• Proceedings of the Korea Air Pollution Research Association Conference
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• 2002.04a
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• pp.231-232
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• 2002

대기중에 존재하는 미량의 극성 유기화합물들은 비극성 유기화합물 보다는 반응성이 크고 불안정하므로 이를 채취하여 분석하는 과정이 매우 어려운 실정이다. 일반적으로 sampling에 자주 사용되는 stainless steel로 특수 내면처리 시킨 canister를 이용하였으나 이 방법에 의한 시료 채취방법은 고가의 비용이 소요되며, 반응성이 큰 VOC의 경우에는 성분에 따라 안정도가 낮은 경우도 많다. 그러므로 본 연구에서는 대기 시료를 bag 이나 캐니스터와 같은 용기로서 채취하여 측정할 경우 극성 VOC 성분이 얼마나 안정하게 유지될수 있는지를 조사하고저 하였다. (중략)

• Korean Journal of Food Science and Technology
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• v.53 no.6
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• pp.669-681
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• 2021

The content of major constituents and antioxidant activities of two lavers (Pyropia seriata, Pyropia dentata) selected through breeding at different regions (Jangsan-do, Amtae-do, Dali-do, Jin-do, Muan) were compared in this study. The mineral contents of both cultivars were in the following order: K>Na>Mg>Ca>Fe>Zn>Mn>Cu. The content of major fatty acids was as follows: eicosapentaenoic acid>palmitic acid>arachidonic acid>dihomo-ɣ-linolenic acid. Main constituents of total and free amino acids were as follows: alanine>glutamic acid>aspartic acid. In particular, the total amino acid content in P. dentata was higher than that in P. seriata and was the highest in the sample from Jangsan-do in January. In addition, in terms of total phenolic content, reducing power, and DPPH radical-scavenging activity of both samples collected in January and February, P. dentata showed better characteristics than P. seriata. This study may provide useful information for the selection of laver in high quality.

• Journal of Korean Society for Atmospheric Environment
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• v.13 no.2
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• pp.147-159
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• 1997

One of the most critical problems associated with filter-pack data comparisons from various field networks is the use of different sampling flow rates. In this field study, the effects of various filter-pack(FP) sampling conditions were examined. Experiments were conducted to evaluate the effects of varying sampling flow rates (1.5 to 10 sLpm) on measured concentrations of dry acid deposition species. Collocated FP samples were also collected to determine sampling and analysis data reproducibility. Ambient air samples were collected simultaneously for the seven day durations at varous flow rate. The chemical species measured were sulfur dioxide ($SO_2$), particulate sulfate(P-$SO_{4}^{2+}$), nitric acid ($HNO_3$), and particulate nitrate (P-$NO_{3}^{-}$). The results indicated that the collocated samples can be measured reproducibly and that sampling bias for the species measured is not significant. It was concluded that variations in the flow rates (1.5 to 10 sLpm) did not significantly affect the concentration of the species of interest. Although the results were not significantly different between different flow rates, artifacts were more likely to occur at high flow conditions (>5 sLpm) (e.g., via volatilization of particulate nitrates) than at low flow conditions(<5 sLpm).

• Journal of Korean Society of Environmental Engineers
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• v.37 no.1
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• pp.45-51
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• 2015

PBDEs (polybrominated diphenyl ehters) are rarely dissolved in water due to their strong hydrophobicity and large molecular mass so not many researches were done in aqueous environment compared to other environmental compartments. However, the mass loading from wastewater treatment plant into aquatic environment, re-suspension from bottom sediment and partitioning from floating particles and colloids may not be negligible. It is, therefore, important but also difficult to investigate PBDEs in water environment. Recent overcoming resolution towards this barrier to monitor hydrophobic organic compounds in aquatic environment is using passive sampling technique like semipermeable membrane device. By using passive sampling, it might be possible to obtain long-term reproducible monitoring result and detect the trace amounts of PBDEs, with controlling fluctuation of surrounding environmental factors during the sampling event. So therefore, this study is purposed to confirm the possibility of using SPMD (semi-permeable membrane device) as water monitoring tool. Grab samples, composite samples and SPMDs were applied in river bank to evaluate the concentration difference and temporal fluctuation by various water sampling method, and to assess the water concentration prediction capability of SPMD for the PBDEs.

• Journal of the Korean GEO-environmental Society
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• v.23 no.7
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• pp.11-20
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• 2022

Planetary geotechnical investigation in charge of drilling and soil sampling is of a great importance in providing extraterrestrial geotechnical information. Extraterrestrial subsurface investigation, which includes drilling, soil sampling, and sample transportation, will be loaded in a lander or a rover. Scientists from all over the world are interested in the design and development of a drilling system with various functions due to potential applications in planetary surface exploration mission. However, it is difficult to build a fully functional drilling system in extreme environment conditions. This paper presents engineering considerations for the design and development of soil sampling including drilling and performance verification in extreme environment conditions in detail.

• Korean Journal of Clinical Laboratory Science
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• v.53 no.4
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• pp.326-332
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• 2021

Swabs are useful and common sampling tools in various research fields, such as medicine, ecology, biotechnology, forensic medicine, and pollutant monitoring systems. Collection reagents are one of the essential components in sampling. It is important to develop a sample collection kit and designate an appropriate storage temperature because samples need to be stored for a long time. The purpose of this study was to identify the effects of three collection reagents and three storage temperatures on the recovery of living bacteria without media. We selected Escherichia coli and Staphylococcus aureus as representative environmental bacteria. Distilled water (DW), phosphate buffered saline (PBS), and Tris-EDTA (TE) buffer were used as collection reagents and stored at 22℃, 4℃, and -70℃ after sampling. The results of using each collection reagent and storage temperature on the bacteria were compared using relative light units (RLU) and the number of colony forming units (CFU). When using -70℃ storage temperature and the TE buffer, the number of living bacteria and the RLU values remained constant. It is therefore recommended that the sample be stored at -70℃ immediately after collection and a TE buffer solution be used as the collection reagent.

• Analytical Science and Technology
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• v.37 no.3
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• pp.174-188
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• 2024

This review summarized research trends regarding sample collection methods, pretreatment method, and types of analysis devices for microplastics (MPs) in soil and groundwater matrices. Soil sampling considers the selection of sampling location, depth, and volume. The typically sampling depth is within 15 cm (topsoil), and about 1 kg of mixed each sample. Among spot sampling and continuous flow sampling, groundwater sampling mainly used a continuous flow sampling, with collection rates 2 to 6 L/min in the range of 300~1,000 L, and followed by immediate on-situ filtration. Pretreatment method, applied to soil and groundwater, consist of organic digestion and density separation. In the organic digestion method, H₂O₂ is recommended among H₂O₂, acidic, alkaline, and enzymatic method. NaCl is primarily used as a reagent in density separation. However, depending on the density of MPs, other regents can be selectively used like ZnCl₂, ZnBr₂, and etc. Representative analysis device includes Fourier Transform Infrared (FTIR) and Raman spectroscopy for non-destructive analysis and Pyrolysis Gas Chromatography Mass Spectrometry (Py-GC/MS) for destructive analysis. µ-FTIR and Raman can count MPs of larger than 10 and 1 ㎛, and analyze MPs materials. However, it is need to sufficiently remove interference, like organic matter, in spectroscopic analysis using essential pretreatment method. Py-GC/MS is being continuously researched because it doesn't require complex pretreatment method and allows quantitative analysis of specific materials.

• Journal of the Korean Society of Hazard Mitigation
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• v.5 no.4 s.19
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• pp.29-36
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• 2005

In this study, relations among unconfined compressive strength, strain at maximum strength and depth were compared with each other. Test specimen is marine clay originated from the place near Ga-duck island in Busan city. In addition, influence of impure material contained in specimen and that of total core recovery(TCR) on unconfined compressive strength and degree of disturbance were investigated. As a result of tests, unconfined compressive strength decreases as strain corresponding to maximum strength increases. Also, the deeper the sampling depth and the bigger the TCR, the unconfined compressive strength increases. Especially, as the TCR increases, the unconfined compressive strength Increases and quality of specimen is enhanced.

• Journal of the Korean Geotechnical Society
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• v.15 no.5
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• pp.125-139
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• 1999

It is difficult to evaluate the shear strength of weathered residual soils because of the difficulties of undisturbed sampling. In this study, a sampling device, direct shear box with shoe, was developed in order to get undisturbed samples easily for direct shear tests, and undisturbed samples could be successfully obtained. Through direct shear tests on undisturbed samples, the shear strength was evaluated with the variation of saturated conditions. In order to consider the effect of disturbance on the shear strength, a static compaction device was developed, and then it was found that undisturbed samples show greater shear strengths than the disturbed ones under natural water contents and similar strengths to the ones under soaked conditions. Further, the shear strength evaluated from direct shear tests was compared with the result of triaxial tests on undisturbed samples, and soaked strengths of the former were similar to the latter. As the result of stability analyses on an actual failed slope, it was found that the shear strength can be evaluated reasonably using direct shear box with shoe.

• Proceedings of the KSEG Conference
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• 2004.03a
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• pp.14001-14039
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• 2004

시추조사는 지반상태를 파악하기 위한 조사중에서 가장 기본적이며 구체적인 조사방법이다. 원 하는 심도의 시료를 채취하여 지층을 직접 확인할 수 있고, 이 시료를 가지고 각 종 시험을 할 수 있기 때문이다. 더구나 시추공에서 시험할 수 있는 각종 정밀한 장비들이 개발되면서 시추공시험으로써 많은 지하정보를 얻을 수 있게 되었다. 이 정보들은 현장의 정보이기 때문에 실내시험에서 얻는 정보보다는 훨씬 가치가 있으므로 시추조사의 목적은 시료채취보다는 공내시험에 더 비중을 두게 되었다. 시추공 시험은 1.6에 편집되었지만 시추조사와 연계시켜 이용하는 것이 편리하다. (중략)