• Title/Summary/Keyword: $MS^n$

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아까시나무와 밤나무 유래 propolis의 휘발성 향기 성분 특징

  • Song, Hyo-Nam;Kim, Yeong-Eon;Lee, Yeong-Cheol
    • Bulletin of Food Technology
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    • v.12 no.4
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    • pp.28-35
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    • 1999
  • 밀원식물을 달리하여 채집된 두 종류의 국내산 propolis의 향기성분을 Aroma Scan과 GC/MS로 분석하였다. Aroma Scan으로 아까시나무와 밤나무 유래의 두 propolis는 서로 다른 향기를 지닌것을 확인하였다. GC/MS로 분석한 propolis의 향기 성분은 아까시나무 유래 propolis의 44종과 밤나무 유래 propolis의 47종을 포함한 총 55종이 검출되었다. Aldehydes 5종, alcohols 8종, ketones 5종, esters 3종, fatty acid 1종을 비롯하여 27종의 hydrocarbons과 2종의 terpenes 및 4종의 phenolic derivatives가 검출되었다. Benzaldehyde, cinnamyl alcohol, dudesmol 및 benzylbenzoate 등을 포함한 36종의 화합물은 두시료에서 공통적으로 검출되었고, geraniol과 n-undecane을 포함한 8종의 성분은 아까시나무 유래의 propolis에서만 확인되었으며, piperitenone과 valencene을 포함한 11종의 화합물은 밤나무 유래의 propolis에서만 검출되어 밀원식물에 따라 향기성분에 차이가 있는 것으로 나타났다.

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Identification of New Compounds from Catharanthus roseus Hairy Root Cultures

  • Chung, Ill-Min;Ali, Mohd;Yang, Young-Mok;Peebles, Christie A. M.;Chun, Se-Chul;Lee, Sun-Joo;San, Ka-Yiu;Ahmad, Ateeque
    • Bulletin of the Korean Chemical Society
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    • v.28 no.8
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    • pp.1294-1298
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    • 2007
  • Two new compounds lanast-5,8-dien-3β-ol-27-oic acid-3β-D-glucopyranosyl (4'-1'')-10'',11''-dimethoxy anthracene (1), 2-methoxy-6-(n-nonacontan-5'',6''-dionyl)-11-hydroxy-13-methyl-11β-D-rhamnopyranoside anthracene (2) have been isolated from the hairy root cultures of Catharanthus roseus. Their structures have been elucidated with the help of 500 MHz NMR using one- and two-dimensional NMR in combination with IR, EI/MS, FAB/MS and HRFABMS spectroscopy.

Rapid Identification of the ${\alpha}$-Glucosidase Inhibitory Compounds from Geranium thunbergii Sieb. et Zucc. by HPLC-micro-fractionation and HPLC-UV-$MS^n$

  • Choi, Se-Jin;Kim, Jin-Kyu;Lee, Yeon-Sil;Lim, Soon-Sung
    • 한국약용작물학회:학술대회논문집
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    • 2010.10a
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    • pp.430-430
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    • 2010
  • In this study ethanol extracts of aerial part of Geranium thunbergii Sieb. et Zucc. was investigated for their ability to inhibit a-glucosidase, and thus was fractionated using two organic solvents, including dichloromethane, ethyl acetate. The ethyl acetate-soluble fraction, which manifested potent enzyme inhibitory properties, was then followed by tracking down the active compound by combining HPLC micro-fractionation to an enzyme assay in 96-well plate. The ${\alpha}$-glucosidase inhibitory activity profile showed that two peaks exhibited potent inhibitory activity, and then the structural analyses of the two peaks were carried out by HPLC-UV-MS. The main ${\alpha}$-glucosidase inhibitory compounds in the ethyl acetate-soluble fractions of ethanol extracts of Geranium thunbergii Sieb. et Zucc. were tentatively identified as geraniin and kaempferol-7-rhamnoside.

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Volatile Flavor Components of Leek(Allium tuberosum Rottler) (부추(Allium tuberosum Rottler)의 휘발성 향기성분)

  • 김경수;박은령;조정옥;김선민;이명렬
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.27 no.4
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    • pp.563-567
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    • 1998
  • Volatile flavor components of edible portion of leek(Allium tuberosum R.) were extracted by SDE(simultaneous steam distillation and extraction) method using the mixture of n-pentane and diethylether (1 : 1, v/v) as an extract solvent and analyzed by GC-FID and GC/MS. Identification of the volatile flavor components was mostly based on the RI of GC and mass spectrum of GC/MS. A total of sixty-five components from leek extract were classified as 28 sulfur-containing compounds, 12 aldehydes, 9 alcohols, 4 lactones and esters, 3 acids and hydrocarbons, and 2 miscellaneous compouds. The sulfur-containing compounds were predominant in leek extract. Dimethyl disulfide(19.47%) and dimethyl trisulfide(17.38%) were the main compounds and trans-1-propenyl methyl disulfide, trans-2-hexenal and methyl allyl disulfide were also detected large amounts in leek.

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Methylation Methods on Identification of Phenolics in Chebulae Fructus (Chebulae Fructus중 페놀 물질 확인시의 Methylation법 비교)

  • 김정숙
    • Journal of the East Asian Society of Dietary Life
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    • v.4 no.1
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    • pp.79-86
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    • 1994
  • Food quality in food processing and storage were affected by the kinds of phenolics involved. To analyze phenolics of Chebulae Fructus by the way of GC-MSm methylation and trimethylsilyation(TMS) are necessary. The methods of methylation were dimethyl sulfate method and diazomethane method. so this study was undertaken to research the better methylation method before measuring GC-MS. But dimethyl sulfate method of methylation was not sufficient to analyze phenolics. So the phenolics of Chebulae Fructus were analyzed by the diazomethane methylation method and TMS with the pyridine, N-O-bis-trimethylsilyl-acetamide(BSTFA) and trimethylchlorosilane(TMCS). With the exception of pyrogallol and phloroglucinol in insoluble phenolics of Chebulae Fructus, the greater part of phenolics. analysis could be analyzed by GC-MS in company with diazomethane methylation method and TMS.

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Plant Regeneration from Turnip (Brassica rapa ssp. rapifera) Organs

  • Gendaram Sarantuya;Bae Chang-Hyu
    • Plant Resources
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    • v.8 no.3
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    • pp.286-292
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    • 2005
  • Shoot induction system was developed in the recalcitrant plant species, Brassica rapa ssp. rapifera by using optimum selection of profit organ, phytohormone combination, seedling age and kind of culture container. Out of in vitro cultured leaf segment, petiole, hypocotyl, and cotyledon with petiole, only cotyledon with petiole derived from 4 day-old seedlings induced multiple shoot. The optimum combination of auxin and cytokinin for the multiple shoot induction was MS medium containing 5mg/L BA and 0.5mg/L NAA. The major factors for multiple shoot propagation were part of plant organ, age of seedling, and ratio of auxin and cytokinin. In addition, shoot regeneration was promoted in the 100ml Erlenmeyer flask compared with the $90mm{\times}20mm$ Petri-dish. The induced shoots formed roots easy on MS medium containing 0.1mg/L IBA and the whole plants were successfully cultivated in soil.

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New Ceramide from Alocasia macrorrhiza

  • Tien, Nguyen Quyet;Ngoc, PhamHoang;Minh, Pham Hong;Kiem, Phan Van;Minh, Chau Van;Kim , Young-Ho
    • Archives of Pharmacal Research
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    • v.27 no.10
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    • pp.1020-1022
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    • 2004
  • A new ceramide alomacrorrhiza A was isolated from the ethanolic extract of the plant Alocasia macrorrhiza (L.) Schott. Its chemical structure was elucidated as (2S,3S,4R)-2N-[(2'R)-2'- hydroxy-hexacosanoyl]-tetradecane-1,3,4-triol based on extensive 1D, 2D NMR, EI-MS, FABMS, HR-FAB-MS spectroscopic data and chemical degradation studies.

Real-time DSP implementation of IMT-2000 speech coding algorithm (IMT-2000 음성 부호화 알고리즘의 실시간 DSP 구현)

  • Seo, Jeong Uk;Gwon, Hong Seok;Park, Man Ho;Bae, Geon Seong
    • Journal of the Institute of Electronics Engineers of Korea SP
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    • v.38 no.3
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    • pp.68-68
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    • 2001
  • 본 논문에서는 3GPP와 ETSI에서 IMT-2000의 음성부호화 방식 표준안으로 채택한 AMR 음성부호화 알고리즘을 분석하고 C 컴파일러와 어셈블리 언어를 이용한 최적화 과정을 거친 후, 고정 소수점 DSP 칩인 TMS320C6201을 이용하여 실시간 구현하였다. 구현된 codec의 프로그램 메모리는 약 31.06 kWords, 데이터 RAM 메모리는 약 9.75 kWords, 그리고 데이터 ROM 메모리는 약 19.89 kWords 정도를 가지며, 한 프레임(20 ms)을 처리하는데 약 4.38 ms가 소요되어 TMS320C6201 DSP 칩의 전체 가용한 clock의 21.94%만 사용하여도 충분히 실시간으로 동작 가능함을 확인하였다. 또한, DSP 보드상에서 구현한 결과가 ETSI에서 공개한 ANSI C 소스 프로그램의 수행 결과와 일치함을 검증하였고, 구현된 AMR 음성부호화기를 sound I/O 모듈과 결합하여 실험한 결과, 어떠한 음질의 왜곡이나 지연 없이 실시간으로 충분히 동작함을 확인하였다. 마지막으로, Host I/O와 LAN 케이블을 이용하여 AMR 음성부호화 알고리즘을 통한 쌍방간 실시간 통신을 full-duplex 모드로 확인하였다.

MobPrice: Dynamic Data Pricing for Mobile Communication

  • Padhariya, Nilesh;Raichura, Kshama
    • Journal of information and communication convergence engineering
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    • v.13 no.2
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    • pp.86-96
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    • 2015
  • In mobile communication, mobile services [MSs] (e.g., phone calls, short/multimedia messages, and Internet data) incur a cost to both mobile users (MUs) and mobile service providers (MSPs). The proposed model MobPrice consists of dynamic data pricing schemes for mobile communication in order to achieve optimal usage of MSs at minimal prices. MobPrice inspires MUs to subscribe MSs with flexibility of data sharing and intra-peer exchanges, thereby reducing overall cost. The main contributions of MobPrice are three-fold. First, it proposes a novel k-level data-pricing (kDP) scheme for MSs. Second, it extends the kDP scheme with the notion of service-sharing-based pricing schemes to a collaborative peer-to-peer data-pricing (pDP) scheme and a cluster-based data-pricing (cDP) scheme to incorporate the notion of 'cluster' (made up of two or more MUs) in mobile communication. Third, our performance study shows that the proposed schemes are indeed effective in maximizing MS subscriptions and minimizing MS's price/user.

Practical use of MS SDLC for small mobile app development (소규모 앱 개발을 위한 MS 시큐어 소프트웨어 개발 방법론의 활용 연구)

  • Hur, Jung-Hun;Choi, Jin-Young
    • Proceedings of the Korean Information Science Society Conference
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    • 2012.06c
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    • pp.292-294
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    • 2012
  • 최근 모바일과 테블릿 등의 휴대용 디바이스들 활성화로 인해서 어플리케이션의 종류가 확대되고 누구나 어플리케이션 개발에 쉽게 어플리케이션 제작을 할 수 있어짐에 따라서 개발 조직의 소규모와 개인 개발자들의 활동이 늘어가고 있다. 하지만 현재 앱에 관련된 소프트웨어의 개발 방법론은 많지 않다. 그래서 이 논문에서는 1)소프트웨어의 보안개발주기의 최소화를 통해 개발자들에게는 보안가이드 라인을 제공하고 2)소규모의 개발자들이 주어진 보안개발 방법론을 따라 품질과 보안성을 향상하고 3)정부나 앱스토어의 검증성을 높여서 고객이 신뢰하고 검증된 모바일 어플리케이션을 사용할 수 있게 하는 것이다.