• Title/Summary/Keyword: 압착공정

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Effect of $N_2+H_2$ Forming Gas Annealing on the Interfacial Bonding Strength of Cu-Cu thermo-compression Bonded Interfaces (Cu-Cu 열압착 웨이퍼 접합부의 계면접합강도에 미치는 $N_2+H_2$ 분위기 열처리의 영향)

  • Jang, Eun-Jung;Kim, Jae-Won;Kim, Bioh;Matthias, Thorsten;Hyun, Seung-Min;Lee, Hak-Joo;Park, Young-Bae
    • Journal of the Microelectronics and Packaging Society
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    • v.16 no.3
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    • pp.31-37
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    • 2009
  • Cu-Cu thermo-compression bonding process was successfully developed as functions of the $N_2+H_2$ forming gas annealing conditions before and after bonding step in order to find the low temperature bonding conditions of 3-D integrated technology where the quantitative interfacial adhesion energy was measured by 4-point bending test. While the pre-annealing with $N_2+H_2$ gas below $200^{\circ}C$ is not effective to improve the interfacial adhesion energy at bonding temperature of $300^{\circ}C$, the interfacial adhesion energy increased over 3 times due to post-annealing over $250^{\circ}C$ after bonding at $300^{\circ}C$, which is ascribed to the effective removal of native surface oxide after post-annealing treatment.

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Analysis of Benzo[α]pyrene Content in Edible Oils from Korean Market (시중에 유통되는 식용유지 중 benzo[α]pyrene 함량 분석)

  • Nam, Hejung;Seo, Ilwon;Lee, Kyueun;Lee, Songyoung;Shin, Han-Seung
    • Food Engineering Progress
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    • v.13 no.3
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    • pp.211-215
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    • 2009
  • Concentrations of benzo[$\alpha$]pyrene in edible oils from Korean market were evaluated by high performance liquid chromatography. Benzo[$\alpha$]pyrene known of the carcinogenic polycyclic aromatic hydrocarbons(PAHs), has been found at variable concentrations in several foods. This is associated with several factors during the process including contaminated raw materials, exposure of environment, and procedure of process or cooking. The levels of benzo[$\alpha$]pyrene were ranged from 0.5 to 1.4 $\mu$g/kg in virgin olive oil. Benzo[$\alpha$]pyrene contents in refined and virgin olive oil, sesame oil, soybean oil, corn oil, sunflower oil, safflower oil, and processed oil were 0.6-1.0 $\mu$g/kg, 0.9-1.3 $\mu$g/kg, 0.6-3.3 $\mu$g/kg, 0.5-1.1 $\mu$g/kg, 1.2-1.7 $\mu$g/kg, 1.0-2.1 $\mu$g/kg, and 1.0-1.4 $\mu$g/kg, respectively.

A Study on Manufacturing Method of Standard Void Specimens for Non-destructive Testing in RFI Process and Effect of Void on Mechanical Properties (RFI 공정 부품 비파괴검사용 표준 기공률 시편 제조 방법 및 기공률에 따른 기계적 물성 영향에 대한 연구)

  • Han, Seong-Hyeon;Lee, Jung-Wan;Kim, Jung-Soo;Kim, Young-Min;Kim, Wee-Dae;Um, Moon-Kwang
    • Composites Research
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    • v.32 no.6
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    • pp.395-402
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    • 2019
  • The RFI process is an OoA process that fiber mats and resin films are laminated and cured in a vacuum bag. In case that resin film is insufficient to fill empty space in fibers, it makes void defect in composites and this void decrease mechanical properties of the composites. For this reason, non-destructive testing is usually used to evaluate void of manufactured composites. So, in this study, a manufacturing method of standard void specimens, which are able to be used as references in non-destructive testing, was proposed by controlling resin film thickness in the RFI process. Also, a fiber compaction test was proposed as a method to set the resin film thicknesses depending on target voids of manufacturing panels. The target void panels of 0%, 2%, and 4% were made by the proposed methods, and signal attenuation depending on void was measured by non-destructive testing and image analysis. In addition, voids of specimens for tensile, in-plane, short beam and compressive tests were estimated by signal attenuation, and mechanical properties were evaluated depending on the voids.

The Fabrication and Characterization of Embedded Switch Chip in Board for WiFi Application (WiFi용 스위치 칩 내장형 기판 기술에 관한 연구)

  • Park, Se-Hoon;Ryu, Jong-In;Kim, Jun-Chul;Youn, Je-Hyun;Kang, Nam-Kee;Park, Jong-Chul
    • Journal of the Microelectronics and Packaging Society
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    • v.15 no.3
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    • pp.53-58
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    • 2008
  • In this study, we fabricated embedded IC (Double Pole Double throw switch chip) polymer substrate and evaluate it for 2.4 GHz WiFi application. The switch chips were laminated using FR4 and ABF(Ajinomoto build up film) as dielectric layer. The embedded DPDT chip substrate were interconnected by laser via and Cu pattern plating process. DSC(Differenntial Scanning Calorimetry) analysis and SEM image was employed to calculate the amount of curing and examine surface roughness for optimization of chip embedding process. ABF showed maximum peel strength with Cu layer when the procuring was $80\sim90%$ completed and DPDT chip was laminated in a polymer substrate without void. An embedded chip substrate and wire-bonded chip on substrate were designed and fabricated. The characteristics of two modules were measured by s-parameters (S11; return loss and S21; insertion loss). Insertion loss is less than 0.55 dB in two presented embedded chip board and wire-bonded chip board. Return loss of an embedded chip board is better than 25 dB up to 6 GHz frequency range, whereas return loss of wire-bonding chip board is worse than 20 dB above 2.4 GHz frequency.

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Manufacturing of Goami Flakes by using Extrusion Process (압출성형공정을 이용한 고아미 후레이크 제조)

  • Tie, Jin;Lee, Eui-Suk;Hong, Soon-Teak;Ryu, Gi-Hyung
    • Korean Journal of Food Science and Technology
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    • v.39 no.2
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    • pp.146-151
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    • 2007
  • Resistant starch (RS) content, paste viscosity, water solubility and absorption index, bulk density, color, compression force, and bowl life of Goami flakes manufactured by extrusion process were determined to evaluate Goami (high fiber rice) as a food material. Various extrusion process conditions included barrel temperature (90, 110, $130^{\circ}C$) and moisture content (50, 55%). RS content in the extruded pellet and defatted flake ranged from $8.00{\sim}8.56%$ and $6.57{\sim}9.53%$ respectively. RS content increased as moisture increased from 50% to 55%. Peak viscosity, trough viscosity, final viscosity, and setback viscosity of the extruded pellet and defatted flake decreased with steeping for 1 hr, and the breakdown viscosity significantly increased. The water solubility and absorption index increased in the flake compared to Goami and extruded pellet. The water solubility index of the extruded pellet was lower than that of Goami, while its water absorption index was higher than Goami. The bulk density of the flake ranged from $0.35{\sim}0.44$ g/mL. The bowl life of the flake was $12.4{\sim}19.4$ min, which was longer than commercial breakfast cereals on the market.

Study on the Manufacturing of Leather-like Material using Leather and Textile Scrap (피혁 및 섬유 제조공정 폐기물을 활용한 피혁 대체 소재의 제조에 관한 연구)

  • Kim, Won-Ju;Ko, Jae-Yong;Heo, Jong-Soom
    • Journal of the Korea Organic Resources Recycling Association
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    • v.8 no.4
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    • pp.93-99
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    • 2000
  • Treatment of shaving scrap, a chrome containing solid scrap generated by leather manufacturing process, has been so far depended on mainly incineration, soil landfill and ocean dumping, which give bad impact on environment and cause pollution. Shaving scrap generates from the mechanical work for controlling the final thickness of leather and its main components are collagen protein and pan of chromium compound. For the purpose of reusing this leather waste as resources, researches in connection with collagen fiber recovery, gelable protein recovery and liquid fertilizer is being speedily progressed. In the experiment, shaving scrap went through wet pulverizing treatment by physical and chemical methods. Then, making the leather sheet evenly, it is mixed with natural latex and every kind of binding materials in the container, and the mixtures were passed through experimental hydraulic press machine and applied to Fourdrinier machine respectively. Lastly, a test for fading out physical strength and properties of multiple-purpose of leather-like material was performed on a continuous leather sheet prepared by the experiment. In result, the physical strength and properties of leather-like material showed noticeable differences according to mixing ratio of binding materials, beating methods and the Ends of binding materials selected, and generally tear strength was the weakest property among others. Also, by the pilot scale experiment in sequence, it was possible to manufacture recycled goods made of soft and hard types of leather-like material with various performances.

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Reason and Prevention of Color Reversion of Corn Oil in Summer (옥수수기름의 하절기 변색현상 원인규명 및 방지대책)

  • Koo Bon-Soon
    • Food Science and Preservation
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    • v.11 no.4
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    • pp.485-490
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    • 2004
  • Crude corn oil (CCO) was obtained through the expression-extraction process from corn germ. The CCOs of final process at $90^{\circ}C,\;70^{\circ}C\;and\;50^{\circ}C$ were stored in outdoor storage tanks. From the samples, refined CCO (RCCO) were prepared with $0\%,\;10\%\;and\;20\%$ excessive of phosphoric acid, caustic solution and acidic clay were used in degumming-alkali refining-bleaching process. RCCOs were stored at room temperature in dark places. The color change was not effected by the amount of phosphoric acid, caustic solution and acidic clay, but temperature of process affects the color change. Finally, the prevention for color reversion of RCCO could be obtained by lowering the temperature of final process and optimal temperature of RCCO in summer was found about less than $50^{\circ}C$.

FE-Analysis on void closure behavior during hot open die forging process (열간 자유단조 공정시 내부 기공 압착 거동에 관한 해석)

  • Kwon, Y.C.;Lee, J.H.;Lee, S.W.;Jung, Y.S.;Kim, N.S.;Lee, Y.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.160-164
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    • 2007
  • In the steel industry, there is a need to produce large forged parts for the automobile industries, the flight and shipping industries ad military industries. In the steel-industry application, a cogging technique for cast ingots is required, because the major parts are needed as one large body in order to obtain higher quality. Therefore, cogging process is the primary step in manufacturing of practically large open-die forging. In the cogging process, internal voids have to be eliminated as defects, The present work is concerned with the elimination of the internal voids in large ingots so as obtain sound products. In this study, hot compression tests were carried out to obtain the flow stress of cast microstructure at different temperature and strain rates. The FEM analysis are performed to investigate the overlap defect of cast ingots during cogging stage. The measure flow stress data were used to simulate the cogging process of cast ingot using the practical material properties. Also the analysis of void closure are performed by using the $DEFORM^{TM}$-3D. The calculated results of void closure behavior are compared with the measured results before and after cogging, which are scanned by the X-ray scanner. From this result, the criteria for deformation amounts effect on the void closure can be investigated by the comparison of practical experiment and numerical analysis.

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The influence of factors on the strength of formed coke made with anthracite and phenolic resin (무연탄(無煙炭)과 페놀수지(樹脂)의 혼합(混合)소성에 의해 제조(製造)된 함형(咸形)코크스의 강도(强度))

  • Lee, Gye-Seung;Song, Young-Jun
    • Resources Recycling
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    • v.17 no.6
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    • pp.57-61
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    • 2008
  • The aim of this study is to produce the coke which can be used for the production of ferroalloy, by mixing phenolic resin and anthracite and sintering it. The influence of factors on the strength of coke were investigated. The results of this study are as follows: It is found that the anthracite coke of $100{\sim}150\;kgf/cm^2$ strength for ferroalloy can be made by a series of process as follows; Mixing homogeneously 6% liquefied phenolic resin and 6% water with $35{\sim}325$ mesh anthracite of low ash content. Making pellet by press the mixture in $10-50\;kgf/cm^2$ pressure. Dehydrating the pellet for 6 hrs at $50^{\circ}C$, and hardening it for 180 min at $200^{\circ}C$. Sinter the mixture for 6 hrs at $1,200^{\circ}C$.

Effect of Colloidal Silica on Selective Catalytic Reduction (SCR) Catalyst Activity and Thermal Stability (Colloidal Silica의 특성이 SCR 촉매의 성능 및 열적 안정성에 미치는 영향)

  • Cha, Jin-Sun;Lee, Hyung Won;Shin, Min-Chul;Jeong, Bora;Kim, Hong-Dae
    • Applied Chemistry for Engineering
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    • v.31 no.1
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    • pp.61-66
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    • 2020
  • In this study, the effect of characteristics of colloidal silica, which was used as an additive in the compression/coating catalyst process, on activities and thermal stabilities of the catalysts was investigated. The shape, size, specific surface area and porosity, and composition of four different types of colloidal silica materials were analyzed, and the NOx conversion of V2O5/TiO2 catalyst prepared by these colloidal silica were studied. Properties of the catalysts prepared by colloidal silica depend on the nature of the colloidal silica used, in particular the alkaline substances such as Na in the silica were evaluated to be directly effect on the deNOx conversion of the catalyst. In addition, higher silica contents in the colloidal silica were found to improve the deNOx activity and thermal stability of the catalyst.