• Journal of the Korean Applied Science and Technology
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• v.23 no.1
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• pp.92-97
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• 2006

In this paper, magenta coupler was prepared by the reaction of 1-(2,4,6-Trichlorophenyl)-3-(5-amino-2-chloroanilino)-5-pyrazolone with 2,4-di-tert-pentyl-phenoxy butanoyl chloride in the presence of pyridine. The product was identified by using various analytical tools such as melting point, elemental analyzer, IR spectrophotometer, UV-Vis spectrophotometer and GC-mass spectrometer. The reaction of magenta coupler with CD-3 (color development agent) was shown magenta color.

• Journal of the Korean Applied Science and Technology
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• v.24 no.2
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• pp.205-210
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• 2007

In this paper, we describe a study on the relationship between neutral emulsion manufacture and hardening test of films. The hardeners were prepared by condensation of equimolar amounts of trichlorotriazine with benzene- or naphthalene-based amino or oxy acids at 0 to $5^{\circ}C$ and at pH 7, and used as hardening agents for gelatin. The hardening test of neutral emulsion layers was studied at pH 7.0. For example I(R=ONa) had strong hardening properties, I substituted with an aminobenzosulfonate moiety $(R=NHC_6H_4-p-SO_3Me$ where Me = K, Na) was a much weaker gelatin hardener, and when substituted with amino- or oxynaphthalene derivative (II, III) did not harden gelatin at all. Compound with 2 dichlorotriazine groups as IV exhibited hardening properties. The hardener can be used in neutral emulsion layer of film and showed good hardening effect.

• Journal of the Korean Applied Science and Technology
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• v.23 no.2
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• pp.125-129
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• 2006

Benzoxazolo carbocyanine compounds were synthesized by condensation of a suitable ortho-ester with an appropriately substituted 2-methylbenzoxazole in the presence of triethylamine. This compounds used as green sensitizing dyes in photographic emulsions. The compounds are characterized by fast atom bombardment mass spectrometry. The values(m/z) of structurally significant ions observed in FAB spectra. It was showed tentative fragmentation pattern in FAB spectroscopy of $HN(C_2H_5)_3$ cations in glycerol/trifluoroacetic acid matrix.

• Journal of the Korean Applied Science and Technology
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• v.28 no.4
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• pp.449-454
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• 2011

This surfactant can be used as a cosmetics and chemical dispersants. The variation of critical micelle concentration(CMC) with temperature for N-eicosyl pyridinium bromide over the range $40^{\circ}C$ to $60^{\circ}C$ has been measured by drop methods. Thermodynamic quantities for micellization of N-eicosyl pyridinium bromide in water have been calculated by polynominal equation.

• Environmental Analysis Health and Toxicology
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• v.8 no.1_2
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• pp.1-10
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• 1993

This study was done to determine the toxic effect of fthalide in rats which have oral administration at levels of 100 mg/kg/day for twelve days. It was examined the hematogram and serological parameters, and also the content of cytochrome P-450, the activity of NADPH-cytochrome c reductase, glucose-6-phosphatase, cholinesterase and carboxylesterase in liver. Any significant alteration of hematogram was not found but the value of AST, LDH and content of glucose in serum were statistically increased. The content of cytochrome P-450, the activty of NADPH-cytochrome c reductase were increased but glucose-6-phosphatase were slightly decreased compare with that of control group. The activity of cholinesterase was decreased slightly and on the contrary the activity of carboxylesterase was found to be the tendeny of increase in both of liver and serum.

• Proceedings of the KIEE Conference
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• 1998.11c
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• pp.898-900
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• 1998

This paper describes the motion characteristics and micro-discharge of the free conducting particles between plain electrodes under alternating voltage. The particles move between both electrodes due to electrostatic force by applied AC voltage. Various types and sizes of free conducting particles were used to study the motion and micro-discharge characteristics. The micro-discharge and breakdown were observed during the particle motion.

• Journal of Korean Society of Transportation
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• v.15 no.3
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• pp.53-74
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• 1997

신호연동화모형에서 통과폭모형은 지체를 최소화하지 못하고 지체도모형은 좌회전현시순서를 최적화하지 못한다. 이러한 모형의 단점을 극복하고자 개발된 KS_SIGNAL은 지체를 최소화하는 신호연동화모형이지만 지체를 산정하는데 있어 많은 한계를 갖고 있다. 본 연구에서는 기존에 개발된 KS_SIGNAL의 지체모형을 개선하여 보다 우수한 연동신호시간과 현시순서를 산정해주는 신호최적화모형(KS_SIGNAL II)을 개발하여 FORTRAN 언어로 전산화하였다. 개발된 모형은 다양한 평가를 통하여 기존 모형들보다 전반적으로 우수한 것으로 입증되었다. 본 모형을 통하여 차량 출발 및 도착형태에 따른 대기차량 소거시간을 고려하는 옵셋 산정이 가능해져 지체를 최소화하는 간선도로의 신호최적화모형으로 활용될 경우 도로기능제고 및 지체도 감소에 의한 편익을 얻을 수 있다.

• Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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• 2003.04a
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• pp.111.1-111
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• 2003

삼백초 지상부의 에탄올 추출농도와 추출 시간에 따른 수율, total phenol과 total flavonoid함량, DPPH 라디칼 소거능을 조사하였다. 추출 온도 9$0^{\circ}C$에서 에탄올농도를 증가시키면서 8시간동안 환류추출하였다. 추출수율과 DPPH 라디칼 소거능은 에탄올농도 40%까지는 증가하다가 60%이상에서는 감소하였고 total phenolic compound와 total flavonoid의 함량도 비슷한 경향을 보였다. total phenolic compound의 함량은 40%와 60%에서 큰 차이가 없는 반면 total flavonoid의 함량은 40%에서 더 높았다. total phenolic compound와 total flavonoid 함량, DPPH 라디칼 소거능 및 추출수율은 40% 이상에서는 큰 변화가 없어 추출용매의 조건은 40% 에탄올로 선정하였다. 40% 에탄올로 9$0^{\circ}C$에서 24시간 동안 4시간 간격으로 환류추출하였을 때 total phenolic compound와 total flavonoid 함량, DPPH 라디칼 소거능 및 추출수율은 4시간 이후 큰 차이가 없었다. 삼백초의 용매추출조건으로는 40% 에탄올, 4시간 추출하는 것이 적합하다고 판정된다.

• Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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• 2003.04a
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• pp.110.2-111
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• 2003

삼백초 지상부를 탈지후 60% acetone으로 추출하고 이를 극성에 따라 diethyl ether, ethyl acetate, aqueous fraction과 같이 용매분획하였다. 각 fraction의 superoxide anion, hydrogen peroxide, hydroxyl radical, DPPH radical 에 대한 소거활성을 측정하였다. Diethyl ether fraction의 ROS 소거효과가 비교적 강하였으며 superoxide anion 소거활성은 100ppm에서 86.88%였고, hydroxyl radical 소거활성은 1ppm에서 85.3%로 나타났다. Hydrogen peroxide, DPPH radical 소거활성은 ethyl acetate fraction이 강하게 나타났다. Diethyl ether fraction으로부터 silica gel column chromatography, sephadex LH-20 column chromatography, preparative HPLC에 의하여 수 종의 성분을 분리하였으며 현재 구조동정과 이들의 LDL산화억제 효과 시험 중에 있다.

• The KSFM Journal of Fluid Machinery
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• v.3 no.3 s.8
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• pp.19-24
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• 2000

It is well known that the finite element analysis often has an inaccuracy when it is in conflict with test results. Model updating is concerned with the correction of analytical model by processing records of response from test results. The famous one of the model updating methods is FRF sensitivity method. However, it has demerit that the solution is not unique. So, the neural network is recommended when an unique and exact solution is desired. The generalization ability of radial basis function neural network is used in model updating. As an application model, a cantilever and a rotor system are used. Specially the machined clearance($C_p$) of a journal bearing is updated.