• Title/Summary/Keyword: 어닐링

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Preparation and Interface Characteristics of $PbTiO_3$ Ferroelectric Thin Film (강유전성 $PbTiO_3$ 박막의 형성 및 계면특성)

  • Hur, Chang-Wu;Lee, Moon-Key;Kim, Bong-Ryul
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.26 no.7
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    • pp.83-89
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    • 1989
  • Ferroelectric $PbTiO_3$ thin film is deposited with rf sputtering at substrate temperature of $100-150^{\circ}C$. It is found that this has pyrochlore structure of amorphous type by X-ray diffractive analysis. Thermal annealing has excellent characteristics at $550^{\circ}C$ and laser annealing has best crystalline structure in case of scanning with 50 watts. Interface states in MFST and MFOST structure with a $PbTiO_3$ ferroelectric thin film gate have been investigated from analysis of C-V data. The interface states density has been drastically reduced by inserting an oxide layer between ferroelectric and semiconductor. The observed effect increase feasibility of employing ferroelectric thin films such as nonvolatile memory field effect transistor, IR optical FET, and Image Devices with a ferroelectric layer.

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Color Image Segmentation Based on Morphological Operation and a Gaussian Mixture Model (모폴로지 연산과 가우시안 혼합 모형에 기반한 컬러 영상 분할)

  • Lee Myung-Eun;Park Soon-Young;Cho Wan-Hyun
    • Journal of the Institute of Electronics Engineers of Korea SP
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    • v.43 no.3 s.309
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    • pp.84-91
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    • 2006
  • In this paper, we present a new segmentation algorithm for color images based on mathematical morphology and a Gaussian mixture model(GMM). We use the morphological operations to determine the number of components in a mixture model and to detect their modes of each mixture component. Next, we have adopted the GMM to represent the probability distribution of color feature vectors and used the deterministic annealing expectation maximization (DAEM) algorithm to estimate the parameters of the GMM that represents the multi-colored objects statistically. Finally, we segment the color image by using posterior probability of each pixel computed from the GMM. The experimental results show that the morphological operation is efficient to determine a number of components and initial modes of each component in the mixture model. And also it shows that the proposed DAEM provides a global optimal solution for the parameter estimation in the mixture model and the natural color images are segmented efficiently by using the GMM with parameters estimated by morphological operations and the DAEM algorithm.

A Study of Gamma-ray Irradiation Effects on Commercially Available Single-mode Optical Fiber using Fiber Bragg Grating Sensor Systems (광섬유 브래그 격자 센서를 이용한 국내외 상용 단일모드 광섬유의 감마선 영향 연구)

  • Kim, Jong-Yeol;Lee, Nam-Ho
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.16 no.10
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    • pp.2287-2292
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    • 2012
  • In this study, $Co^{60}$ gamma-ray induced loss on Ge-doped single mode (SM) fiber has been measured. Gamma-ray is irradiated for 4 hours at the dose rate of 0.5 kGy/hr, 2 kGy/hr, 8 kGy/hr. Consequently, gamma-ray induced loss based on radiation effects in Ge-doped SM fiber occur significantly. Furthermore, dose rate effect was observed, that dose rate using the same total dose increased higher, then optical fiber loss increased more. Also annealing effect was observed, that the loss after irradiation, increased higher, then the recovery rate of loss was increased. This results are foreseen to be base data in the future radiation-hardened optical fiber study.

Research on the development of the properties of PLA composites for automotive interior parts (자동차 내장재 적용을 위한 PLA 복합재료의 물성개선에 관한 연구)

  • Jung, Jae-Won;Kim, Seong-Ho;Kim, Si-Hwan;Park, Jong-Kyoo;Lee, Woo-Il
    • Composites Research
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    • v.24 no.3
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    • pp.1-5
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    • 2011
  • Since the environmental problems and new stricter regulations are forcing the industries to introduce more ecological materials for their products, biodegradable materials have attracted increasing attention. Among these materials, Polylactic acid(PLA) is a promising candidate for its modulus, strength, chemical resistance. However, PLA could not be used for automobile industries for its low heat resistance and impact strength. In this study natural fibers were (jute fiber was) introduced as reinforcements in order to improve heat resistance and impact strength of PLA. Especially for improving the adhesion between PLA and jute, various surface treatments were tried. With each treatment, we verified that the impact strength of composite was improved. With annealing treatment, we found a remarkable increase of heat resistance of PLA composite.

Ti-50.4 at% Ni 합금의 형상기억특성에 미치는 냉간가공률의 영향

  • Go, Won-Gi;Kim, Jae-Il;Park, Su-Ho;Kim, So-Jin;Kim, Hyeon;Lee, Gi-Yeong
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2012.05a
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    • pp.106.2-106.2
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    • 2012
  • Ti-Ni합금은 CsCl구조의 B2상, monoclinic 구조의 B19'(M)상과 rhombohedral 구조의 R상(R)이 나타난다고 알려져 있고, 이들 상의 변태에 의해 열탄성 마르텐사이트와 응력유기 마르텐사이트에 의한 형상기억효과와 초탄성 효과를 가지고 있다. 또한 Ti-Ni 합금은 우수한 형상기억특성을 가질 뿐만 아니라 생체적합성, 가공성 및 내식성 등이 뛰어나 공업분야 및 생체분야에서 폭 넓게 활용되고 있다. Ti-Ni합금의 형상기억특성은 냉간가공 후 어닐링 처리의 온도와 시간에 따른 matrix 내 Ni의 농도, 석출물의 밀도와 크기, 전위밀도와 전위주위의 응력장에 의해 영향을 받는다고 알려져 있다. 본 연구에서는 Ti-Ni합금의 형상기억 특성 및 변태온도에 미치는 영향을 조사하기 위해 다양한 냉간가공률의 시료를 제작하여 다양한 온도에서 Annealing 처리를 하여 냉간가공률 및 Annealing 온도가 형상기억특성에 미치는 영향을 조사하였다. Ti-50.4 at.% Ni 합금은 진공 아크 용해로에서 용해 하였으며, 용해된 Ingot는 열간단조 및 열간 압출한 후 냉간 인발과 중간온도에서 어닐링을 반복하면서 직경 0.5mm의 선재로 만들었다. 최종적으로 제작한 선재의 냉간가공률은 9.5%, 18.2%, 34.5%, 45% 이었다. 각 시편은 5X10-5torr의 진공으로 석영관에 진공 봉입하여 각각 673K, 723K, 783K에서 1hr 열처리 하였다. 합금의 형상기억특성과 변태온도는 DSC에 의해 조사되었다. DSC 측정 결과, 냉간가공률이 증가함에 따라 마르텐사이트 변태 온도는 감소하였고, 어닐링 온도가 증가함에 따라 마르텐사이트 변태 온도는 증가하였다. 또한 가공률이 증가하여도 R상 변태온도는 큰 변화가 없었고, Annealing온도가 증가함에 따라 R상 변태온도는 감소하였다. 또한, 형상기억특성은 인장시험기를 이용한 정하중 열싸이클 테스트를 이용하여 평가 하였다. 냉간 가공률이 증가함에 따라 안정한 형상기억특성을 나타내었다.

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Effects of Dopants Introduced into the Poly-Si on the Formation of Ti-Silicides (Poly-Si에 첨가한 도펀트가 Titanium Silicides 형성에 미치는 영향 Ⅱ)

  • Ryu, Yeon-Soo;Choi, Jin-Seog;Paek, Su-Hyon
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.27 no.2
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    • pp.73-80
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    • 1990
  • The formation of Ti-silicides with the type of substrate, the species and the concentration of dopant, and the annealing temperature was investigated with sheet resistance and thickness measurement, elemental depth profilling, and microstructure. It was directly affected by the type of substrate, the species and the concentration of dopant, and the annealing temperature. For the amorphous Si substrate, the smothness of $TiSi_2/Si$ interface was increased. Above concentr-ation of $1{\times}10^{16}ions/cm^2$, the rate of $TiSi_2/Si$ formation was decreased and the sheet resistance was increased. The initial profile of dopant according to the implantation energy was one of the factors influencing the out-diffusion of dopant. In $POCI_3$ process, this was less than in ion implantation process.

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An Energy Optimization Algorithm for Maritime Search and Rescue in Wireless Sensor Networks (무선 센서 네트워크에서 해양 수색 및 구조를 위한 에너지 최적화 알고리즘)

  • Jang, Kil-woong
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.22 no.4
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    • pp.676-682
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    • 2018
  • In wireless sensor networks, we propose an optimization algorithm in order to minimize the consumed energy of nodes for maritime search and rescue. In the marine environment, search and rescue operations are mainly performed on the surveillance side and passively on the rescued side. A self-configurable wireless sensor network can build a system that can send rescue signals in the operations. A simulated annealing algorithm is proposed to minimize the consumed energy of nodes in the networks with many nodes. As the density of nodes becomes higher, the algorithmic computation will increase highly. To search the good result in a proper execution time, the proposed algorithm proposes a new neighborhood generating operation and improves the efficiency of the algorithm. The proposed algorithm was evaluated in terms of the consumed energy of the nodes and algorithm execution time, and the proposed algorithm performed better than other optimization algorithms in the performance results.

Microstructure and Conductivity of Cu-Nb Microcomposites Fabricated by Bundling and Drawing Process (다발체형성과 인발공정에 의해 제조된 Cu-Nb 미세복합재료의 미세조직과 전도도)

  • Kwon, Hoi-Joon;Hong, Sun-Ig;Jee, Kwang-Koo
    • Korean Journal of Materials Research
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    • v.11 no.2
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    • pp.115-119
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    • 2001
  • The electrical properties of heavily drawn bundled Cu- Nb filamentary microcomposite wires were examined and correlated with the microstructural changes caused by thermomechanical treatments. The cross sectional shape of Nb filaments in wires fabricated by bundling and drawing appear straight or slightly curved. The different shape of Nb filaments is attributed to the break- up and cylinderization of Nb filaments during the bundling process at high temperatures. The resistivity of Cu-Nb microcomposites is predominantly controlled by electron scattering at Cu-Nb interfaces. The decrease of the conductivity below the annealing temperature of $400^{\circ}C$ is due to the increasing contribution of the scattering associated with coherency strains of needle- shaped precipitates. The slight decrease of the resistivity ratio (${\rho}_{295K}/{\rho}_{75K}$) is also due to the precipitation of Nb atoms. The increase in conductivity in Cu-Nb microcomposites at an annealing temperature of 50$0^{\circ}C$ is due to the coarsening and spheroidization of Nb filaments.

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Study on Electrical Characteristics of FDM Conductive 3D Printing According to Annealing Conditions (FDM 3D 전도성 프린팅 어닐링 조건 따른 전기적 특성 연구)

  • Lee, Sun Kon;Kim, Yong Rae;Yoo, Tae Jung;Park, Ji Hye;Kim, Joo Hyung
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.6
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    • pp.53-60
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    • 2018
  • In this paper, the effect of different 3D printing parameters including laminated angle and annealing temperature is observed their effect on FDM conductive 3D printing. In FDM 3D printing, a conductive filament is heated quickly, extruded, and then cooled rapidly. FDM 3D Print conductive filament is a poor heat conductor, it heats and cools unevenly causing the rapid heating and cooling to create internal stress. when the printed conductive specimens this internal stress can be increase electrical resistance and decrease electrical conductivity. Therefore, This experiment would like to use annealing to remove internal stress and increase electrical conductivity. The result of experiment when 3D printing conductive specimen be oven cooling of annealing temperature $120^{\circ}C$ electrical resistance appeared decrease than before annealing. So We have found that 3D printing annealing removes internal stresses and increases the electrical conductivity of printed specimens. These results are very useful for making conductive 3D printing electronic circuit, sensor ect...with electrical conductance suitable for the application.

Effect of Heat Treatment on Mechanical Properties of Cross-Linked Ultra-High Molecular Weight Polyethylene Used for Artificial Joint Liner (인공관절 라이너용 가교된 초고분자량폴리에틸렌(UHMWPE)의 열처리 조건에 따른 기계적 특성 변화)

  • Kim, Hyun-Mook;Kim, Dong-Hoon;Gu, Ja-Uk;Choi, Nak-Sam;Kim, Sung-Kon
    • Composites Research
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    • v.22 no.2
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    • pp.1-6
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    • 2009
  • The mechanical characteristics of gamma-ray irradiated UHMWPE specimens were investigated under various heat treatment conditions. The heat treatment was performed in the range of annealing and remelting temperatures. The annealing treatment below the temperature of $130^{\circ}C$ hardly induced changes in the tensile strength, the strain at the failure and the hardness. However the remelting treatment above $140^{\circ}C$ deteriorated those mechanical properties. It was shown in an FTIR analysis that the annealing treatment caused some oxidation of free radicals created by the pretreatment of the irradiation. These quantitative data represented by the behavior of mechanical properties might be used as basic informations for the design and analysis of various artificial joints.