• Journal of the Korean Crystal Growth and Crystal Technology
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• v.8 no.4
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• pp.619-625
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• 1998

The effect of softening point and glass amount of glass frit on the sintering behavior of low temperature cofirable glass/ceramic composites was studied and according to these results, glass/ceramic composites with high sintered density was fabricated. The density of composites was increased as the glass amount was increased. In case of using the glass with low softening point, the deformation of specimen was occurred though the ratio of the glass amount in the specimen was low. But, in case of using the glass with high softening point, the sintered density of composites was increased in accordance with glass amount. With the specimen of high softening point, the deformation was not happened. Therefore, it was found that the densification was progressed continuously in high glass amount. From the study on the effect of softening point of glass on sintering behavior, the suitable softening point and glass amount for fabrication of glass/ceramic composites can be anticipated. When glass frit with softening point of $790^{\circ}C$ was chosen according to this result, low temperature cofirable glass/ceramic composites with high density (97%) at $900^{\circ}C$ was fabricated.

• Journal of the Microelectronics and Packaging Society
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• v.1 no.1
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• pp.51-60
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• 1994

RuO2 계 후막저항체에 사용된 유리의 입도 및 연화점이 후막저항체의 전기적 특성 에 미치는 영향을 시험하기 위하여 연화점이 서로 다른 두 종류의 유리를 제조하고 이들을 미분쇄하여 각각 세 조류의 평균입도로 분급하였다. 이 유리분말들을 이용하여 여섯 종류의 후막저항체를 제조하고 그 저항체들의 전기적 특성을 평가하고 고찰하였다. 연화점이 높은 유리로 만든 후막저항체들보다 높은 쉬트 저항을 나타냈다. 또한 후막저항체들의 쉬트 저항 및 저항온도계수는 저항체들의 미세조직과 밀접한 관계가 있음을 확인하였다.

• Proceedings of the Acoustical Society of Korea Conference
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• 1998.06d
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• pp.9-12
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• 1998

공기경계층을 갖는 유리평판에서 힘의 크기가 10N이고 상승시간이 약 280ns 인 경사 점하중이 인가된 경우에 대하여 진앙점에서 입자 변위와 입자 속도를 계산하였다. 이론적으로 계산된 수직성분이 입자속도가 PZT변환자에 입사한다고 가정하여 PZT 변환자의 과도 응답특성을 Mason 등가회로와 격자점을 이용하여 계산하였다. 유리모세관의 파과시에 방출괴는 과도탄성파를 이용하여 유리평판의 진앙점에서 PZT 변환기의 응답을 조사하였고, 이론과 비교한 결과 상당히 일치하였다. 이를 이용하여 음향방출 시스템인 발생원, 전파매질, 변환자 및 신호분석시스템을 수학적으로 모형화할 수 있는 기초를 마련하였다.

• Journal of Korean Society of Forest Science
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• v.77 no.4
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• pp.421-428
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• 1988

The purpose of this study was to analyze the working time and the efficiency according to plot shape and plot size under the same conditions. We chose two stands which were relatively gently sloped end evenly distributed in number of trees and surveyed 198 plots, and 306 plots in each stand. 1. As to the time advantage of plot establishment method, the direct-four line establishment method was more favorable than the diagonal-line establishment method in a rectangular plot. 2. The method by Blumeleiss-$Me{\beta}$ trommel was more favorable than the method using a tape in a circular plot. 3. As to the time advantage, the circular plot was more favorable than the rectangular plot. Especially, the circular plot was twice more available than rectangular plot in small plot size, but enlargement of plot size gradually decreased time advantage of circular plot.

• Journal of Conservation Science
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• v.33 no.3
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• pp.215-223
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• 2017

The purpose of this study is to reveal the characteristics, correlations, and colorant materials of those using the chemical compositions of 30 glasses excavated from the Sarari hall of the Mireuksaji stone pagoda, and to determine the correlations between them and other glass excavated from the Wanggungri site. The results of the chemical analysis of the 11 glass beads show that they are a soda glass group with high contents of $SiO_2$ and $Na_2O$; these can be further subdivided into soda-alumina groups ($Na_2O-Al_2O_3-CaO-Si_2O$). The characteristics of the stabilizer are classified as being of the high alumina glass group (LCHA), except for two glasses. It was concluded that colorant materials affected the coloring for glass beads by various components including Ti, Mn, Fe, Cu and Pb. In addition, we examined six lead glasses which are glass plate and unknown fragments that are of a common lead glass system ($PbO-SiO_2$) with respect to the average contents of PbO (70wt.%) and $SiO_2$ (30wt.%). As a result of comparing these relics with those of the glass beads excavated by Wanggungri, there is a similarity in that they belong to the soda glass group. However, the contents of $Na_2O$ are relatively higher than that of the glass beads in the Mireuksaji pagoda, and most of relics include glasses with a low content of $K_2O$ and CaO. In addition, the PbO and $SiO_2$ contents are slightly different in the lead glass. It seems that the glass relics made at two different sites may have used different raw materials or techniques.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.213-213
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• 2003

저온소성 가능하며 저 융점유리인 고 투과율의 Pb-free 조성으로서 PDP(Plasma Display panel)의 투명유전체에 응용하고자 P$_2$O$_{5}$-ZnO-RO 계인 인산염 유리의 열적, 광학적성질을 연구하였다. 이 삼원계인 인산염유리계를 PDP의 투명 유전체에 응용하기에는 열적특성에서 문제점이 제기되어, (30-50)P$_2$O$_{5}$ - (20-50)ZnO - (15-45) RO (mol%)계에 유리망목형성제인 A1$_2$O$_3$, SiO$_2$, B$_2$O$_3$등을 첨가하여 열적성질 및 소성후 투광성 등을 조사하였다. 열적특성은 DTA와 TGA를 이용하여 유리전이점(Tg) 및 선팽 창계수(CTE)와 연하점(Ts) 을 측정하였으며, 투광성은 500-58$0^{\circ}C$에서 1시간동안 소성하여 UV-visible spectrometer을 이용하였다 그 결과로, 380-46$0^{\circ}C$의 Tg와 8-$10^{-6}$K의 CTE 및 70-80%의 광투과율을 나타내었다. 이러한 결과는 P$_2$O$_{5}$-ZnO-RO계는 PDP의 투명유전체에 적용하기에는 상당히 높거나 낮은 Tg를 형성하였지만 유리형성제를 수 mol%을 첨가함으로써 적절한 Tg점과 높은 투과율을 얻을 수 있었다.수 있었다.

• Magazine of the Korea Concrete Institute
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• v.5 no.3
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• pp.187-194
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• 1993

본 논문에서는 유리섬유의 적층수, 유리섬유의 배향각도에 대한 유리섬유 강화 플라스틱(Glass Fiber Reinforced Plastics ; GFRP)의 인장거동 변화를 고찰하고, 이들의 상관관계를 규명하기 위하여 일련의 GFRP 시험체에 대하여 인장실험을 수행하였다. 시험체는 폭12.5mm, 길이 60mm크기로 일정하게 제작하였으며, 시험체에 대하여 인장실험을 수행하였다. 시험체 제작시 유리섬유로 적층수는 14, 22, 30층, 유리섬유의 배향각도는 0$^{\circ}$, 30$^{\circ}$, 45$^{\circ}$로 하였다. 인장실험시 각 시험체의 파괴양상, 극한하중 및 하중변화에 대한 인장변형율을 조사하였고, 이들 결과를 토대로 유리섬유의 적층수와 배향각도에 따른 GFRP의 극한하중, 응력-변형율 선도 및 탄성계수 등을 비교 분석하였다. 한편 본 논문에서는 유리섬유의 적층수, 직경 변화에 따른 GFRP관의 파괴거동을 고찰하기 위하여 4점 재하법에 의한 GFRP관의 휨파괴실험을 수행하였다. 실험에 사용된 시험체는 길이 1200mm로 하였으며, 유리섬유의 적층수를 30, 35, 40층, 관의 직경을 50, 100, 150mm로 하였다. 파괴실험시 각 시험체의 하중변화에 대한 휨 변형율, 중앙점 처짐량 및 항복하중을 측정하였고, 이들 결과를 토대로 유리섬유으 적층수와 관의 직경에 따라 GFRP관의 항복하중 및 파괴에너지를 비교 분석 하였으며, 항복시 파괴에너지를 추정할 수 있는 제안식을 유도하였다.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.11a
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• pp.195-195
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• 2003

PDP, FED 등의 디스플레이와 각종 IC 칩부품에 적용 가능한 저융점 유리 프릿 중에서 환경규제가 이루어지고 있는 납성분이 포함되어 있지 않은, Bi계 유리 프릿의 열적 거동 연구를 행하였다. 열처리 온도에 따른 열거동에 따라 프릿의 소성온도 및 미세구조가 결정되므로, 열처리 온도에 따른 유리 프릿의 젖음각을 측정하였고, DTA와 TMA를 통해 유리전이온도, 연화점, 열팽창계수 변화 경향성을 관찰하였다. 본 연구에서 제조된 유리는 조성에 따라 전이온도가 390-50$0^{\circ}C$, 연화점이 400-55$0^{\circ}C$, 열팽창계수가 65-120$\times$10-7/$^{\circ}C$ 범위를 나타내었으며, 고온현미경 측정 결과 Pb-계 유리와 비교시 유사한 열거동을 나타내었다.

• Journal of Conservation Science
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• v.36 no.5
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• pp.405-420
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• 2020

A convergence research was conducted on glass beads excavated at the ruins of Hapgang-ri, Sejong, using the archeology and conservation approach. The period of appearance of Jugu Towangmyo in the ruins of Hapgang-ri can be estimated to begin in the late 2^nd century; for Jugu Towangmyo No. 15, the period spans from the late 2^nd to early 3^rd century. Form, color, and manufacturing techniques of complete glass beads were examined, and the cross-sections and chemical composition of 16 samples were observed. Based on these analyses, the glass beads were divided into blue, purple, and red colors. The blue-colored beads could be further sub-divided based on their gloss and brightness; in contrast, the red-colored beads were highly uniform with regard to these parameters. Based on the stripe and bubble arrangement on the surface of the glass beads, their drawing technique was identified. Traces of heat treatment or polishing were observed at the ends of the beads. According to their chemical composition, the 16 samples were classified into 3 potash glass and 13 soda glass groups; in the latter, the properties of the stabilizers were divided according to the blue and red bead colors. The stabilizers of the red beads are unique in that they allow the distinction among beads excavated in other areas in South Korea owing to their compositional differences. Colorants in blue- and red-colored beads are cobalt (containing MnO), and copper and iron, respectively.

• Journal of Conservation Science
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• v.28 no.3
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• pp.205-216
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• 2012

65 samples of glass bead excavated from Mahan tombs of Asan Bakjimeure site consists of 13 of potash glass group and 52 of soda glass group and soda glass is superior in numbers. When classified according to color, purple blue glass bead is accompanied potash and soda glass group whereas purple glass bead is potash glass group and red, greenish blue, green and gold foil glass bead is soda glass group. Purple blue glass bead is classified as LCA type in which the content of the stabilizer is low. Of this, the soda glass categorized as LMK type with low content of MgO and $K_2O$ is determined that natron is used as the raw material. As to red glass, the homogeneous glass is LCA-B/HMK type and the heterogeneous glass is HCLA/LMK type. Thus, each of these two types are likely to be used plant ash and natron respectively. Greenish blue and green glass depends of the type that round glass is LCA-A/LMHK type and the segmented glass is LCA-B/HMK type. The gold foil glass bead is manufactured by the purity of 19.9~22.6K gold foil and the soda glass of HCLA/LMK type. In other words, the most of the glass bead of Asan Bakjimeure site is similar to the composition of the glass confirmed in other sites of the Baekche period. On the other hand, the greenish blue and green segmented bead and some red round bead is a different chemical composition is considered that the difference in raw materials. These characteristics is expected to be an important evidence for the understanding of the trade system of the ancient glass.