• Journal of the Speleological Society of Korea
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• no.71
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• pp.1-4
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• 2006

Chloromethylnaphthalene is a valuable compound for obtaining of the plant growing stimulator - -napthylacetic acid. Chloromethylation of naphthalene by paraformaldehyde in the presence of glacial acetic acid, phosphoric and hydrochloric acids at temperature 80 - 85C and duration - 6 hours the -chloromethylnaphthalene yield was 55-57%. Using Box-Wilson method for mathematical planning of experiment carried out optimization of its synthesis for purpose increasing -chloromethylnaphthalene yield. Preliminary, one - factor experiments were carried out for selecting independence main parameters influencing on the synthesis. A full factor experiment of 23 with extended matrix of planning was used for optimization. Aiming to increase the -chloromethylnaphthalene yield, the obtained mathematical model was used for program of sharp raising on the reply surface. The received optimal conditions for the -chloromethylnaphthalene synthesis were selected as following: molar ratio of naphthalene parapfsormaldehyde of 1 : 2 temperature - 105C duration of the reaction - 3 hours. The yield of -chloromethylnaphthalene under these optimal conditions was 75%.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.22 no.3
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• pp.269-276
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• 2009

Antimony doped tin oxide ($SnO_2:Sb$) films, which are used as the front contact and back reflector of thin film solar cells, have been deposited by d,c, magnetron sputtering. The dependence of electrical and optical properties of the films on the preparation conditions, such as $O_2$ gas ratio, substrate temperature, annealing temperature was investigated. The sputter gas composition was found to affect the properties of the films. With incorporating $O_2$ gas, the electrical and optical properties of films significantly were improved. The minimum resistivity and optical transmittance over 80 % in visible region were obtained at the oxygen concentration of 30 %, When the substrate temperature was higher, the resistivity of $SnO_2:Sb$ films was decreased, while the absorption edge shifted to shorter wavelength, indicating higher optical band gap. Heat treatment over $600^{\circ}C$ resulted in poorer electrical and optical properties due to SnO phase (102) plane.

• Smart Structures and Systems
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• v.18 no.5
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• pp.1063-1085
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• 2016

Taking advantage of the high sensitivity and long-distance detection capability of acoustic emission (AE) technique, this paper focuses on the crack detection in rail head, which is one of the most vulnerable parts of rail track. The AE source location and noise cancellation were studied on the basis of practical rail profile, material and operational noise. In order to simulate the actual AE events of rail head cracks, field tests were carried out to acquire the AE waves induced by pencil lead break (PLB) and operational noise of the railway system. Wavelet transform (WT) was first utilized to investigate the time-frequency characteristics and dispersion phenomena of AE waves. Here, the optimal mother wavelet was selected by minimizing the Shannon entropy of wavelet coefficients. Regarding the obvious dispersion of AE waves propagating along the rail head and the high operational noise, the wavelet transform-based modal analysis location (WTMAL) method was then proposed to locate the AE sources (i.e. simulated cracks) respectively for the PLB-induced AE signals with and without operational noise. For those AE signals inundated with operational noise, the Hilbert transform (HT)-based noise cancellation method was employed to improve the signal-to-noise ratio (SNR). Finally, the experimental results demonstrated that the proposed crack detection strategy could locate PLB-simulated AE sources effectively in the rail head even at high operational noise level, highlighting its potential for field application.

• Advances in materials Research
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• v.9 no.3
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• pp.203-218
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• 2020

This research paper presents the outcomes in terms of mechanical and microstructural characteristics of binary and ternary concrete when exposed to elevated temperature. Three parameter were taken into account, (a) elevated temperature (i.e., 200, 400, 600 and 800℃) (b) binary concrete with cementitious material sugarcane bagasse ash (SCBA) and ground granulated blast furnace slag (GGBFS) replacement percentage (i.e., 0, 15, 20, 25 and 30%) and (c) ternary concrete with cementitious material SCBA and GGBFS replacement percentage (i.e., 0, 15, 20, 25 and 30%). A total of 285 standard cube specimens (150 mm × 150 mm × 150 mm) containing Ordinary Portland Cement (OPC), SCBA, and GGBFS were made. These specimens then exposed to several elevated temperatures for 2 h, afterword is allowed to cool at room temperature. The following basic physical, mechanical, and microstructural characteristics were then determined and discussed. (a) mass loss ratio, (b) ultrasonic pulse velocity (UPV) (c) physical behavior, (d) compressive strength, and (e) field emission scanning electron microscope (FESEM). It was found that compressive strength increases up to 400℃; beyond this temperature, it decreases. UPV value and massloss decrease with increase in temperature as well as the change in color and crack were observed at a higher temperature.

• Proceedings of the Korean Society of Marine Engineers Conference
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• 2012.06a
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• pp.123-124
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• 2012

Effervescent atomizer in which the liquid is ejected from nozzle with bubble caused by gas injection into the liquid is one of twin-fluid atomizers. Effervescent atomizer is operated with the lower injection pressure and the smaller air flow rate when compared with those of other twin-fluid atomizers. In this study, we attempted experiment study to investigate the atomization characteristics of effervescent atomizer related with the internal flow condition. The nozzle was made with acrylic material to investigate the nozzle internal flow. The macroscopic spray analysis was conducted with internal flow images and spray images. Furthermore, SMD was measured by using the laser diffraction method. According to this study, the internal flow condition changed from bubbly flow to annular flow as the air-liquid mass ratio(ALR) increases. At that time, the atomization characteristics were improved.

• The Transactions of the Korean Institute of Power Electronics
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• v.9 no.2
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• pp.178-186
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• 2004

This paper proposes a two-phase RCD-PWM scheme which is much better than a three-phase RCD-PWM scheme from the standpoint of the broadening and linearizing effect of the power spectrum. To implement the proposed scheme and conventional scheme, the experiment based on the SAB-Cl67 micro-controller was executed. Based on the space vector modulation technique, the duty ratio of the pulses is calculated using the SAB-Cl67 and each of PWM pulses is located randomly in each switching interval. The power spectrum of the output voltage, output current, the d.c link current and the acoustic noise radiated from inverter drives are experimentally investigated. 1'hen, the performance of the proposed scheme was compared and discussed with the conventional scheme.

• Journal of Surface Science and Engineering
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• v.28 no.6
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• pp.386-392
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• 1995

The RF planar magnetron sputtering technique was used to fabricate uniform ZnO/$SiO_2$/Si thin films at high growth rate. A detailed crystallographic character of these thin films has been carried oct using XRD, XRC, and SEM. These thin films have the configuration of c-axis orientation perpendicular to $SiO_2$/ Si substrate. The dependence of the thickness of ZnO/$SiO_2$/Si films on applied RF power parameters was also investigated. The crystallinity of films was improved as the substrate temperature was high, RF input power increased, and Ar/$O_2$ ratio decreased. Also, most of ZnO films fabricated on $SiO_2$/Si were suitable for SAW filter since a standard deviation of XRC (002) peak was less than $6^{\circ}$. The presence of the $SiO_2$ layer has a beneficial effect on the crystalline quality of the grown ZnO films.

• Journal of Microbiology and Biotechnology
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• v.18 no.12
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• pp.1927-1931
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• 2008

In this study, the enzymatic process for biodiesel production was optimized using a mixture of immobilized Rhizopus oryzae and Candida rugosa lipases. The optimal temperature and agitation speed for biodiesel production were $45^{\circ}C$ and 300 rpm, respectively. The optimal ratio of R. oryzae and C. rugosa lipases in the mixture was 3:1 (w:w). When 3 mmol of methanol was the initial reaction medium and 3 mmol of methanol was added every 1.5 h during biodiesel production, biodiesel conversion was over 98% at 4 h. In addition, when the immobilized lipase mixture was reused, biodiesel conversion exceeded 80% after 5 reuses.

• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 2000.11b
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• pp.307-312
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• 2000

This study was carried out to develop an automatic grafting system suitable for fruit-vegetable seedlings. The study consisted of two research sections: 1) development of a medium-sized, low-cost automatic grafting system for cooperative farms and commercial seedlings production company, and 2) commercializing research for prototype development based on the above concepts. The grafting robot developed in this research can be described as follows, a. Developed grafting robot can cover the whole operations for grafting scion and rootstock, only if operator provides scion and rootstock tray. b. Five seedlings can be grafted at one time, and about 1,200 seedlings can be grafted in one hour. c. The success ratio of mechanical grafting scion and rootstock with ceramic pin bonding provided by the holder is more than 95% when the conditions of seedlings are satisfied. d. The grafting efficiency has improved over 10 times compared with manual work, and the grafting cost generated 44% savings.

• Applied Biological Chemistry
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• v.24 no.1
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• pp.74-83
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• 1981

Agricultural departmental curricular of the universities have been compared and analyzed with an exception of that of Chung Nam National University where agricultural chemistry department was established in 1979. The analysis reveals that major subjects covered by the undergraduate curricula of all the universities in agricultural cheimstry departments are in the fields of soil science, plant nutrition, agricultural chemicals, biochemistry, and fermentation technology or applied microbiology, although there are minor differences in curricula among universities. Besides, it must be pointed out that the ratio of students to teaching staffs, a significant index of the educational quality, is shown to be somewhat lower than expected for an appropriate college education. According to the analysis, the curricula of universities located in various areas in Korea do not show substantial differences among them, indicating that there is no locality. Thus, it may be recommendable to set up a unified curriculum of agricultural chemistry departments in Korea so as to achieve a balanced educational improvemet.