• Composites Research
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• v.16 no.3
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• pp.49-57
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• 2003

This paper presents the tensile characteristics for carbon/epoxy, carbon/phenolic and silica/phenolic composites under elevated temperature, which are considered for vehicle structure or thermal protection materials. The tensile test was conducted with servo-hydraulic testing machine and high temperature furnace, and the mechanical properties such as tensile strength, elastic modulus and Poisson's ratio were evaluated by using high temperature strain gages. Also, they were compared each other with respect to fiber orientation and temperature effect. These test results were used for designing and analyzing some airframe structures with these composites.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2006.05a
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• pp.81-85
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• 2006

Through-the-thickness properties of thick-walled cylindrical composites are required to determine structural performances because interlaminar tensile stress is primarily responsible for structural failure of the composites during their curing process. It is necessary for evaluating the tensile properties to find individual test methods to find appropriate methods because there are no recognised international standards(test methods and test specifications) available for generating reliable tensile properties in the direction. This paper has performed an experimental Study to measure that properties of carbon fabric/phenolic composites are produced by domestic company. Several test methods using an aluminum specimen were compared and evaluated. The best method, found out, was adopted to measure transverse through-the-thickness properties of composite materials. The results show that strain trends on four faces of composite specimen are the same.

• Journal of the Korean Society of Propulsion Engineers
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• v.10 no.3
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• pp.48-52
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• 2006

Through-the-thickness properties of thick-walled cylindrical composites are required to determine structural performances because interlaminar tensile stress is primarily responsible for structural failure of the composites during their curing process. It is necessary for evaluating the tensile properties to find individual test methods to find appropriate methods because there are no recognised international standards(test methods and test specifications) available for generating reliable tensile properties in the direction. This paper has performed an experimental study to measure that properties of carbon fabric/phenolic composites which are produced by domestic company. Several test methods using an aluminum specimen were compared and evaluated. The best test method to measure transverse through-the-thickness properties of composite materials was developed by the experimental results that strain trends on all faces of composite specimen are the same.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2007.11a
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• pp.371-376
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• 2007

Pan and rayon materials, two types of carbon fabric/phenolics composites, are using as thermal protectors for SRM's nozzle. After burning tests, It was required to analyze the performance of nozzles by ablated shape because ablative patterns were different from each other. For studying of performance on supersonic nozzles that have ablated shape, 1-dimensional analysis and numerical analysis were performed and results were presented in this paper. As the results of this study, in case of the thrust loss, rayon was predicted about 0.53% higher than pan and in case of total impulse loss, rayon was predicted about 0.4% higher than pan.

• Journal of the Korean Society of Propulsion Engineers
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• v.9 no.2
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• pp.25-31
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• 2005

The theory developed in a preceding paper [1] for poroelastic composite material behavior under thermal and gas diffusion is applied to thermo-chemical decomposition of a carbon-phenolic composite rocket nozzle liner under typical operating conditions. Specifically, the structural component simulated is the cowl ring for which distributions of pressure in the material pores, temperature and across-ply stress are presented. The results for particular composite designs show that across-ply failure occurs due to tensile stress in the material which is indicative of plylift. This prediction corroborates observations of plylift in a nozzle cowl. Simulations suggest designs to avoid plylift in the cowl zone.

• Polymer(Korea)
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• v.24 no.6
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• pp.845-853
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• 2000

The optimum cure cycle and carbonization condition were selected by the DSC and TGA analysis and green bodies were prepared by the method of hot press molding and then carbonized up to 140$0^{\circ}C$. Additives such as graphite powder, carbon black, milled carbon fiber and carbon fiber mat, which were considered to be effective in improving the interlaminar shear strength, were also added to check their effects on the density and porosity of products. Then, their relations with mechanical properties such as ILSS and flexural strength were investigated. The composites added 9 vol% of graphite powder showed the greatest values of ILSS and flexural strength. Otherwise, in case of adding carbon black, the composites showed the slight improvement of ILSS at its contents of 3 vol% but the flexural strength was decreased. When milled carbon fiber and carbon fiber mat were added, the lack of resin and the heat shrinkage during the carbonization caused the delamination, resulting in decreasing the density, ILSS and flexural strength.

• Journal of the Korean Society of Propulsion Engineers
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• v.5 no.4
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• pp.1-11
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• 2001

A theory for time-dependent, high temperature ablation of poroelastic carbon composite insulators is applied using finite element methods to determine material properties from experimental data. The theory contains important revisions to that in Lee, Salamon and Sullivan[1] by making a sharp distinction between Biots constants and permeability and setting both to analytical functions of porosity. The finite element program and material modeling has been modified to (1) more closely adhere to porous-material theory, (2) include a newly discovered analytical simplification and (3) refine the material property descriptions. Application to experimental problems and comparisons with data permit determination of Biots constants and permeability and their evolution with respect to matrix decomposition and clearly show how material parameters affect the material response, e.g., amplitude and the location of peaks with respect to temperature. In particular, the response is very sensitive to permeability and dominated by it.

• Proceedings of the KAIS Fall Conference
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• 2009.05a
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• pp.372-375
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• 2009

반도체 봉지재란 실리콘 칩, 골드와이어, 리드프레임 등의 반도체 소지를 열, 수분, 충격으로부터 보호하기 위해 밀봉하는 재료로서 EMC(Epoxy Moding Compound)가 가장 많이 쓰인다. EMC는 기계적, 전기적 성능향상을 위한 무기재료로 실리카(Silica), 열에 의해 경화되어 3차원 경화구조를 형성하는 에폭시수지, 빠른 경화특성을 부여하기 위한 경화제로서의 페놀수지, 유기재료와 무기재료 사이의 결합력을 높이기 위해 커플링제, 카본블랙, 이형성 확보를 위한 왁스(Wax), 착색제(Colorant), 난연제(Flame Retardant)등의 첨가제로 구성되는 복합소재로써 본 연구에서는 에폭시의 유형에 따른 용융 실리카를 주충진재로 하여 각각의 봉지재의 첨가제를 기준으로 할 때 다양한 형태의 친환경 비할로겐계 반응형 난연제를 합성하는 기술을 개발하고 비 할로겐계 및 Sb 계 첨가형 난연제의 혼용 배합을 통해 친환경 EMC용 난연제의 제조기술을 개발하였다. 이들 EMC의 요구특성은 요구특성은 외부환경으로부터 칩 보호, 칩을 전기적으로 절연특성 유지, 칩의 작동시 발생되는 열의 효과적인 방출 특성 유지, 실장(Board Mounting)의 간편성 특성을 확보해야 하는 특성을 지니고 있어 이들 요구특성에 적합한 특성조사가 함께 이루어졌다.