The results showed that, since Poisson's ratio was considered, the more accurate test values could be obtained using modified ECM equation than original ECM. PMA mixture showed higher stiffness and fracture toughness than normal asphalt mixture under very low temperatures.

• Journal of Technologic Dentistry
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• v.31 no.4
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• pp.37-43
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• 2009

This study evaluated the effect of concentration of glass fiber reinforcement on the flexural properties of auto and heat polymerized denture base resin. The test specimens($64{\times}10{\times}3.3mm$) were made of auto and heat polymerized resin(Vertex, Dentimax, Netherlands). Glass fiber(ER 270FW, Hankuk Fiber Glass, Korea) were used to reinforce the denture base resin. The 2.6%, 5.3% and 7.9% volume pre-impregnated fiber were located at the bottom of specimen. The test specimens(n=7) of each group were stored in distilled water at $37^{\circ}C$ for 50 hours before test. The flexural strength and modulus were measured by an universal testing machine(Z020, Zwick, Germany) at a crosshead speed of 5 mm/min in a three-point bending mode. The data was analyzed by one-way ANOVA and the Duncan's multiple range test(${\alpha}$=0.05). The difference of auto polymerized resin groups and heat polymerized resin groups were statistically analyzed by t-test(${\alpha}$=0.05). Glass fiber showed significant reinforcing effects on auto and heat polymerized resin. For flexural strength and modulus, auto polymerized resin was the highest in 7.9% volume, while heat polymerized resin was the highest in 5.3% volume. In this study, glass fiber at 7.9% volume ratio showed most effective reinforcing effect on auto polymerized resin and glass fiber at 5.3% volume ratio showed most effective reinforcing effect on heat polymerized resin in terms of flexural strength and flexural modulus.

• Journal of the Korean Society for Precision Engineering
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• v.29 no.3
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• pp.307-312
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• 2012

This study aims to investigate the effect of the post weld treatments on the fatigue life of T-type welded structure made by a SM50A steel material, generally used for excavators, because changes in the geometry, material and surface properties of welded regions affect the fatigue life of welded structures. T-type test specimens were prepared by the CO2 welding of rolled steel plates (SM50A steel) with a thickness of 10 mm at a welding speed of 30 cm/min and these Ttype welded specimens were further treated by UIT (Ultrasonic Impact Treatment) and/or toegrinding post welding treatment methods. In order to investigate improvements on the fatigue life of the samples. 3-point bending fatigue tests were conducted with a stress ratio of R=0.1 under a cyclic loading environment at a frequency of 5 Hz, via a hydraulic fatigue testing machine (${\pm}100\;kN$, MTS 809). The tests were performed at room temperature. The fatigue life of UIT specimens was approximately 25 times longer than that of as-welded specimens at a stress amplitude of 281 MPa, while toe-grinding specimens exhibited 4.15 times longer fatigue life. The current results could provide important guidelines to determine the proper post weld treatment methodologies of T-type welded parts for excavators with a satisfactory fatigue life although under severe operating conditions.

• Journal of the Korean Ceramic Society
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• v.46 no.6
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• pp.662-667
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• 2009

Porous SiC candle filter preforms were fabricated by extrusion and ramming process. To fabricate SiC candle filter preform, commercially available 85 ${\mu}m\;{\alpha}-$-SiC powder and 44 ${\mu}m$ mullite, CaC$O_3$ powder were used as the starting materials. The candle type preforms were fabricated by vacuum extrusion and ramming process, and sintered at $1400{^{\circ}C}$ 2 h in air atmosphere. The effect of forming method on porosity, density, strength (flexural and compressive strength) and microstructure was investigated. Also, corrosion test of the sintered candle filter specimens as forming method was performed at $600{^{\circ}C}$ in IGCC syngas atmosphere. The sintered SiC filter which was formed by ramming process has more higher density and exhibit higher strength than extruded filter. Its maximum density and 3-point bending strength were 2.00 g/$cm^3$ and 45 MPa, respectively.

• Applied Chemistry for Engineering
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• v.10 no.3
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• pp.394-399
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• 1999

As the prosthetic application of natural mineral substituted for chemical reagent, composites and a glass-ceramics containing hydro-xyapatite isolated from tuna bone were prepared by solid state reaction. On x-ray examinations, the major phases of composites were identified as pseudowollastonite(${\alpha}-CaSiO_3$) and ${\beta}$-tricalcium phosphate($\beta$-TCP) and the phase of a glass-ceramics was observed as $\beta$-TCP and fluoroapatite caused by $CaF_2$ respectively. SEM images depict that the microstructures of grain at the composites were a function of temperature. The measured strength of a glass-ceramics prepared at $900^{\circ}C$ for 4 hr in air was 90 MPa as a 4-point bending method and this value was similar to the cortical bone, as 50~150 MPa but it was lower than its maximum strength.

• Advances in concrete construction
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• v.14 no.5
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• pp.299-307
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• 2022

Cement-based matrixes have low tensile strength and negligible ductility. Adding fibres to these matrixes will improve their mechanical properties and make these composites suitable for structural applications. Post-cracking tensile strength of steel fibers-reinforced cementitious composite materials is directly related to the number of transverse fibers passing through the crack width and the pulling-out behavior of each of the fibers. Therefore, the exact recognition of the pullout behavior of single fibers is necessary to understand the uniaxial tensile and bending behavior of steel fiber-reinforced concrete. In this paper, an experimental study has been carried out on the pullout behavior of 3D (steel fibers with totally two hooks at both ends), 4D (steel fibers with a total of four hooks at both ends), and 5D (steel fibers with totally six hooks at both ends) in which the fibers have been located either perpendicular to the crack width or in an inclined manner. The pullout behavior of the mentioned steel fibers at an inclination angle of 0, 15, 30, 45, and 60 degrees and with embedded lengths of 10, 15, 20, 25, and 30 millimetres is studied in order to explore the simultaneous effect of the inclination angle of the fibers relative to the alongside loading and the embedded length of fibers on the pullout response in each case, including the maximal pullout force, the slip of the maximum point of pullout force, pullout energy, fiber rupture, and concrete matrix spalling. The results showed that the maximum pullout energy in 3D, 4D, and 5D steel fibers with different embedded lengths occurs at 0 to 30° inclination angles. In 5D fibers, maximum pullout energy occurs at a 30° angle with a 25 mm embedded length.

• Composites Research
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• v.12 no.3
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• pp.8-16
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• 1999

Carbon woven fabric/C/SiC composites were fabricated by multiple impregnations of carbon woven fabric/carbon preform with the polymer precursor of SiC, i.e., polycarbosilane. In addition, two kinds of low density carbon/carbon preforms which had different fiber volume fraction and fiber orientation, i.e., a carbon woven fabric(${\thickapprox}$55 vol%)/carbon and a chopped carbon fiber${\thickapprox}$40 vol%)/carbon composites, were reaction-bonded with a silicon melt at 1$700^{\circ}C$ in a vacuum to fabricate dense carbon fiber/Si/SiC composites. The reaction-bonding process increased the density to ~2.1 g/$cm^3$ from 1.6 g/$cm^3$ and 1.15 g/$cm^3$ of a carbon woven and a chopped carbon preforms, respectively. All of the composites fractured with extensive fiber pull-out. The higher the density the higher the stiffness and proportional limit stress. The mechanical properties obtained from a three-point bend and tension tests were compared. The ratios of the peak tensile stresses to the bending strengths of a carbon woven and a chopped carbon composites were about one-third, respectively. The carbon woven fabric/Si/SiC composites with density of 2.06 g/$cm^3$ showed ~120 MPa of ultimate strength and ~80 MPa of proportional limit in bend testing.

• Polymer(Korea)
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• v.25 no.3
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• pp.435-440
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• 2001

The objective of this study was to examine the effect of oxidation inhibitor contents on the work of adhesion, fracture toughness, and impact strength of the unidirectional carbon-carbon composites (C/C composites). The molybdenum disilicide ($MoSi_2$) used as an oxidation inhibitor was impregnated with phenolic resins to improve the anti-oxidation properties of the composites in different concentrations of 4, 12 and 20 wt%. Based on Wilhelmy equation, the work of adhesion of C/C composites was calculated by contact angle methods. Fracture toughness and impact strength were pressured by three-point bending test for the critical intensity factor ($K_IC$) and Izod test method, respectively. As a result, the composites made with $MoSi_2$ resulted in an increasing of both fracture toughness and impact strength. Especially, the composites made with 12 wt% $MoSi_2$ content showed the highest value of London dispersive component, $W_A\;^L$, in work of adhesion, resulting from improving the interfacial adhesion force among fibers, filler, and matrix in this system.

• The Journal of Advanced Prosthodontics
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• v.5 no.4
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• pp.396-401
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• 2013

PURPOSE. The purpose of this in vitro study was to investigate the flexural properties of a recently introduced urethane dimethacrylate denture base material (Eclipse) after being repaired with two different materials. MATERIALS AND METHODS. Two repair groups and a control group consisting of 10 specimens each were generated. The ES group was repaired with auto-polymerizing polymer. The EE group was repaired with the Eclipse. The E group was left intact as a control group. A 3-point bending test device which was set to travel at a crosshead speed of 5 mm/min was used. Specimens were loaded until fracture occurred and the mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations were calculated for each group and the data were statistically analyzed. The results were assessed at a significance level of P<.05. RESULTS. The mean "displacement", "maximum load before fracture", flexural strength" and "flexural modulus" rates of Group E were statistically significant higher than those of Groups ES and EE, but no significant difference (P>.05) was found between the mean values of Group ES and EE. There was a statistically significant positive relation (P<.01) between the displacement and maximum load of Group ES (99.5%), Group EE (94.3%) and Group E (84.4%). CONCLUSION. The more economic and commonly used self-curing acrylic resin can be recommended as an alternative repair material for Eclipse denture bases.