• Korean Journal of Food Science and Technology
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• v.27 no.5
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• pp.680-689
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• 1995

Rice based infant foods of carrot, of beef, and of egg for 4-6 month old infants were prepared using freeze drying (FD) process. The optimum moisture content prior to FD and the plate temperature in the drier were determined with the use of response surface methodology. For all the infant foods under this study, FD time was longer as the initial moisture content was higher and the plate temperature was lower. Brittleness of the dried infant foods increased as the moisture content decreased and the plate temperature increased. Among the sensory attributes, hydration rate, uniformity, and smoothness were greater with increased moisture content and with decreased plate temperature. Ease to spoon increased as moisture content increased and mouthcoating increased as both the moisture content and the plate temperature increased. Optimum moisture content and plate temperature for the FD of carrot, beef and egg foods were 88.5% and $34^{\circ}C$, 88.5% and $28^{\circ}C$, and 87.3% and $39^{\circ}C$, respectively.

• Polymer(Korea)
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• v.24 no.1
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• pp.105-112
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• 2000

Using a commercial epoxy/carbon fiber composite prepreg (DMS 2224) as a model system, the cure kinetics of vitrifying thermoset system were analyzed by isothermal and dynamic-heating experiments. Focusing on the processing condition of high performance composite systems, a phenomenological kinetic model was developed by using differential scanning calorimetry (DSC) and reaction kinetics theories. The model system exhibited a limited degree of cure as a function of isothermal temperature seemingly due to the diffusion-controlled reaction rates. The diffusion-controlled cure reaction was incorporated in the development of the kinetic model, and the model parameters were determined from isothermal experiments. The first order reaction was confirmed from the characteristic shape of isothermal cure thermograms, and the activation energy wes 78.43 kJ/mol. Finally, the proposed model was used to predict a complex autoclave thermal condition, which was composed of several isothermal and dynamic-heating stages.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2018.06a
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• pp.113-113
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• 2018

환경 친화형 전기자동차, 하이브리드 자동차, 전철 등에서는 고내압 및 소형으로 전력손실을 감소시킬 수 있는 파워 디바이스가 필수이다. 최근, 실리콘 카바이드(SiC, silcon carbide)는 기존 실리콘(Si)보다 스위칭 손실의 저감 및 고온환경에서의 동작 특성이 우수하여, 차세대 저 손실 전력반도체 재료로서 기대를 받고 있다. 용액 성장 법에서 고품질 SiC 결정을 만들 수 있다. 그러나 늦은 성장 속도 때문에 SiC의 양산을 어렵게 하고 있다. 현재까지 성장 속도 향상을 위한 Si용매에 Cr을 첨가하여 탄소 용해도를 높이는 방법이 사용되고 안정된 성장을 위한 Si-Cr용매에 Al를 첨가하는 등 다양한 금속을 첨가하는 방법이 이용되고 있다. 선행 연구에서는 다양한 용매인 탄소 용해도를 실측하고 특히 큰 탄소 용해도를 보인 것은 Co이었다. 본 연구에서는 $Si_{0.6}Cr_{0.4}$원료와 Co를 첨가한 $Si_{0.56}Cr_{0.4}Co_{0.04}$의 용매에 의한 SiC용액 성장을 실시하고 결정 성장 속도 및 표면 상태의 변화를 검토했다. on-axis 4H-SiC(000-1)을 사용한 Top-seeded solution growth(TSSG)법과 원자 비율로 $Si_{0.6}Cr_{0.4}$와 $Si_{0.56}Cr_{0.4}Co_{0.04}$의 용매를 이용하여 SiC 용액 성장을 실시했다. Ar가스에서 저항 가열로 내를 치환 후에 $1800^{\circ}C$까지 가열하고 종자화 후에 120분간 유지하고 결정 성장을 실시했다. 냉각 후에 성장의 표면에 남은 용매를 $HF+HNO_3$에서 제거했다. 광학 현미경을 이용하여 결정면과 두께를 관찰 측정했다. Co를 첨가한 $Si_{0.56}Cr_{0.4}Co_{0.04}$의 경우는 $Si_{0.6}Cr_{0.4}$의 경우보다 결정 성장 속도가 향상됐다. 또한 $Si_{0.6}Cr_{0.4}$보다 step-flow의 성장을 나타낸 결정의 표면이 전반적으로 관찰됐으며 안정된 결정성장을 나타냈다. 본 연구에서 실시한 연구 방법과 결과는 고품질 및 고속의 SiC 용액성장을 위한 매우 유용한 자료로 활용 될 수 있을 것으로 판단한다.

• Proceedings of the Korean Radioactive Waste Society Conference
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• 2010.05a
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• pp.401-402
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• 2010

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.11a
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• pp.239-239
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• 2003

탄소재료의 산화반응을 설명한 대부분의 논문은 TGA(Thermo Gravimetric Analysis)를 이용한 연구이다. TGA 장치는 가열이 필요한 물질의 반응연구에 다양하게 이용되고 있는데, 온도에 대한 무게 변화를 간편하게 알 수 있다는 장점과 함께 보편적으로 편리한 Arrhenius형태의 속도식으로 해석된다. 많은 연구자들은 TGA를 이용하여 다양한 탄소재료에 대한 반응속도상수를 구하였으며, 반응기체, 반응온도 및 원료물질에 따라 다른 속도를 나타내는 실험결과를 표준화된 속도식으로 표현하고자 하는 노력이 있었다. 그러나 이런 대부분의 연구는 coal 등과 같은 탄소재료의 연소특성을 이용하려는 에너지 변환 연구가 주를 이루어 왔으며, 탄소섬유의 산화반응에 대한 표준화 식으로 해석한 보고는 거의 없는 실정이다. 이 연구에서는 내부구조가 현격하게 차이나는 다른 두 종류의 피치계 탄소섬유를 TGA를 이용하여 등온 산화반응 시켰다. 반응기체의 종류와 반응온도를 변화시켜 산화반응조건에 따른 중량변화를 관찰하였고, 여러 산화조건에서 얻어진 산화속도를 Kasaoka 등에 의해 제안된 표준화식을 이용하여 산화반응의 평균 속도상수 K와 전환율이 0.5일 때의 속도상수 $k_{f=0.5}$ 결과를 비교하여 산화 반응속도를 정량적으로 해석하고자 하였다.다.

• Korean Journal of Food Science and Technology
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• v.34 no.2
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• pp.238-243
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• 2002

The effects of concentration and temperature on degradation of anthocyanins of purple-fleshed sweet potato pigment concentrate and a Japanese plum juice were determined over temperature ranges of 60 to $90^{\circ}C$ and 5 to $60^{\circ}C$, respectively. Degradation of anthocyanins in pigment concentrates followed the first-order reaction rate. Activation energies of the pigment solutions ranged 51.29-73.02 kJ/mol, linearly decreasing as concentration increased except the pigment solution of $8.4^{\circ}Brix$ which was not concentrated after extraction. Anthocynins in Japanese plum juice was also degraded by the first-order reaction kinetics with activation energy of 75.80 kJ/mol. Storage life of the beverage was extended with decreasing storage temperature. Pigment was ratained more than 80% until 8 months storage at $5^{\circ}C$.

• Fire Science and Engineering
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• v.18 no.1
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• pp.31-36
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• 2004

The purpose of this study is to present data for the reusing, rehabilitation and estimation of safety of RC structure damaged by fire, and for the prevention of explosive spatting by investigation the properties of explosive spalling, compressive strength and ultrasonic pulse velocity according to kinds of fine aggregate, admixture and water-cement ratios. In explosive spalling properties with kinds of aggregate, explosive spalling does not appear or little at surface in the case of used sea sand, but the case of using recycled sand or crushed sand is worse and worse. Property with the kind of admixture does not appear specially. And high strength concrete with W/C 30.5% was taken spalling, but 55% does not appear. It is found that residual compressive strength after exposed at high temperature showed 45％ in W/C 55%, and 64％ in W/C 30.5％ of its original strength averagely. Ultrasonic pulse velocity is different with kinds of aggregate. W/C. and heating time. When 3 month age after heating ultrasonic pulse velocity is recovered abut 1.3％～8.4％ of its 1 month age after heating.

• Applied Chemistry for Engineering
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• v.9 no.3
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• pp.364-371
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• 1998

A theoretical model of particle agglomeration was developed to investigate the adhesive force between contiguous coal particles in CWM agglomerate. While heating bituminous coal to about $400^{\circ}C$ or above, the transient occurrence of plastic behavior of coal particles can be observed. The adhesive force in the process of agglomeration of coal particles was found to be proportional to the duration of plasticity of the particles. In the research, how the heating rate and the particle size distribution of CWM fuel influenced the formation of the agglomerate in CWM fuel at the heat-up stage was investigated by the model of particle agglomeration. Simulation program used to this experiment was RKG method and was programmed by Fortran. It was represented that by the model of particle agglomeration, the adhesive force in the process of the particle agglomeration in CWM fuel was inversely proportional to the heating rate but proportional to particle size.

• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.5
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• pp.436-442
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• 2013

Friction welding is a very useful joining process to weld metals which have axially symmetric cross section. In this paper, the feasibility of industry application was determined by analyzing the mechanical properties of weld region for a specimen of tube-to-tube shape for excavator hose nipple with friction welding, and optimized welding variables were suggested. In order to accomplish this object, friction heating pressure and friction heating time were selected as the major process variables and the experiment was performed in three levels of each parameter. An acoustic emission(AE) technique was applied to evaluate the optimal friction welding conditions nondestructively. AE parameters of accumulative count and event were analyzed in terms of generating trend of AE signals across the full range of friction weld. The typical waveform and frequency spectrum of AE signals which is generated by friction weld were discussed. From this study the optimal welding variables could be suggested as rotating speed of 1300 rpm, friction heating pressure of 15 MPa, and friction heating time of 10 sec. AE event was a useful parameter to estimate the tensile strength of tube-to tube specimen with friction weld.

• Korean Journal of Food Science and Technology
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• v.24 no.5
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• pp.463-469
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• 1992

Effect of thermal processing upon the structure formation of surimi was investigated by differential scanning calorimeter (DSC), rigidity changes during heating, and scanning electron microscopy (SEM). DSC studies showed the transition temperatures and heat capacity of the proteins during heating. Thermal transition peaks of the proteins were shifted to the lower temperatures or disappeared by the addition of salt and higher heating rate or setting treatment ($4^{\circ}C$ or $40^{\circ}C$). Whereas setting at $4^{\circ}C$ for 24hr produced elastic component and showed a permanent effect in rigidity development during heating, setting at $40^{\circ}C$ for 30 min produced a temporary effect. SEM studies in conjunction with rigidity scanning provided an insight into the structural features of the gel and helped clarify the setting and protein modification effects.