• Title/Summary/Keyword: 작은시편

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Eco-Friendly Backfill Materials with Bottom Ash (바톰애시를 이용한 환경친화적 뒤채움재)

  • Lee, Kwan-Ho;Kim, Seong-Kyum
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.3
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    • pp.1385-1390
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    • 2012
  • Couple of laboratory for controlled low strength materials with bottom ash and recycled in-situ soil have been carried out. The optimum mix ratios for 4 cases with flowability and unconfined compressive strength were determined. The optimim mixing ratios were 25 to 45% of insitu soil, 30% of bottom ash, 10 to 20% of fly ash, 0 to 3% of crumb rubber, 3% of cement and 22% of water. Each mixture was satisfied the standard specification, minimum 20cm of flowability and 127 kPa of unconfined compressive strength. Two different curling methods, at room temperature and wet condition, were adopted. The average secant modulus(E50) was 0.07 to 0.08 * $q_u$. The compressive strength at wet condition showed 10% larger than at room temperature. The range of internal friction angle and cohesion for mixtures were 36.5o to 46.6o and 49.1 to 180 kPa, respectively. The mixture with crumb rubber(case 4) showed higher choesion and lower internal friction angle than the others. The pH of all the mixtures was over 12 which is strong alkine.

CUSPAL DEFLECTION IN CLASS V CAVITIES RESTORED WITH COMPOSITE RESINS (5급 와동의 복합레진 수복 시 발생되는 교두굴곡에 관한 연구)

  • Park, Jun-Gyu;Lim, Bum-Soon;Lee, In-Bog
    • Restorative Dentistry and Endodontics
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    • v.33 no.2
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    • pp.83-89
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    • 2008
  • The purpose of this study was to evaluate the effect of the polymerization shrinkage and modulus of elasticity of composites on the cusp deflection of class V restoration in premolars. The sixteen extracted upper premolars were divided into 2 groups with similar size. The amounts of cuspal deflection were measured in Class V cavities restored with a flowable composite (Filtek flow) or a universal hybrid composite (Z-250). The bonded interfaces of the sectioned specimens were observed using a scanning electron microscopy (SEM). The polymerization shrinkage and modulus of elasticity of the composites were measured to find out the effect of physical properties of composite resins on the cuspal deflection. The results were as follows. 1. The amounts of cuspal deflection restored with Filtek flow or Z-250 were $2.18\;{\pm}\;0.92{\mu}m$ and $2.95\;{\pm}\;1.13\;{\mu}m$, respectively. Filtek flow showed less cuspal deflection but there was no statistically significant difference (p > 0.05). 2. The two specimens in each group showed gap at the inner portion of the cavity. 3. The polymerization shrinkages of Filtek flow and Z-250 were 4.41% and 2.23% respectively, and the flexural modulus of elasticity of cured Filtek flow (7.77 GPa) was much lower than that of Z-250 (17.43 GPa). 4. The cuspal deflection depends not only on the polymerization shrinkage but also on the modulus of elasticity of composites.

Compression Strength Test of FRP Reinforced Concrete Composite Pile (FRP-콘크리트 합성말뚝 시편의 압축강도실험)

  • Lee, Young-Geun;Choi, Jin-Woo;Park, Joon-Seok;Yoon, Soon-Jong
    • Journal of the Korean Society for Advanced Composite Structures
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    • v.2 no.4
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    • pp.19-27
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    • 2011
  • In this paper, we present a part of results to develop new type hybrid FRP-concrete composite pile (i.e., concrete filled fiber reinforced plastic circular tubes, hybrid CFFT, HCFFT). The purpose of this paper is to evaluate compressive loading capacity through compressive strength test. Before compressive strength test of HCFFT, we investigated mechanical properties of pultruded fiber reinforced plastic (PFRP) and filament winding fiber reinforced plastic (FFRP). For estimating the compressive strength of HCFFT, uni-axial compression strength tests of HCFFT compression members were conducted. The test variables are compressive strengths of concrete and thickness of FFRP. In addition, uni-axial compression strength tests of concrete filled fiber reinforced plastic circular tube (CFFT) except PFRP members were conducted. The test variable in the test is thickness of FFRP. From the test result, the compressive strength of the HCFFT in larger than compressive strength of CFFT as much as 47%. It can be observed that the uni-axial compressive strength of the HCFFT increased if the concrete strength and the thickness of exterior filament winding FRP tube increased. In addition, the finite element analysis result is compared with the experimental result. The difference between the experimental and FEM results is in the range of 0.14% to 17.95%.

Liquid Phase Sintered SiC-30 wt% TiC Composites by Spark Plasma Sintering (스파크 플라즈마 소결에 의한 액상소결 SiC-30 wt% TiC 복합체)

  • 조경식;이광순;송진호;김진영;송규호
    • Journal of the Korean Ceramic Society
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    • v.40 no.8
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    • pp.751-757
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    • 2003
  • Rapid densification of a SiC-30 wt% TiC powder with additive 10 wt% A1$_2$O$_3$-Y$_2$O$_3$-CaO was conducted by Spark Plasma Sintering(SPS). The fully-densified materials can be obtain through the SPS process with very fast heating rate and short holding time. In the present work, the heating rate and applied pressure were kept to be $100^{\circ}C$/min and 40 MPa, while sintering temperature varied from $1600^{\circ}C$ to $1800^{\circ}C$ for 10 min. The full densification of SiC-30 wt% TiC composites with the addition of $Al_2$O$_3$, $Y_2$O$_3$ and CaO was achieved at the temperature above $1700^{\circ}C$ by spark plasma sintering. The XRD found that 3C-SiC and TiC were maintained the entire SPS process temperature, without phase transformation of SiC and formation of YAG phase to $1800^{\circ}C$. The microstructures of the rapidly densified SiC-30 wt% TiC composites consisted of smaller equiaxed SiC grains and larger TiC grains. The biaxial strength of 635.2 MPa and fracture toughness of 6.12 MPaㆍ$m^{1/2}$ were found for the specimen prepared at $1750^{\circ}C$.

The Influence of Microwave Sintering Process on the Adaptation of CAD/CAM Zirconia Core (마이크로 웨이브 소결 과정이 CAD/CAM 지르코니아 코아의 적합도에 미치는 영향)

  • Kim, Keun Bae;Kim, Jee Hwan;Lee, Keun-Woo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.25 no.2
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    • pp.95-107
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    • 2009
  • The purpose of this research was to examine the fitness of zirconia cores that were made by different sintering methods; generic electricity furnace and microwave furnace. Firstly, 12 cores for each group were made by using each different sintering process and attached them to a metal die with silicon. The internal and marginal gap of sintered zirconia was measured by using Skyscan 1076 micro-CT, then it was reorganized by CT-An software. To each samples, we extracted B-L image, M-D image of cutting side, and cross-sectional side of tooth long axis and calculated the mean value of marginal, axial, and occlusal gap each side. Results: 1. The mean marginal gap of sintered zirconia was $36.20{\mu}m$ for EVE, $47.67{\mu}m$ for LAV, $52.47{\mu}m$ for DEN, and $54.63{\mu}m$ for CER. 2. For the axial wall, the research showed the largest value of $63.49{\mu}m$ for EVE, but there were no statistical significance. 3. In related to the occlusal internal measurement, DEN showed the smallest value ($77.06{\mu}m$), EVE and CER showed significantly high value. From this study, it is suggested that CAD/CAM zirconia core which was made in the process of microwave sintering has clinically acceptable values in marginal and internal gap.

Study on the Prediction of Surface Color Change of Cultural Properties Materials by Fog Occurrence (안개 발생에 따른 문화재 표면의 색 변화 예측 연구)

  • Han, Ye Bin;Park, Sang Hyeon;Yu, Ji A;Chung, Yong Jae
    • Journal of Conservation Science
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    • v.32 no.4
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    • pp.491-500
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    • 2016
  • Fog is atmospheric in which tiny drops of water vapor are suspended in the air near the ground. Its form, occurrence, etc., change according to the temperature, relative humidity, wind and geographical features of the space around it. In particular, fog tends to occur near a source of water because of temperature and relative humidity difference. These days, climate change is increasingly affecting the occurrence of fog. Therefore the purpose of this study was to investigate how fog affects materials that are part of our cultural properties through outdoor exposure tests and artificial degradation. The degradation evaluation of materials as a function of fog occurrence frequency, showed that the color of metals changed noticeably, whereas dyed silk and Dancheong showed degradation on the surface and color differences but no particular tendencies. Therefore, damage prediction by color differences as a function of fog occurrence frequency was based on metal samples, which showed constant color differences. Through a comparison of the predictive value and color difference by outdoor exposure, the accuracy and applicability of the damage prediction formula was confirmed. If a more complex damage prediction formula is created, it is expected that prediction of the degree of material damage in the field would be possible.

Effect of Sintering Time on Microwave Dielectric Properties of Layered Mg0.93Ca0.07TiO3-(Ca0.3Li0.14Sm0.42)TiO3 Ceramics (소결시간에 따른 적층형 Mg0.93Ca0.07TiO3-(Ca0.3Li0.14Sm0.42)TiO3 세라믹스의 마이크로파 유전특성)

  • Cho, Joon-Yeob;Yoon, Ki-Hyun;Kim, Eung-Soo;Kim, Tae-Hong
    • Journal of the Korean Ceramic Society
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    • v.39 no.9
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    • pp.890-895
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    • 2002
  • Effect of the sintering time on the microwave dielectric properties of the layered Functionally Graded Materials(FGMs) of the Mg0.93Ca0.07TiO3(MCT) with (Ca0.3Li0.14Sm0.42)TiO3(CLST) ceramics was investigated. The dielectric constant of layered FGMs specimens showed a nearly constant value and did not change significantly with sintering time. The quality factor, however, was affected by the relative density and thermal stress developed in each dielectric layer. With an increase of the relative density and the decrease of the induced thermal stresses, quality factor of the layered FGMs specimens increased and the quality factor was incluenced sensitively by the change of compressive stress developed in MCT layers which had a lower thermal expansion coefficient than that of CLST. For the layered FGMs specimen sintered at 1300$^{\circ}C$ for 9h, the compressive stress developed in MCT layer showed the maximum value, which, in turn, the quality factor of the specimen was the minimum value.

An Experimental Study on the Evaluation of Shear Strength of Weathered Soil Containing Coarse Particles (굵은 입자가 포함된 풍화토의 전단강도 평가에 대한 실험연구)

  • Joon-Seok Kim
    • Journal of the Society of Disaster Information
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    • v.20 no.1
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    • pp.169-176
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    • 2024
  • Purpose: In this paper, an experimental study was conducted to analyze the difference in shear strength caused by the problem of excluding coarse particles due to the size of the test specimen in the direct shear test. Method: A large-scale direct shear test was conducted on three weathered soils containing coarse aggregates with a maximum diameter of 50mm. In addition, a small-scale direct shear test was performed using a sample with a maximum diameter of 5 mm, excluding coarse aggregates. Result: In the case of the small-scale direct shear test, compared to the results of the large-scale direct shear test containing large particles, the internal friction angle was about 2.3% smaller, and there was no significant difference. In terms of cohesion, compared to the large-scale direct shear test, the small-scale direct shear test derived about 80.3% smaller value, showing a relatively large difference. Conclusion: In the large-scale direct shear test, it was analyzed that the coarse particles had a greater impact on the cohesion than the internal friction angle. Therefore, granite weathered clay containing coarse particles is judged to have the same shear strength as the cohesive force that is not affected by vertical stress. In this study, it was analyzed that the small-scale direct shear test, which excludes the coarse particles that are commonly used, provides results on the safety side by excluding the effect of coarse particles.

Optical Microscopic Image Analysis for Damaged GFRP Rebar by Alkali and High Temperature Exposures (알칼리와 고온노출에 의한 GFRP 보강근 손상에 대한 현미경분석 연구)

  • Bae, Jung-Myung;Moon, Do-Young;Park, Cheol-Woo;Park, Young-Hwan
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.2
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    • pp.53-59
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    • 2017
  • In this experimental study, the characteristic of damages on GFRP rebar exposed to high temperature only and immerged in alkaline solution after the exposure to high temperature was analyzed through microscopic image analysis. The found microcrack and pores in resin matrix were quantitatively compared if there was effect of pre-exposure to high temperature. The damages, such as microcrack and pores in resin matrix, by alkali exposure were mainly found in rebar surface. On the other hand, the pores caused by high temperatures were extensively found in a section and had greater width than those caused by the alkali exposure. In results of the quantitative comparison, the accumulated length and widths of microcrack and pores in resin matrix in pre-exposed GFRP rebar to high temperature were respectively 1.5 and 1.4 times of those in the GFRP rebar only immerged in alkali solution. Therefore, the deterioration of resin matrix by the alkali exposure could be accelerated due to the pre-exposure to high temperature.

A Study on the Electrochemical Deposition and p-Type Doping of ZnTe Films as a Back Contact Material for CdTe Photovoltaic Solar Cells (CdTe계 태양전지에 응용되는 ZnTe 박막의 전기화학적 제조 및 Cu 도핑 연구)

  • Kim, Dong-Hwan;Jeon, Yong-Seok;Kim, Gang-Jin
    • Korean Journal of Materials Research
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    • v.7 no.10
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    • pp.856-862
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    • 1997
  • 박막형 CdTe/CdS 태양전지의 배면전극(back contacts)물질로서 Cu도핑된 ZnTe 박막(ZnTe:Cu)을 전착법(electroplating)으로 제조하는 연구를 수행하였다. Sulfate계의 전해질 수용액에서 CdTe 기판과 투명전극으로 코팅된 유리(In$_{2}$O$_{3}$: Sn, ITO)기판 위에 ZnTe 박막을 코팅하는 방법으로써 potentiostat와 기판(cathode), Pt counter electrode, Ag/AgCI 표준전극으로 구성된 장치를 사용하여 pH=2.5-4, T=70-8$0^{\circ}C$, 0.02M $Zn^{2+}$ 1x$10^{-4}$M TeO$_{2}$, 0.2M $K_{2}$SO$_{4}$조건에서 -0.800 Vs~-0.975 V 범위의 전압(V$_{a}$ )에 걸쳐 실험하였다. ITO박막을 기판으로 사용하여 cyclic voltammogram을 작성한 결과 약 -0.50 V 에서 Te환원 peak이 나타났다. Auger electron spectroscopy (AES)로 조성분석한 결과 표면에서 Zn signal이 강하게 나왔고 시편의 두께에 따라 Zn의 signal감소하는 반면 Cd signal은 증가하는 것이 확인되었다. SEM 사진으로부터 ZnTe의 표면이 작은 입자 (0.2$\mu\textrm{m}$ 이하)로 구성되어 있으며 낮은 V$_{a}$ 에서는 입자가 작아지면서 조직이 치밀해짐이 관찰되었다. Optical transmission방법에 의하여 ITO기판위에 입혀진 박막의 밴드갭은 2.5 eV으로 측정되었다. 수용액중의 Cu$_{2+}$와 triethanolamine(TEA)은 산성용액에서 착물형성이 이루어지지 않았으며 1,10-phenanthroline과는 pH=2에서도 착물이 형성되었다.

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