• KOREAN JOURNAL OF CROP SCIENCE
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• v.53 no.4
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• pp.359-368
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• 2008

Black soybean has been widely utilized as foods and oriental medicinal materials. The pigmentation in the seed coat of black soybean is due to accumulate anthocyanins in the epidermis palisade layer. The anthocyanins of black soybean seed coat are considered as a parameter of quality evaluation of black soybean. Therefore, the purpose of this study was to investigate the most suitable HPLC condition for simultaneous determination of anthocyanins in black soybean seed coats extracts. The efficient HPLC analytical condition of D3G, C3G, and Pt3G contained extracts of black soybean seed coats was developed. The gradient elution employed a $250\;mm\;{\times}\;4.6\;mm$ i.d. YMC-pak ODS-AM 303 column. The gradient system was used two mobile phases. A gradient elution was performed with mobile phase A, consisting of 5% aqueous formic acid, and mobile phase B, comprising 5% formic acid - acetonitrile, and delivered at a flow rate of 0.7 mL/min as follows: $0{\sim}35\;min$, $90%\;A{\sim}60%\;A$; 36 min, 90% A; 46 min, 90% A. The UV-VIS. detection wavelength was set at 520 nm. The limit of detection (LOD) for D3G, C3G, and Pt3G were under 10 ng/mL.

• Korean Chemical Engineering Research
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• v.44 no.6
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• pp.650-658
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• 2006

The recycling of TDA from solid waste of TDI plant(TDI-R) by near-critical hydrolysis reaction had been studied by means of a statistical design of experiment. The main and interaction effects of process variables had been defined from the experiments in a batch reactor and the correlation equation with process variables for TDA yield had been obtained from the experiments in a continuous pilot plant. It was confirmed that the effects of reaction temperature, catalyst type and concentration, and the weight ratio of water to TDI-R(WR) on TDA yield were significant. TDA yield decreased with increases in reaction temperature and catalyst concentration, and increased with an increase in WR. As a catalyst, NaOH was more effective than $Na_2CO_3$ for TDA yield. The interaction effects between catalyst concentration and temperature, WR and temperature, catalyst type and reaction time on TDA yield had been defined as significant. Although the effect of catalyst concentration on TDA yield at $300^{\circ}C$ as subcritical water was insignificant, the TDA yield decreased with increasing catalyst concentration at $400^{\circ}C$ as supercritical water. On the other hand, the yield increased with an increase in WR at $300^{\circ}C$ but showed negligible effect with WR at $400^{\circ}C$. The optimization of process variables for TDA yield has been explored with a pilot plant for scale-up. The catalyst concentration and WR were selected as process variables with respect to economic feasibility and efficiency. The effects of process variables on TDA yield had been explored by means of central composite design. The TDA yield increased with an increase in catalyst concentration. It showed maximum value at below 2.5 of WR and then decreased with an increase in WR. However, the ratio at which the TDA yield showed a maximum value increased with increasing catalyst concentration. The correlation equation of a quadratic model with catalyst concentration and WR had been obtained by the regression analysis of experimental results in a pilot plant.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.20 no.7
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• pp.606-610
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• 2007

This paper describes the Raman scattering characteristics of polycrystalline (poly) 3C-SiC thin films, in which they were deposited on the oxidized Si substrate by APCVD method according to growth temperature. Since the phonon modes were not measured for $0.4{\mu}m$ thick 3C-SiC, $2.0{\mu}m$ thick 3C-SiC deposited on the oxidized Si at $1180^{\circ}C$, in which TO (transverse optical mode) and LO (longitudinal optical mode) phonon modes were appeared at 794.4 and $965.7cm^{-1}$, respectively. The broad FWHM (full width half maximum) can explain that the crystallinity of 3C-SiC deposited at $1180^{\circ}C$ becomes polycrystalline instead of disorder crystal. Additionally, the ratio of intensity $I_{LO}/I_{TO}{\approx}1.0$ of 3C-SiC indicates that the crystal disorder of $3C-SiC/SiO_2/Si$ is small. Compared poly $3C-SiC/SiO_2$ with $SiO_2/Si$ interfaces, $1122.6cm^{-1}$ phonon mode was measured which may belong to C-O bonding and two phonon modes, 1355.8 and $1596.8cm^{-1}$ related to D and G bands of C-C bonding in the Raman range of 200 to $2000cm^{-1}$.

• International Journal of Aeronautical and Space Sciences
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• v.18 no.4
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• pp.614-622
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• 2017

The characteristics of aerodynamic drag for Transonic Vehicle in Evacuated Tube was investigated using computational fluid dynamics. At first, parametric study on the system was performed according to the Mach number of the vehicle's speed ($Mach_v$), evacuated pressure of the tube ($Pre_t$), and blockage ratio (BR) between the vehicle and tube via axisymmetric flow analysis; the $Mach_v$ ranged from 0.3 to 1.0. The $Pre_t$ was 100, 1,000 and 10,000 Pa and the BR was 0.1, 0.2, and 0.4. In the calculations, the aerodynamic drag of the vehicle was larger when the BR and the pressure became larger. Concerning the $Mach_v$, the drag coefficient ($C_d$) became the maximum when the $Mach_v$ was near the Kantrowitz limit and decreased, which showed the typical transonic flow pattern. Then, three dimensional flow analysis was performed by changing the $Mach_v$ from 0.3 to 1.0 and setting the BR and the $Pre_t$ as 0.34 and 100 Pa, respectively by referring the Hyperloop Alpha documentation. From the calculations, the $C_d$ from three dimensional flow simulations were somewhat larger than those of axisymmetric ones because of the eccentricity of the vehicle inside the tube. However, the pattern of $C_d$ according to the $Mach_v$ was compatible with that of axisymmetric ones.

• Structural Engineering and Mechanics
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• v.25 no.5
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• pp.565-576
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• 2007

The article describes a technique for the measurement of the level of complexity of fracture surfaces by the method of vertical sections, and a performed statistical analysis of the effect of profile lines on the fractographic and fractal parameters of fractures, i.e. the profile line development factor, $R_L$, and the fracture surface development factor, $R_S$, (as defined by the cycloid method), as well as the fractal dimension, $D_C$, (as determined by the chord method), and the fractal dimension, $D_{BC}$, (as determined by the box method). The above-mentioned parameters were determined for fracture surfaces of basalt and gravel concretes, respectively, which had previously been subjected to fracture toughness tests. The concretes were made from mixtures of a water/cement ratio ranging from 0.41 to 0.61 and with a variable fraction of coarse aggregate to fine aggregate, $C_{agg.}/F_{agg.}$, in the range from 1.5 to 3.5. Basalt and gravel aggregate of a fraction to maximum 16 mm were used to the tests. Based on the performed analysis it has been established that the necessary number of concrete fracture profile lines, which assures the reliability of obtained testing results, should amount to 12.

• Journal of the Society of Disaster Information
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• v.4 no.1
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• pp.86-100
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• 2008

It is needed to classify the kinds of construction and demolition(c&d) debris to 6 catagories of waste concrete, waste asphalt concrete, waste wood, scraps, combustible waste and incombustible waste in order to properly do a separate discharge and to estimate unit generation rate in construction site. Also, in this case, the unit treating cost for mixed wastes should be applied with the unit treating cost for combustible waste. The construction standard materials estimation data is used for basic data for estimating unit generation rate. The mixed wastes in this data should be classified to waste wood, combustible waste and incombustible waste, and their ratio is obtained by using the unit generation rate of Asia Pacific Environment and Management Institute and Seoul Metropolitan Development Institute. The waste amounts generated from newly-built construction can be obtained from multiplying the loss rate by the amount of materials used from construction standard estimation data. Also, those from dismantling construction can be obtained by subtracting waste amount generated during newly-built construction from total input amount of materials in newly-built construction. Those in two cases can be used in construction site. It can be used for estimating the amount generated and establishing the treating plan in the case of setting up the policy of waste management and doing the environment impact assessment.

• JSTS:Journal of Semiconductor Technology and Science
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• v.17 no.3
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• pp.438-445
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• 2017

This paper presents a low-power high-resolution band-pass ${\Sigma}{\Delta}$ ADC for accelerometer applications. The proposed band-pass ${\Sigma}{\Delta}$ ADC consists of a high-performance 6-th order feed-forward ${\Sigma}{\Delta}$ modulator with 1-bit quantization and a low-power, area-efficient digital filter. The ADC is fabricated in 180 nm 1P6M mixed-signal CMOS process with a die area of $5mm^2$. This high-resolution ADC got 90 dB peak signal to noise plus distortion ratio (SNDR) and 96 dB dynamic range (DR) over 4 kHz bandwidth, while the intermediate frequency (IF) is shifting from 100 KHz to 200 KHz. The power dissipation of the chip is 5.6 mW under 1.8 V (digital)/3.3 V (analog) power supply.

• Progress in Superconductivity and Cryogenics
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• v.5 no.1
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• pp.13-16
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• 2003

Adhesion of $SrZrO_3$ resistive oxide barrier on Ag sheathed Bi(2223) tapes prepared by the sol-gel and dip-coating method was evaluated with an aid of Taguchi method and Lie($2^1{\times}3^7$) orthogonal arrays to determine the optimal process combination of levels of factors that best satisfy the bigger is better quality characteristic (QC=B). For analyses of results statistical calculations such as average and analysis of variance (ANOVA) were employed to analyze the results for improving the performance qualities of the dip-coated $SrZrO_3$ film. Experimentally, the performance of the films was evaluated in terms of bond strength by varying Sr/Zr moi ratio (A), amount of organic vehicle additives (B), drying temperature (C) and time (D), heat treatment temperature (E) and time (F), respectively. The optimal combination of levels of factors was determined to be $A_3B_2C_3D_2E_1F_3$ having a 90% confidence level.

• 한국연소학회:학술대회논문집
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• 1999.10a
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• pp.173-182
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• 1999

Internally Circulating Fluidized Bed Combustor(ICFBC) has been used for the incineration of waste sewage sludge. In this study hydrodynamic characteristics of two phase flow have been studied in a riser section of ICFBC. A lab-scale riser(l/5 scale of pilot plant) is designed and SiC (Geldart type B) is used for solid particles. Experiments are performed by controlling the fluidization parameters including superficial velocity, particle diameter and secondary air to primary air ratio for determination of solid holdup profiles in the riser. Our flow regime during experiments mainly belongs to the onset of turbulent regime(for d_{p}:300{\mu}m) and fast fluidization regime(for d_{p}:100{\mu}m). Superficial velocities of each regime are well agreed with results obtained by other researches. The results show that the axial solid holdup distributions calculated by measuring differential static pressures in the riser are found to show a basic profile described by a simple exponential function. As the particle size decreases, solid holdup along the riser is more uniformly distributed. To prove these experimental results, numerical calculations are being performed.

• Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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• 2001.04a
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• pp.7-10
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• 2001

Adsorption of the pesticides (phosphamidon, fenitrothion, triadimefon and diniconazole) in natural zeolite (CL $I_{N}$) and several synthetic zeolites was incestigated. The pesticides were not adsorbed on zeolites (Na-Pl, SOD, ANA, JBW and CAN) synthesized from Jeju scoria. The distribution coefficient ( $K_{D}$) and the Freundlich constant ( $K_{F}$) decreased in the following sequences. FC $C_{W}$ (waste catalytic cracking catalyst)>FA $U_{F}$ (FAU Synthesized from coal fly ash)>(FAU+Na-Pl)$_{SF}$ (the mixture of FAU and Na-Pl synthesized from the ratio of Jeju scoria 6 to coal fly ash 4 by weight)>CL $I_{N}$ among the zeolites; diniconazole>fenitrothion> triadimefon>phosphamidon. As the temperature was increased, the amount of pesticide adsorbed per unit mass of zeolite increased for FC $C_{W}$, FA $U_{F}$ and (FAU+Na-Pl)$_{SF}$ but it decreased for CL $I_{N}$, for all the pesticides used in this study. It was independent of pH for phosphamidon, fenitrothion and triadimefon, but decresed as pH was increased for all the zeolites used in this study.y.udy.y.y.y.y.y.y.