• Title/Summary/Keyword: 접착전단강도

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A STUDY OF SHEAR BOND STRENGTH OF ORTHODONTIC BRACKET UNDER BLOOD-CONTAMINATED CONDITIONS (혈액 오염 환경 하에서 접착된 교정용 브라켓의 전단 강도에 관한 연구)

  • Shin, Ji-Sun;Kim, Jong-Soo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.32 no.2
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    • pp.191-199
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    • 2005
  • This study was experienced in order to obtain the shear bond strength of orthodontic bracket adhesives under the blood contamination that can be occurred during the procedure of bracket bonding under window opening surgery. As a result of this study, shear bond strength of all glass ionomer groups were lower than resin cement groups. However, the strength of uncontaminated and post-contaminated group of glass ionomer was strong enough to perform an orthodontic forced eruption. This study revealed that during a window opening surgery, glass ionomer without etching procedure is available in order to bond a bracket if surface of teeth is not pre-contaminated by blood before the adhesive application. Both simple procedure and less adhesives remnant after bonding failure could make light-cured glass ionomer cement the ultimate choice for racket bonding.

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THE EXPRESSION OF OSTEONECTIN AND OSTEOCALCIN IN THE EXPERIMENTAL TOOTH MOVEMENT IN RAT (백서의 실험적 치아이동시 osteonectin 및 osteocalcin의 발현)

  • Bae, Sung-Real;Kim, Sang-Cheol
    • The korean journal of orthodontics
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    • v.28 no.5 s.70
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    • pp.699-716
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    • 1998
  • This study was designed to evaluate the expression of non-collagenous protein in periodontal tissue during the experimental movement of rat incisors, by LSAB(labelled streptavidine biotin) immunohistochemical staining for osteonectin and osteocalcin. Twenty seven Sprague-Dawley rats were divided into a control group(3 rats) and 6 experimental groups(24 rats) where 75g of force was applied from helical springs across the maxillary incisors. Rats of experimental groups were sacrificed at 12 hours, 1, 4, 7, 14 and 28 days after force application, respectively. And the tissues of a control group and experimental groups were studied immunohistochemically and histologically. The results were as follows : 1. Until 28 days after force application, periodontal fibers had been strectched on tension side and compressed in pressure side of all the experimental groups, and the arrangement of periodontal fibers had not been recovered yet. 2. The expression of osteonectin in control group was rare in dentin, cementum and osteocyte, and was mild in odontoblasts and matrix of alveolar bone. 3. The expression of osteocalcin in control group was negative in gingiva, osteoblasts, osteocyte and cementum, and was rare in predentin, capillaries in pulp and periodontal ligament and the matrix of alveolar bone. 4. There was no difference in the expression of osteocalcin or osteonectin in dentin, cementum, pulp, odontoblasts, between of control and of experimental groups. 5. The expression of osteonectin in intermaxillary suture got the peak in 7-day and was declined after 14-day. The expression of osteocalcin remained in a same degree since it became mild in 14-day. 6. The expression of osteonectin in pressure side of periodontal ligament of experimental group was rare, which was similar to control group. But in tension side, it was increased until 14-day aftrer which it was declined. 7. The expression of osteocalcin in periodntal ligament was rare in 12-hour to 14-day, but became severe in 28-day, which was greater in tension side than in pressure side, and in the periodontal fiber next to alveolar bone than to tooth surface. 8. The expression of osteocalcin in alveolar bone was rare until 14-day in pressure side, but became moderate in 28-day. The expression of osteonectin was increased from 7-day by time dependency, which was greater in tension side than in pressure side.

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Comparative Study on Test Methods for Mechanical Properties of Structural Adhesives Used in FRP Strengthening (구조보강용 FRP 함침·접착수지의 역학적 특성 분석을 위한 시험방법 비교 연구)

  • You, Young Chan;Choi, Ki Sun;Kim, Keung Hwan
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.12 no.2
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    • pp.103-112
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    • 2008
  • Pull-off test is generally used to evaluate bond strength of FRP composite with concrete at job site. However, some damages on FRP composites can not be avoided during pull-off test and moreover test range of pull-off strength is limited by maximum tensile strength of concrete. Accordingly, it is required to set-up a test method that can evaluate mechanical properties of structural adhesive indirectly prior to pull-off test. In this study, the standard test methods for structural adhesive which can simply evaluate mechanical performance of adhesive were suggested through comparative experiments from each different standard in various countries. Particularly, gluing thickness of adhesive in tensile lap-shear tests, the section dimension of compression and bending test specimens become unified, and standard test specimen size is achieved by test results.

THE INFLUENCE OF $CARISOLV^{TM}$ ON SHEAR BOND STRENGTH OF COMPOSITE RESIN RESTORATIONS ($Carisolv^{TM}$의 사용이 복합레진 수복물의 전단결합강도에 미치는 영향)

  • Kim, Dae-Eop
    • Journal of the korean academy of Pediatric Dentistry
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    • v.30 no.1
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    • pp.47-53
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    • 2003
  • This study evaluated the influence of chemomechanical caries removal agent $Carisolv^{TM}$(MediTeam, Sweden) for composite resin adhesion to sound human permanent and primary dentin. The buccal/labial surfaces of 80 permanent molars and 80 primary incisors were used. Four types of adhesives and one composite resin were used; AQ Bond(Sun Medical, Japan), Clearfil SE Bond(Kuraray, Japan), Single Bond(3M, USA), Scotchbond Multi-Purpose(3M, USA) and Z100(3M, USA). One drop of $Carisolv^{TM}$(MediTeam, Sweden) was pretreated on the dentin for 0 second(control) and 60 seconds. The specimens were thermocycled for 1,000 times in baths kept 5 degrees C and 55 degrees C with a 30 seconds dwell time. Shear bond strengths were tested and the data was statistically analyzed using one-way ANOVA with subsequent post hoc Scheffe test at p<0.05. $Carisolv^{TM}$ treatment significantly decreased the shear bond strength. Shear bond strength of permanent dentin was significantly higher than that of primary dentin. Clearfil SE Bond treatment groups showed the highest shear bond strength and AQ Bond treatment groups showed the lowest shear bond strength.

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A STUDY ON THE SHEAR BOND STRENGTH BY PLASMA ARC CURING SYSTEM FOR BRACKET BONDING (Plasma arc curing system을 이용한 브라켓의 접착에 관한 연구)

  • Kim, Jung-Yoon;Kim, Jong-Soo;Kwon, Soon-Won
    • Journal of the korean academy of Pediatric Dentistry
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    • v.28 no.4
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    • pp.638-642
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    • 2001
  • Recently, plasma arc curing system for curing resin composites has been introduced. This is characterized by a high output of light energy, which has the advantage of reducing the chair time and thereby making the treatment more comportable for the patients as well as for the dentist. The purpose of this study was to compare the shear bond strengths of light-cured orthodontic adhesive polymerized with conventional halogen light and plasma arc light. The 2 curing devices used were the XL3000 (3M, USA) conventional curing light and the Flipo (LOKKI, France) plasma arc light. The results from the present study can be summarized as fellows; 1. The mean shear bond strength for three groups were quite similar for 50 second conventional light group, 2 second plasma arc curing light group, 5 second plasma arc curing light group. 2. There was no statistically significant difference for three groups(p>0.05).

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Effect of Different Types of Bonding Agent and Application Methods on Shear Bond Strength of Orthodontic Bracket (Bonding agent의 종류 및 적용 방법에 따른 교정용 브라켓의 전단결합강도에 관한 연구)

  • Lee, Jaehee;Kim, Jongsoo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.44 no.4
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    • pp.419-426
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    • 2017
  • Attachment of the orthodontic bracket conducted during the window opening procedure can result in failure due to various adverse conditions such as blood or saliva contamination, or other wet conditions. For the success of the bracket attachment, reduction of total operation time is crucial. The purpose of this literature is to evaluate the differences between the final resultant shear bond strength of the conventional method of using phosphoric acid and self-etching primer, and that of the operation time-reduced method in which the curing step is omitted subsequent to the primer application. A total of 40 human maxillary incisors were prepared. Group I(control group) and II were etched with 37% phosphoric acid and Group III and IV were conditioned with self-etching primer. Attachment of the group I and III was conducted by manufacturer's instructions. The operation time of Group II and IV was reduced by eliminating the curing step after the primer application. The resultant shear bond strength of each group was measured and an adhesive remnant index (ARI) was recorded. The mean shear bond strength of group I, II, III, and IV were 14.16 MPa, 8.33 MPa, 8.29 MPa, and 6.48 MPa respectively. Significant differences could only be found between the control group and the experimental groups (p < 0.05). The ARI indicated no significant difference among all groups.

Shear bond strength of ceramic brackets bonded with antimicrobial monomer-containing self-etching primer (항미생물제제를 포함한 self-etching primer로 접착한 세라믹 브라켓의 전단 결합 강도)

  • Kwon, Tae-Hun;Kang, Jang-Mi;Chang, Na-Young;Kang, Kyung-Hwa
    • The korean journal of orthodontics
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    • v.41 no.1
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    • pp.16-24
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    • 2011
  • Objective: The purpose of this study was to determine (1) the shear bond strength (SBS) of an antimicrobial monomer-containing self-etching primer according to ceramic bracket types and (2) the bracket-adhesive failure mode using an adhesive remnant index (ARI). Methods: A total of 90 extracted human teeth were randomly divided into 6 groups. Each group consisted of one of two ceramic brackets (monocrystalline, polycrystalline) and one of three primers (Transbond XT primer, Transbond Plus SEP, Clearfil Protect Bond) with each group containing 15 specimens. The SBS was measured, and adhesive residues left on the tooth surface were assessed. Results: The SBS of polycrystalline ceramic bracket groups was Significantly higher than that of the monocrystalline ceramic bracket groups (p < 0.001). The SBS of Transbond XT primer groups was significantly higher than those of Transbond Plus SEP groups and Clearfil Protect Bond groups (p < 0.001). All the groups showed bonding failures between the bracket base and adhesive. Conclusions: The combination of a self-etching primer with a monocrystalline bracket is recommended for clinical use, considering its acceptable SBS and mode of failure.

A Study on the Fabrication of the Laminated Wood Composed of Poplar and Larch (포푸라와 일본잎갈나무의 집성재 제조에 관한 연구)

  • Jo, Jae-Myeong;Kang, Sun-Goo;Kim, Ki-Hyeon;Chung, Byeong-Jae
    • Journal of the Korean Wood Science and Technology
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    • v.2 no.2
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    • pp.25-31
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    • 1974
  • 1. Various gluing qualities applying Resorcinol Plyophen #6000 were studied on aiming the strength relationships of laminated woods resulted by single species [poplar (Populus deltoides), larch(Larix leptolepis)], mixed species of (poplar and larch), preservatives, treated poplar the scarf joint with mixed species of poplar and larch and the scarf joint treated with preservatives. 1. 1 On the block shear and on the DVL tension test, the mean wood failure ratio showed an excellent value i.e., above 65% and the tangential strength for larch was higher than that of radial, but it was reversed for poplar as shown in Tables 1 and 2. 1. 2 The lamina treated with Na-PCP reduced slightly the strength but the limited strength allowed for manufacturing laminated wood was not influenced by treating Na-PCP as shown in Tables 3 and 4. 1. 3 The safe scarf ratio in the plane scarf joint was above 1/12 for larch and 1/6 for poplar regard less of the chemical treatment or untreatment as shown in Tables. 5, 6, 7 and 8. 2. In the normal and boiled state, the gluing quality of the laminated wood composed of single[poplar (Populus deltoides), larch (Larix leptolepis)] and double species (poplar and larch) glued with Resorcinol Plyophen #6000 were measured as follow, and also represented the delamination of the same laminated wood. 2.1 The normal block shear strength of the straight and curved laminated wood (in life size) were more than three times of the standards adhesion strength. And, the value of the boiled stock was decreased to one half of the standard shear adhesion strength, but it was more than twice the standard strength for the boiled stock. Thus, it was recognized that the water resistance of the Resorcinol Plyophen #6000 was very high as shown in Tables 9 and 10. 2. 2 The delamination ratio of the straight and curved laminated woods in respect of their composition were decraesed, in turn, in the following order i. e., larch, mixed stock (larch+poplar) and poplar. The maximum value represented by the larch was 3.5% but it was below the limited value as shown in Table 11. 3. The various strengthes i.e., compressive, bending and adhesion obtainted by the straight laminaced wood which were constructed by five plies of single and double species of lamina i. e., larch (Larix leptolepis) and poplar (Populus euramericana), glued with urea resin were shown as follows: 3. 1 If desired a higher strength of architectural laminated wood composed of poplar (P) and larch (L), the combination of the laminas should be arranged as follows, L+P+L+P+L as shown in Table 12. 3.2 The strength of laminated wood composed of laminas which included pith and knots was conside rably decreased than that of clear lamina as shown Table 13. 3.3 The shear strength of the FPL block of the straight laminated wood constructed by the same species which were glued with urea adhesives was more than twice the limited adhesion strength, thus it makes possible to use it for interior constructional stock.

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Evaluation of Shear Strength by Direction of Wood Grain for Korean Pine Using PRF Adhesive (페놀레조시놀공축합수지로 접착된 국산 잣나무의 목리방향별 전단성능평가)

  • Park, Sun-Hyang;Kim, Kwang-Mo;Pang, Sung-Jun;Kong, Jin Hyuk;Lee, Sang-Joon
    • Journal of the Korean Wood Science and Technology
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    • v.45 no.3
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    • pp.243-249
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    • 2017
  • This study was performed to find out the optimum adhesive conditions on manufacturing a cross-laminated timber (hereinafter CLT) with using domestic Korean Pine (Pinus koraiensis). The adhesive conditions including a applied amount of the glue and a Pressure are the one of the most important key factors on establishing CLT production process. The shear strength was examined with differing the adhesive conditions while using Phenol Resorcinol Formaldehyde Resin Adhesive (PRF resin). The optimum adhesive conditions was confirmed to be: glue spread of $250g/m^2$ and Pressure of 0.8 MPa respectively. The grain directions of glued specimens were also considered, perpendicularly bonded and parallelly bonded groups. Shear strength of the former group showed lower values than the latter group which is considered to be the effect of a rolling shear. Meanwhile the shear strength of both group satisfied the Korean Standard (KS F 3021) and the European Standard (EN 14080 and EN 16351). The results derived from this study can be used as the basic data for manufacturing the CLT with domestic Korean Pine. And additional researches for the other species including domestic Korean Larch and Pitch Pine is also now being performed.

The Effect of Surface Treatment on the Shear Bond Strength of Resin Cement to Zirconia Ceramics (표면처리가 지르코니아와 레진 시멘트의 전단결합강도에 미치는 효과)

  • Jung, Seung-Hyun;Kim, Kye-Soon;Lee, Jae-In;Lee, Jin-Han;Kim, Yu-Lee;Cho, Hye-Won
    • Journal of Dental Rehabilitation and Applied Science
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    • v.25 no.2
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    • pp.83-94
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    • 2009
  • The aim of this study was to investigate the shear bond strength between zirconia ceramic and resin cement according to various surface treatments. The surface of each zirconia ceramic was subjected to one of the following treatments and then bonded Rely X Unicem or Rely X ARC resin cement; (1) Rocatec system and $50{\mu}m$ surface polishing, (2) No treatment and $50{\mu}m$ surface polishing, (3) Rocatec system and $1{\mu}m$ surface polishing, (4) No treatment and $1{\mu}m$ surface polishing. Each of eight bonding group was tested in shear bond strengths by universal testing machine(Z020, Zwick, Ulm, Germany) with crosshead speed of 1mm/min. The results were as follows; 1. Rocatec treatment groups showed greater bonding strengths than No Rocatec groups. There was significant difference of among groups(P<0.001) 2. For Rocatec groups, $50{\mu}m$ surface roughness groups showed greater bonding strengths than $1{\mu}m$ surface roughness groups.(P<0.001) But for No Rocatec groups, There was no significant difference of among groups(P>0.05) 3. Rely X Unicem groups showed greater bonding strengths than Rely X ARC groups. There was significant difference of among groups(P<0.01) Within the conditions of this study, Rocatec treatment was an effective way of increasing zirconia bonds to a resin cement, even in the case of self-adhesive resin cement.