• Title/Summary/Keyword: 회절 방사

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Infinite Elements for Analysis of Diffraction and Radiation Problems in the Vertical Plane (연직 2차원 회절 및 방사문제 해석을 위한 무한요소)

  • 박우선;이달수;오영민;정원무
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.3 no.4
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    • pp.235-243
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    • 1991
  • This paper is concerned with developing infinite elements which are applicable to wave diffraction and radiation problems in the vertical plane. The near need region surrounding the solid body is modeled using conventional finite elements. but the far fold region is represented using the infinite elements developed in this study. The shape functions for the infinite elements are derived from the analytical eigenseries solution of the scattered waves in the far field region. The system matrices of the elements are constructed by performing the integration in the infinite direction analytically to achieve computational efficiency. Numerical analysis is carried out for two floating bodies with different cross-sectional shapes to prove the efficiency and validity of the elements. Numerical experiments are also performed to determine the suitable location of the infinite elements which directly affect accuracy and efficiency of the solution.

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Survey on ultrafast time resolved X-ray diffraction measurements of crystal structure (X선의 초고속 결정구조 측정법)

  • Koo, Y.D.;Kim, Y.C.;Oh, C.S.
    • Journal of Energy Engineering
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    • v.23 no.3
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    • pp.13-16
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    • 2014
  • We have surveyed on significant progress in recent developments of accelerator-based pulsed X-ray sources has offered the opportunity for time-resolved studies on fast structure dynamics on the nanometer scale. The required and currently available techniques for time resolved X-ray diffraction measurements using the third-generation synchrotron radiation sources are summarized. Ultrafast X-ray experimental techniques are discussed for femtosecond studies at future synchrotron radiation sources.

UHV x-ray scattering system for surface structural studies (표면원자구조 연구를 위한 초고진공 X-선 산란 장치)

  • 김효정;강현철;노도영;강태수;제정호;김남동;이성삼;정진욱
    • Journal of the Korean Vacuum Society
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    • v.10 no.1
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    • pp.93-97
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    • 2001
  • We introduce the structure and the capability of a UHV x-ray scattering system constructed for surface structural studies. The system consists of vacuum parts required for surface preparation and a vertical-horizontal diffractometer using the S2D2 geometry. To illustrate the capability of the system, we measured the 7$\times$7 reconstruction peak of a Si (111) surface. The peak count rate was 216 counts/sec and the domain size of the 7$\times$7 reconstruction was larger than 1600 $\AA$. This demonstrates that the system is capable of providing surface structural information.

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Compressibility Study of Pyromorphite at High Pressure (고압 하에서 녹연석의 압축성에 대한 연구)

  • Kim, Young-Ho;Lee, Nuri
    • Journal of the Mineralogical Society of Korea
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    • v.29 no.4
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    • pp.191-198
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    • 2016
  • Pyromorphite($Pb_{4.85}(P_{1.02}O_4)_3Cl_{1.04}$) which belongs to the apatite group was compressed up to 33.4 GPa for its equation of state at ambient temperature. High pressure experiment was performed with symmetrical diamond anvil cell employing the angle dispersive X-ray diffraction method. Pressure was determined by ruby fluorescence calibration method. No phase transition were observed and bulk modulus was determined to be 80(7) GPa when $K{_0}^{\prime}=13(2)$. Employing the normalized pressure-normalized strain analysis, reliability check of the compressible behavior was conducted.

In-situ Phase Transition Study of Minerals using Micro-focusing Rotating-anode X-ray and 2-Dimensional Area Detector (집속 회전형 X-선원과 이차원 검출기를 이용한 광물의 실시간 상전이 연구)

  • Seoung, Dong-Hoon;Lee, Yong-Moon;Lee, Yong-Jae
    • Economic and Environmental Geology
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    • v.45 no.2
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    • pp.79-88
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    • 2012
  • The increased brightness and focused X-ray beams now available from laboratory X-ray sources facilitates a variety of powder diffraction experiments not practical using conventional in-house sources. Furthermore, the increased availability of 2-dimensional area detectors, along with implementation of improved software and customized sample environmental cells, makes possible new classes of in-situ and time-resolved diffraction experiments. These include phase transitions under variable pressure- and temperature conditions and ion-exchange reactions. Examples of in-situ and time-resolved studies which are presented here include: (1) time-resolved data to evaluate the kinetics and mechanism of ion exchange in mineral natrolite; (2) in-situ dehydration and thermal expansion behaviors of ion-exchanged natrolite; and (3) observations of the phases forming under controlled hydrostatic pressure conditions in ion-exchanged natrolite. Both the quantity and quality of the in-situ diffraction data are such to allow evaluation of the reaction pathway and Rietveld analysis on selected dataset. These laboratory-based in-situ studies will increase the predictability of the follow-up experiments at more specialized beamlines at the synchrotron.

Texture Analysis of Cu Interconnects Using X-ray Microdiffraction (X-ray Microdiffraction 을 이용한 구리 Interconnect의 Texture 분석)

  • 정진석
    • Korean Journal of Crystallography
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    • v.12 no.4
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    • pp.233-238
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    • 2001
  • X-ray microdiffraction which uses x-ray beam focused down to a micron size from synchrotron radiation sources allow precision measurements of local orientation and strain variations in polycrystalline materials. Using x-ray microdiffraction setup at Pohang Light Source, we investigated the tex-ture of Cu interconnects with various widths on Si wafer by collecting Laue images and focused to about 2×3㎛ ² in size. Our results show that 1㎛ wide Cu interconnect had grains in rather ran- dom orientation. On the other hand the 20㎛ wide interconnects showed a 〈111〉fiber texture near the center. The grains were 2∼5㎛ long at the 1㎛ wide interconnect and 6∼8㎛ in size at the 20㎛ wide interconnect.

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Compression Study of Goethite at Room Temperature (상온에서 괴타이트에 대한 압축 연구)

  • Kim, Y.H.;Hwang, G.C.;Do, J.K.
    • Journal of the Mineralogical Society of Korea
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    • v.20 no.4
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    • pp.261-266
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    • 2007
  • A natural FeOOH-goethite was compressed up to 9.5 GPa at room temperature using a DIA-type large volume apparatus with synchrotron radiation. Energy dispersive x-ray diffraction method was employed to measure its compressibility and NaCl was used for high pressure determinations. Bulk modulus was determined to be 131.1 (${\pm}5.8$) GPa by the Birch-Murnaghan equation of state with $K_0'$ fixed to 4. The present result is not in accord with the previous measurements, which vary from 111 to 147.9 GPa.

Electrospinning Fabrication and Characterization of Poly(vinyl alcohol)/Waterborne Polyurethane/Montmorillonite Nanocomposite Nanofibers (전기방사법을 이용한 폴리(비닐 알코올)/수분산 폴리우레탄/몬모릴로나이트 나노복합섬유의 제조 및 특성분석)

  • Kim, In-Kyo;Yeum, Jeong-Hyun
    • Polymer(Korea)
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    • v.35 no.6
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    • pp.553-557
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    • 2011
  • Poly(vinyl alcohol) (PVA)/waterborne polyurethane (WBPU)/montmorillonite clay (MMT) nanocomposite nanofibers were prepared using electrospinning technique of aqueous solutions. Scanning electron microscopy, transmission electron microscopy, X-ray diffraction and thermal gravimetric analyzer were used to characterize the morphology and properties of the nanocomposite nanofibers. Since PVA, WBPU and MMT are hydrophilic, non-toxic and biocompatible materials, these nanocomposite nanofibers can be used for filter and medical industries as wound dressing materials, antimicrobial filters, etc.

A Study on Anisotropic Compression Behavior of Illite (일라이트의 비등방적 압축특성 연구)

  • Yun, Seohee;Lee, Yongjae
    • Korean Journal of Mineralogy and Petrology
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    • v.33 no.1
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    • pp.11-18
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    • 2020
  • High-pressure synchrotron X-ray powder diffraction experiments were performed on natural illite (K0.65Al2(Al0.65Si3.35)O10(OH)2) using diamond anvil cell (DAC) under two different pressure transmitting media (PTM), i.e., water and ME41 (methanol:ethanol = 4:1 by volume). When using water as PTM, occasional heating was applied up to about 250℃ while reaching pressure up to 2.7 GPa in order to promote both hydrostatic conditions and intercalation of water molecules into the layer. When using ME41, pressure was reached up to 6.9 GPa at room temperature. Under these conditions, illite did not show any expansion of interlayer distance or phase transitions. Pressure-volume data were used to derive bulk moduli (K0) of 45(3) GPa under water and 51(3) GPa under ME41 PTM. indicating no difference in compressibility within the analytical error. Linear compressibilities were then calculated to be βa = 0.0025, βb = 0.0029, βc = 0.0144 under ME41 PTM showing the c-axis is ca. six times more compressible than a- and b-axes. These elastic behaviors of illite were compared to muscovite, one of its structural analogues.

Interaction Analysis on Deployment of Multiple Wave Energy Converters in a Floating Hybrid Power Generation Platform (부유식 복합발전 플랫폼내의 다수 파력발전기 배치를 위한 상호작용 해석)

  • Lee, Hyebin;Cho, Il Hyoung;Kim, Kyong-Hwan;Hong, Keyyong
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.19 no.3
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    • pp.185-193
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    • 2016
  • In this study, the present deployment of the multiple wave energy converters (WECs) in a floating wind-wave hybrid power generation platform was estimated considering the interaction effect among WEC buoys. The interaction processes of multiple buoys were very complex, since scattered and radiated waves from each buoy affected the others in the array. The interaction analysis of the diffraction and radiation problem by the array of WECs was applied by matched eigenfunction expansion method (MEEM). The analytical solutions were compared with the results of numerical calculation based on WAMIT. The overall performance of 24 WECs installed in the hybrid power generation platform was evaluated by the q-factor representing the interaction effect among buoys.