• Title/Summary/Keyword: 습식-건식법

Search Result 76, Processing Time 0.025 seconds

효소저해법을 이용한 Carbamate계 농약의 간편한 잔류분석법

  • 김정호;조동현;박문기;문영수
    • Proceedings of the Korean Environmental Sciences Society Conference
    • /
    • 2004.05a
    • /
    • pp.271-273
    • /
    • 2004
  • Enzyme inhibition기술을 이용한 습식 및 건식 kit는 carbmate계 농약의 잔류를 검출하는데 매우 민감하므로, carbmate계 잔류농약을 신속하게 검색할 수 있다. 즉 AChE효소를 이용한 습식 및 건식 kit로 carbamate계 농약을 검출 할 수 있다. 따라서 빠르고 간편하게 carbamate계 농약을 검출하기 위한 습식 kit 및 건식 kit로 상업화 할 수 있다.

  • PDF

Enhancement of Lowsintering Temperature and Electromagnetic Properties of (NiCuZn)-Ferrites for Multilayer Chip Inductor by Using Ultra-fine Powders (초미세 분말합성에 의한 칩인덕터용 (NiCuZn)-Ferrites의 저온소결 및 전자기적 특성 향상)

  • 허은광;강영조;김정식
    • Journal of the Microelectronics and Packaging Society
    • /
    • v.9 no.4
    • /
    • pp.47-53
    • /
    • 2002
  • In this study, two different (NiCuZn)-ferrite which were fabricated by using ultra-fine powders synthesized by the wet processing and conventionally commercialized powder, were investigated and compared each other in terms of the low temperature sintering and electromagnetic properties. Composition of x and w in $(Ni_{0.4-x}Cu_xZn_{0.6})_{1+w}(Fe_2O_4)_{1-w}$ were controlled as 0.2 and 0.03, respectively. The sintering temperature were $900^{\circ}C$ for ultra-fine powders by way of initial heat treatment and $1150^{\circ}C$ for commercialized powders. The (NiCuZn)-ferrite by ultra-fine powders showed love. sintering temperature than that of commercialized powders by over $200^{\circ}C$, and excellent electromagnetic properties such as the quality factor which is a important factor in the multi-layered chip inductor. In addition, characteristics of B-H hysteresis, crystallinity, microstructure and powder morphology were analyzed by a vibrating sample method(VSM), x-ray diffractometer(XRD), transmission electron microscope (TEM) and scanning electron microscope(SEM).

  • PDF

Effects of Silane-treated Silica on the Cure Temperature and Mechanical Properties of Elastomeric Epoxy (실란 커플링제로 처리된 실리카가 탄성에폭시의 경화온도 및 기계적 물성에 미치는 영향)

  • Choi, Sun-Mi;Lee, Eun-Kyoung;Choi, Seo-Young
    • Elastomers and Composites
    • /
    • v.43 no.3
    • /
    • pp.147-156
    • /
    • 2008
  • In this work, epoxy/carboxyl-terminated butadiene acrylonitirile (EP/CTBN) composites were prepared by employing a reinforcing filler, silica treated with silane coupling agent in different ratio by dry and wet method. Their curing characteristics, surface free energy, interface morphologies and mechanical properties such as tensile strength and impact resistance were carefully investigated. Differential scanning calorimetry(DSC) results showed that curing temperature was lowered with the increase of silane coupling agent because of the increase of relative curing agent cotent by filling the pores of silica. Wet method was proved to be more effective for lowering curing temperature of EP/CTBN composite. In general, surface free energy and impact resistance were increased with the increase of silane coupling agent in this work. Tensile strength, however, was observed to be decreased at 4 wt% of silane coupling agent. It was found that the dry method was proved to be preferable for pretreatment of silica with coupling agent.

RF-Plasma를 이용한 Ru-Cr 금속합금 분말 제조 및 특성

  • Ho, Jong-Hwan;Im, Seong-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2013.05a
    • /
    • pp.211-211
    • /
    • 2013
  • Ru-Cr은 차세대 반도체 메모리(RAM, MRAM, FeRAM), 헤드(MR, TMR), 캐피시터의 웨이퍼 등에 전극층이나 시드층 형성을 위해 스퍼터링 타겟으로 제조되며, IT산업이 발달함에 따라 수요가 증가하고 있다. 기존의 스퍼터링 타겟은 산처리와 주조와 같은 습식법이 주를 이루었으나, 긴 제조시간과 강산사용의 위험성화 강산폐유의 처리가 문제되고 있다. 최근에는 습식공정을 보완하기 위한 건식법의 연구가 진행 중이며, 합금소재에 대한 건식법의 연구가 필요하다. 본 연구에서는 폐 Ru-Cr 금속합금 스퍼터링 타겟을 Hammer-mill, jet-mill 등 건식으로 분쇄하고 RF-Plasma를 이용하여 소결에 용이한 구형, 고순도 Ru-Cr금속합금분말을 제조하였다.

  • PDF

Comparison of Particle Size Analysis and Distribution of Heavy Metals in River and Lake Sediments (하천 및 호소 퇴적물 입도분석 방식의 비교와 입도에 따른 중금속물질의 분포경향)

  • Oh, Hyungsuk;Shin, Wonsik;Kim, Joonha;Hwang, Inseong;Hur, Jin;Shin, Hyunsang;Oh, Jeongeun;Huh, Inae;Kim, Younghun
    • Journal of the Korean GEO-environmental Society
    • /
    • v.11 no.5
    • /
    • pp.15-23
    • /
    • 2010
  • Dry sieving, wet sieving and photoscattering analyzer were tested as particle size analyzing methods for sediments from rivers and lakes of Han river, Nakdong river, Youngsan river, and Kumgang river area. Dry sieving showed a big error due to coagulating effect over drying process and this phenomena was severe for lake sediment. Wet sieving and PSA showed an accurate results though wet sieving needs more labor and complicate processes. Freeze-dry or freeze-dry after oxidation of organics with hydrogen peroxide showed improved results but gave lower portion of fine particles in comparing with wet sieving. Heavy metal contents and extractable metal contents were investigated for the sediments and high heavy metal content and extractable amount were obtained from fine particles as expected. Using of proper particle size analyzing method is important and the sediment management should be focused on the fine particles.

The manufacture of Nd:glass by Using the sol-gel process (Sol-Gel 법을 이용한 Nd:glass의 제조)

  • Choi, Cheol-Ho;Kim, Jeong-Ho;Park, Yong-Pil
    • Proceedings of the KIEE Conference
    • /
    • 2003.10a
    • /
    • pp.140-141
    • /
    • 2003
  • 졸겔법은 건식공정에서 습식공정으로 마이크로 단위에서 나노 단위로의 전환을 의미하는 정밀세라믹스의 제조공정에 새로운 개념으로서 세라믹스의 초기 제조공정에 표면이나 계면을 조절함으로써 재료내에 이들로 인해 발생하는 불균질을 제거하여 우수한 물성의 세라믹스를 얻고자 하는 것이다. 본 논문에서는 고출력 레이저 발진용 매질로 각광받고 있는 Nd:glass를 기존의 건식공정인 용융법대신 습식공정인 sol-gel process를 이용하여 제조하고자 연구하였다.

  • PDF

Influence of Silane Coupling Agent Treatments on Physical Properties of Rubbery Materials (실란 커플링제 처리방법이 고무 물성에 미치는 영향)

  • Woon, Jin-Bok
    • Elastomers and Composites
    • /
    • v.36 no.4
    • /
    • pp.237-245
    • /
    • 2001
  • A study was made on the chemical treatment of silica and silane coupling agents, bistriethox ysilylpropyltetrasulfide(Si 69) and ${\gamma}$-mercaptopropyltrimethoxy silane (MPS) for reinforcement of silica formulation. The effects of chemical treatment method and the most popular two coupling agents were examined. The results clearly indicate that the wet method, coupling agent is combined chemically with the silica prior to mixing, has more dispersion, wetting ability, dynamic properties and stability than the dry method, coupling agent is premixed directly with the silica. The mixing was done using a bench-type kneader having two mixing cam and a two-roll mill, under approximately similar conditions. The physical properties of SBR vulcanizates give rise to marked improvements by addition of Si 69 and MPS in comparison with without silane coupling agents. The optimum amount of Si 69 and MPS was 2 w/w% by experiments in the dry method but was 4 w/w% by EA and TGA analysis in the wet method.

  • PDF

Preparation Method for Atomic Absorption Spectrophotometry of Food Samples -Comparison of Dry, Wet and Aqua-regia Methods- (원자흡광분석(原子吸光分析)을 위한 식품시료(食品試料) 전처리방법(前處理方法) -왕수액(王水液) 처리법(處理法)과 건식(乾式) 및 습식분해법과(濕式分解法)의 비교(比較)-)

  • Woo, Soon-Ja;Ryoo, Si-Saeng
    • Korean Journal of Food Science and Technology
    • /
    • v.15 no.3
    • /
    • pp.225-230
    • /
    • 1983
  • Aqua-regia method is reported for simultaneous determination of potassium, sodium, calcium, magnesium, zinc, manganese, copper and iron in high-fat fish tissue. Samples are digested with conc nitric and conc hydrochloric acid in a volumetric flask. After digestion, aqua-regia extracts of samples are analyzed by direct flame atomic absorption spectrophotometry. The aqua-regia method is compared with dry ashing method and $H_{2}SO_{4}-HNO_{3}$ method. For quantiative determination of calcium, magnesium and zinc, the aqua-regia method and dry ashing method are superior to $H_{2}SO_{4}-HNO_{3}$ method. In case of the other elements-potassium, sodium, manganese, copper and iron-the three methods gave the similar results. Because samples can be processed by aqua-regia method easily, rapidily, cheaply and safely, aqua-regia method is suitable for the routine preparation of a large number of samples simultaneously.

  • PDF

초음파를 응용한 유리섬유의 분산

  • 심현주;홍경아
    • Proceedings of the Korean Fiber Society Conference
    • /
    • 1998.10a
    • /
    • pp.344-347
    • /
    • 1998
  • 유리섬유는 내열성, 절연성이 우수하고 고강도, 저신도이며 특히 고온에서 형태안정성이 우수하여 내열자재, 전자제품용 panel등에 널리 사용되고 있다. 유리섬유를 이용한 부직포 제조는 건식법보다는 수중에서 웹형성을 이루는 습식법이 주로 사용되어지고 있다. 그러나 유리섬유는 수중에서 섬유분산이 양호하지 못하고 수중에서 섬유가 축적되어 뭉치는 현상을 나타낸다. (중략)

  • PDF

A Circulating Fluidized Bed Scrubbing Technology for Dry Removal of the SOx and NOx of Coal Combustion Gases (석탄연소가스내의 SOx/NOx 동시처리를 위한 순환유동식 건식세정기술)

  • 이상권;조경민
    • Proceedings of the Korea Society for Energy Engineering kosee Conference
    • /
    • 1999.05a
    • /
    • pp.69-74
    • /
    • 1999
  • 각종 산업체의 공정에서 혹은 석탄 혹은 석유를 사용하는 화력발전설비에서 다량 발생되는 질소산화물(NOx), 황산화물(SOx)의 배출규제가 점점 강화되어 감에 따라 배출량 절감이 절실히 요구된다. 기존의 배기가스 정화장치는 처리대상에 따라 다양한 방법들이 사용되는데 황산화물의 경우 습식, 반건식, 건식세정법에 의해, 질소산화물은 선택적 촉매환원법(Selective Catalytic Reduction)과 선택적 무촉매환원법(Selective Non Catalytic Reduction)이 널리 이용되고 있다.(중략)

  • PDF