• Title/Summary/Keyword: 상대불확도

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Construction and Measurement of Normal Spectral Emissivity Device using Fourier Transform Infrared Spectrometer (퓨리에 변환 적외선 분광기를 이용한 수직 분광 복사율 측정 장치의 제작과 측정)

  • Jeon, Sang-Ho;Yoo, Nam-Joon;Jo, Jae-Heung;Park, Chul-Woung;Park, Seung-Nam;Lee, Geun-Woo
    • Korean Journal of Optics and Photonics
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    • v.19 no.6
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    • pp.400-407
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    • 2008
  • An Instrument to measure normal spectral emissivity is built using a Fourier Transform-Infrared (FT-IR) spectrometer. The instrument is composed of four main parts, reference blackbody, sample furnace, optics system, and FT-IR spectrometer. Measurement ranges of temperature and wavelength are $200^{\circ}C{\sim}500^{\circ}C$ and $3.5{\mu}m{\sim}20{\mu}m$, respectively. Measured emissivity of the reference blackbody is greater than 0.9993 with combined relative uncertainty less than 0.69%, which can be considered an ideal blackbody. We studied the emissivity of opaque alumina, graphite, anodized aluminum, and steel (IMS 200). It is shown that emissivity increases with the roughness of the steel (IMS 200) surface.

Comparative Analysis of ADCP Flow Measurement According to River Bed Material (하상재료에 따른 ADCP의 유량측정 비교 분석)

  • Choi, Jin-Woo;Hong, Chang-Su;Shin, Kyung-Yong;Lee, Jin Uk;Kim, Jeong-ae;Cho, Yong-Chul;Yu, Soon-Ju
    • Ecology and Resilient Infrastructure
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    • v.5 no.3
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    • pp.156-162
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    • 2018
  • This research aimed at analyzing comparison results between in gravel and sand bed with respect to the detailed Acoustic Doppler Current Profiler (ADCP) measurement in a velocity, depth, and flow rate data based on Acoustic Doppler Velocimeter (ADV) measurement result. Conclusionally, similar results were shown for gravel and sand bed in velocity, depth and flow rate data using ADV and ADCP measurement. The results of the flow rate show a relative error mean of 3.5 - 4.8% in the gravel bed and 0.02 - 3.2% in the sand bed, which is better performance than the mean error of 5% suggested by United States Geological Survey (USGS). The results can be used as a basis data for the measurement of ADCP and potentially able to be utilized for the more detailed uncertainty analysis of ADCP flow rate measurement.

Comparison of Characteristics and Dispersion of Fasting Blood Glucose Data by Administrative Districts and Gender Difference Using the 2017 'Korean Blood Glucose Reference Standard' (2017 '한국인 혈당 참조표준'을 이용한 행정구역별 남녀별 공복 혈당 데이터의 특성 및 산포성 비교)

  • Kwon, Young-Il
    • Korean Journal of Clinical Laboratory Science
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    • v.52 no.1
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    • pp.28-35
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    • 2020
  • This study aimed to investigate the differences in the upper and lower limits of the 95% distribution of fasting blood glucose (FBG) by age groups. We also analyzed the changes in the mean values and dispersion of the data using the Korean Blood Glucose Reference Standard raw data published by the National Health Insurance Service (NHIS). Furthermore, the trends among 16 administrative districts were analyzed and any gender differences were determined. We also assessed whether the study results correlated with the relative standard uncertainty, as published by the NHIS. On the dispersion analysis using the differences between the upper and lower limits of the 95% distribution of FBG by age group, there were significant differences across gender and administrative districts (P<0.05). The gender differences in FBG measurements, as published by the NHIS, were significant across different administrative districts and age groups (P<0.001). This confirmed the need to recalculate the blood glucose reference standards for men and women. No significant correlation was observed between the relative standard uncertainty, as published by NHIS, and the dispersion and number of measurements analyzed in this study. However, it showed a high correlation with the measured mean value (R2=0.95). Therefore, further research on the reference standard and uncertainty is needed.

Development of Primary Reference Gas Mixtures for Liquid Propane (혼합 액체 프로판 표준가스 개발)

  • Jeong, Yun-sung;Kim, Jin-seog;Bae, Hyun-kil;Kang, Ji-hwan;Lee, Seung-ho;Kim, Yong-doo
    • Journal of the Korean Institute of Gas
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    • v.25 no.4
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    • pp.49-56
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    • 2021
  • Liquefied Petroleum Gas is divided into liquefied gases containing propane (C3H8) and butane (C4H10). The quality of LPG varies greatly depending on the composition of the mixture, so it is important to measure the composition accurately. It is difficult to determine the composition of the mixture because liquid and gas coexist at room temperature. Therefore, the uncertainty in determining the concentration of hydrocarbons by component is high, and there are many problems that differ from the actual content standard. Therefore, it is necessary to develop a mixed liquid propane standard gas for the composition and accurate concentration of hydrocarbon substances. Mixed liquid propane standard gas is manufactured into bellows-type constant-pressure cylinders by ISO-6142 (2015). The homogeneity of the four standard gases manufactured was confirmed to be GC-FID. The manufacturer's uncertainty of expansion was 0.01 % to 0.30 % and homogeneity was 0.03 % to 0.25 %. In this mixed liquid propane standard gas, the relative expansion uncertainty of weight method, manufacturing consistency, cylinder adsorption and long-term stability was developed within 0.26 %-1.3 9% (95% of confidence level, k=2).

Development of Carbon Emission Factors and Biomass Allometric Equations for Metasequoia glyptostroboides and Platanus occidentalis in Urban Forests (정주지의 메타세쿼이아와 양버즘나무의 탄소 배출 계수 및 바이오매스 상대생장식 개발)

  • Jun-Young Jung;Subin Im;Hyun-Jun Kim;Kye-Han Lee
    • Journal of Korean Society of Forest Science
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    • v.112 no.2
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    • pp.127-135
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    • 2023
  • This study aimed to develop biomass allometric equations and estimate carbon emission factors, such as the wood density, biomass-expansion factor, and root-to-shoot ratio, for Platanus occidentalis and Metasequoia glyptostroboides planted in urban areas. Twenty M. glyptostroboides and 25 P. occidentalis trees were harvested, and the dry weights and stem volumes of stems, branches, leaves, and roots (>5 mm) were measured. The wood densities of M. glyptostroboides and P. occidentalis were 0.293 ± 0.008 g cm-3 and 0.509 ± 0.018 g cm-3, and the biomass-expansion factors were 1.738 ± 0.031 and 1.561 ± 0.035. The root-to-shoot ratios were 0.446 ± 0.009 and 0.402 ± 0.012. The uncertainty tests (coefficient of variation, %) gave 2.8% and 3.5% values for wood density, 1.8% and 2.3% for biomass-expansion factor, and 2.1% and 2.9% for root-to-shoot ratio, respectively. Among the developed allometric equations, Model I using the diameter at breast height (DBH) was suitable. The allometric equations of M. glyptostroboides and P. occidentalis above ground were y = 1.679 (DBH)1.315 and y = 0.505 (DBH)1.896, and the allometric equations of the root and total were y = 0.746 (DBH)1.315, y = 0.301 (DBH)1.751, y = 2.422 (DBH)1.316, and y = 0.787 (DBH)1.858. If the carbon-emission factors of this study and biomass allometric equations of the three developed models are used to estimate the carbon storage and biomass of urban forests, errors caused by not considering the use of fixed factors and the environmental differences can be reduced.

The Sensitivity Analyses of Initial Condition and Data Assimilation for a Fog Event using the Mesoscale Meteorological Model (중규모 기상 모델을 이용한 안개 사례의 초기장 및 자료동화 민감도 분석)

  • Kang, Misun;Lim, Yun-Kyu;Cho, Changbum;Kim, Kyu Rang;Park, Jun Sang;Kim, Baek-Jo
    • Journal of the Korean earth science society
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    • v.36 no.6
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    • pp.567-579
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    • 2015
  • The accurate simulation of micro-scale weather phenomena such as fog using the mesoscale meteorological models is a very complex task. Especially, the uncertainty arisen from initial input data of the numerical models has a decisive effect on the accuracy of numerical models. The data assimilation is required to reduce the uncertainty of initial input data. In this study, the limitation of the mesoscale meteorological model was verified by WRF (Weather Research and Forecasting) model for a summer fog event around the Nakdong river in Korea. The sensitivity analyses of simulation accuracy from the numerical model were conducted using two different initial and boundary conditions: KLAPS (Korea Local Analysis and Prediction System) and LDAPS (Local Data Assimilation and Prediction System) data. In addition, the improvement of numerical model performance by FDDA (Four-Dimensional Data Assimilation) using the observational data from AWS (Automatic Weather System) was investigated. The result of sensitivity analysis showed that the accuracy of simulated air temperature, dew point temperature, and relative humidity with LDAPS data was higher than those of KLAPS, but the accuracy of the wind speed of LDAPS was lower than that of KLAPS. Significant difference was found in case of relative humidity where RMSE (Root Mean Square Error) for LDAPS and KLAPS was 15.7 and 35.6%, respectively. The RMSE for air temperature, wind speed, and relative humidity was improved by approximately $0.3^{\circ}C$, $0.2m\;s^{-1}$, and 2.2%, respectively after incorporating the FDDA.

Comparison and Optimization of Flux Chamber Methods of Methane Emissions from Landfill Surface Area (매립지 표면의 메탄 발산량 실측을 위한 플럭스 챔버의 방법론적 비교와 최적화)

  • Jeong, Jin Hee;Kang, Su Ji;Lim, Jong Myoung;Lee, Jin-Hong
    • Journal of Korean Society of Environmental Engineers
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    • v.38 no.10
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    • pp.535-542
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    • 2016
  • As one of the most cost-effective methods for surface emission measurements, flux chamber method has been used worldwide. It can be classified into two types: SFC (with slope method) and DFC (with steady-state method). SFC (static flux chamber) type needs only simple equipment and is easy to handle. However, the value of flux might vary with SFC method, because it assumes that the change of concentration in chamber is linear with time. Although more specific equipments are required for DFC (dynamic flux chamber) method, it can lead to a constant result without any ambiguity. We made a self-designed DFC using a small and compact kit, which recorded good sample homogeneity (RSD < 5%) and recovery ( > 90%). Relative expanded measurement uncertainty of this improved DFC method was 7.37%, which mainly came from uncontrolled sweep air. The study shows that the improved DFC method can be used to collect highly reliable emission data from large landfill area.

Development of 10 μmol/mol Hydrogen Sulfide Primary Standard Gas for Odor Measurements (악취측정용 10 μmol/mol 황화수소 표준가스 개발)

  • Kim, Yong-Doo;Bae, Hyun-Kil;Kim, Dalho;Oh, Sang-Hyub;Lee, Jin Hong;Lee, Sangil
    • Journal of the Korean Institute of Gas
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    • v.22 no.2
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    • pp.46-51
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    • 2018
  • Hydrogen sulfide from landfill and sewage treatment plant is a major odor component and causes many civil petitions. Rapidly developing industries release hydrogen sulfide, an odorous gas, to the atmosphere. This study aims to develop a $10{\mu}mol/mol$ concentration level hydrogen sulfide primary standard gas for odor measurement. The hydrogen sulfide gas was prepared at a nominal concentration of $10{\mu}mol/mol$ in nitrogen using the gravimetric method described in ISO 6142. Replicate standard gases were produced in 4 aluminium cylinders, and their concentrations were verified by GC-AED. The uncertainty of production was less than 0.50 %, and the variation of the 4 replicates was 0.22 %. The wall adsorption of hydrogen sulfide in cylinders was 0.10 % at 1500 psi, and the concentration was estimated to be long-term stable for one year. The relative expanded uncertainty of the preparation consistency, adsorption and long-term stability of this hydrogen sulfide standard gas was less than 1.05 % (95 % of confidence level, k=2).

Evaluation of the proficiency testing results using river water-based reference materials for heavy metal analysis (중금속분석용 하천수 매질표준물질을 이용한 숙련도 결과 평가)

  • Song, Ko-Bong;Kim, Young-Hee;Shin, Sun-Kyoung;Lee, Su-Yeong;Kim, Hyun-Jung;Kang, Hak-Gu;Kim, Il-Gyu;An, Hee-Ju
    • Analytical Science and Technology
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    • v.23 no.3
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    • pp.284-294
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    • 2010
  • In this study, river water-based reference materials (RMs), NIER-I08RW and NIER-I09, for trace metal analysis were prepared and certified for Pb, Cd, Cr and Cu with evaluation of uncertainties. The RMs were confirmed to be homogeneous enough to be used as proficiency testing materials since within-bottle homogenieties of the RMs were lower than 0.3 times of targeted standard deviation of proficiency testing. The RMs were distributed to environmental testing laboratories for the proficiency testing and the variation of Z scores of the proficiency testing results were compared for different assigned values. The relative bias, $B_{relative}$, deviations between reference values and consensus values, were lower than ${\pm}$1 except for cadmium of NIERI08RW. The results showed both values were in a good agreement and only 2.9% of Z scores changed by using a different assigned values such as consensus and reference values.

Preparation and characterization of the primary gas standards for isoprene (아이소프렌 일차표준가스의 제조 및 특성 평가)

  • Kim, Taesu;Kang, Chul-Ho;Kim, Yong Doo;Lee, Seungho;Kim, Dalho
    • Analytical Science and Technology
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    • v.27 no.6
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    • pp.357-363
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    • 2014
  • Isoprene is a one of the biogenic volatile organic compounds (BVOCs) and it is known as a source of the tropospheric ozone and formaldehyde. In addition, isoprene is a trace component of the exhaled breath and it is a potential biomarker for the diagnosis of diseases such as lung cancer. In these regards, isoprene gas standards are required for the accurate measurement of isoprene in air samples. To establish a standard for isoprene gas, gravimetric preparation and characterization of primary gas standards were studied. The primary gas standards were produced independently in 4 aluminum cylinders and concentrations were examined by GC-FID. As a result, the uncertainty of the gravimetric preparations including purity of the raw material was 0.01% and reproducibility of the preparation of independent 4 cylinders was 0.08%. The primary gas standards for isoprene showed 14 months of long-term stability. The relative expended uncertainty of 2.8% (95% of confidence level, k=1.96) was assigned to the certified value of 10 ${\mu}mol$/mol level of isoprene based on the quantitative evaluation of the purity, weighing, reproducibility, adsorption and long-term stability.