• Title/Summary/Keyword: $H_2O$ content

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Preparation of $Mg(OH)_2$and MgO from Acid Leaching $Mg^{++}$ Solution (산 침출$Mg^{++}$액으로부터 $Mg(OH)_2$및 MgO 粉末의 製造)

  • 최용각;이종현;원창환;이갑호
    • Resources Recycling
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    • v.10 no.5
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    • pp.16-21
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    • 2001
  • Ultrafine $Mg(OH)l_2$and MgO powders were recovered from the waste solution containing $Mg^{++}$ which was a by-product of SHS (Self-propagating High temperature Synthesis)process. The optimum experimental conditions to prepare $Mg(OH)_2$were 13.0 of pH and 0.7M of $Mg^{++}$ content with addition of 9M of KOH as a pH regulator in acid leaching solution. Complete pre-cipitation of Mg(OH)$_2$from $Mg^{++}$ was realized at that condition. The dehydration reaction of the prepared Mg(OH)$_2$was studied by DSC, and the result was used for calcination process. In order to obtain MgO powder, dried Mg(OH)2 powder was calcined at $400~450^{\circ}C$. Particle size and shape of the prepared $Mg(OH)_2$and MgO powder was similar to those of the commercial powders.

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Persistence of Salmonella enterica, Escherichia coli O157:H7, and Listeria monocytogenes in Soil, Liquid Manure Amended Soil, and Liquid Manure

  • Jung, Kyu-Seok;Kim, Min-Ha;Heu, Sung-Gi;Roh, Eun-Jung;Lee, Dong-Hwan;Lim, Jeong-A;Ryu, Jae-Gee;Kim, Kye-Hoon
    • Korean Journal of Soil Science and Fertilizer
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    • v.47 no.6
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    • pp.432-436
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    • 2014
  • While searching for healthier diets, people became more attentive to agricultural organic products. However, organic foods may be more susceptible to microbiological contamination because of the use of livestock manure compost and liquid manure, potential sources of pathogenic bacteria. This study was undertaken to investigate the persistence of Salmonella enterica, Escherichia coli O157:H7, and Listeria monocytogenes in soil, liquid manure amended soil, and liquid manure. Loamy soil, liquid manure amended soil, and liquid manure were inoculated with S. enterica, E. coli O157:H7, and L. monocytogenes. Samples were incubated in consistent moisture content at $25^{\circ}C$. Samples had been periodically collected during 120 days depending on the given conditions. S. enterica and E. coli O157:H7 survived over 120 days in loamy soil and over 60 days in liquid manure amended soil, respectively. L. monocytogenes decreased faster than other pathogens in soil. S. enterica, E. coli O157:H7, and L. monocytogenes survived for up to 5 days in liquid manure. S. enterica and E. coli O157:H7 in soil decreased by 2 to $2.5log\;CFU\;g^{-1}$ for 120 days. S. enterica and E. coli O157:H7 in liquid manure amended soil decreased slowly for 21 days. However, S. enterica, E. coli O157:H7, and L. monocytogenes sharply decreased after 21 days. S. enterica, E. coli O157:H7, and L. monocytogenes in soil increased by 0.5 to $1.0log\;CFU\;g^{-1}$ for 7 days. Foodborne pathogens in soil and liquid manure amended soil gradually decreased over time.

Optimization of Extraction Conditions for Total Phenolics from Sapium japonicum Using a Pressurized Liquid Extractor

  • Kim, Mi-Bo;Park, Jae-Sung;Lim, Sang-Bin
    • Food Science and Biotechnology
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    • v.18 no.4
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    • pp.996-1000
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    • 2009
  • Sapium japonicum was extracted by a pressurized liquid. Operating parameters such as the type and the ratio of solvent to water, temperature, pressure, and number of extractions were investigated as the main variables that influence the extraction efficiencies of total phenolics (TP). MeOH extracted the highest level of TP as 50.4 mg GAE/g compared to 48.8 and 27.2 mg GAE/g with $H_2O$ and EtOH, respectively. $EtOH:H_2O$ (40:60, v/v) was found to be the best solvent for TP extraction as 90.3 mg GAE/g compared to 85.0 and 84.3 mg GAE/g in 40:60 and 60:40 of $MeOH:H_2O$, respectively. TP were increased with the increase of the number of extraction steps. TP content was increased by 11% as the extraction temperature was increased from 40 (97.4) to $50{\circ}C$ (108.3 mg GAE/g). The optimum extraction conditions of TP were; extraction solvent, $EtOH:H_2O$ (40:60, v/v); temperature, $50{\circ}C$; pressure, 10.2 MPa; 2 extraction steps.

Protective Effect of Ginsenoside Rgl on H2O2-Induced Cell Death by the Decreased Ceramide Level in LLC-PK1 Cells

  • Lee, Youn-Sun;Yoo, Jae-Myung;Shin, Hyun-Woo;Kim, Dong-Hyun;Lee, Yong-Moon;Yun, Yeo-Pyo;Hong, Jin-Tae;Oh, Sei-Kwan;Yoo, Hwan-Soo
    • Journal of Ginseng Research
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    • v.30 no.1
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    • pp.1-7
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    • 2006
  • Ceramide has been involved in celt death and acted as a lipid mediator of stress responses. Elevation of ceramide level was reported to occur in oxidative stress and lead to cell death in many cell types. This study was undertaken to elucidate a protective role of ginsenoside Rgl in cell death induced by oxidative stress. When LLC-PK1 cells were treated with $H_2O_2$ at a concentration of $400{\mu}M$ for 5 hr, cell death was observed and a released LDH activity indicative of cytotoxicity was Increased. $H_2O_2$ exposure to LLC-PK1 cells was shown to elevate the content of total ceramide by approximately 200% compared to control cells. Ceramide level was hypothesized to be a key to a reversal of cell death to survival. Ginsenoside Rgl at the concentrations ranging from 12.5 to $250{\mu}M$ protected LLC-PK1 cells from cell death induced by $H_2O_2\;at\;400{\mu}M$ for 5 hr, and decreased the ceramide level relative to $H_2O_2$. Ginsenoside Rgl inhibited neutral human ceramidase by 71% of controls, while sphingomyelinase was not inhibited. These results suggest that ginsenoside Rgl show the protection against cell death via the modulation of ceramide metabolism, and ceramide may be a promising therapeutic target for human diseases related to cell death.

Fabrication of Al2O3 Dispersed Porous Cu by Freeze Drying of CuO-Al2O3/Camphene Slurry (CuO-Al2O3/camphene 슬러리의 동결건조 공정에 의한 Al2O3 입자분산 Cu 다공체 제조)

  • Kang, Hyunji;Riu, Doh-Hyung;Oh, Sung-Tag
    • Journal of Powder Materials
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    • v.25 no.1
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    • pp.25-29
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    • 2018
  • Porous Cu with a dispersion of nanoscale $Al_2O_3$ particles is fabricated by freeze-drying $CuO-Al_2O_3$/camphene slurry and sintering. Camphene slurries with $CuO-Al_2O_3$ contents of 5 and 10 vol% are unidirectionally frozen at $-30^{\circ}C$, and pores are generated in the frozen specimens by camphene sublimation during air drying. The green bodies are sintered for 1 h at $700^{\circ}C$ and $800^{\circ}C$ in $H_2$ atmosphere. The sintered samples show large pores of $100{\mu}m$ in average size aligned parallel to the camphene growth direction. The internal walls of the large pores feature relatively small pores of ${\sim}10{\mu}m$ in size. The size of the large pores decreases with increasing $CuO-Al_2O_3$ content by the changing degree of powder rearrangement in the slurry. The size of the small pores decreases with increasing sintering temperature. Microstructural analysis reveals that 100-nm $Al_2O_3$ particles are homogeneously dispersed in the Cu matrix. These results suggest that a porous composite body with aligned large pores could be fabricated by a freeze-drying and $H_2$ reducing process.

Changes of Chemical Components during Fermentation of Pear(Pyrus pyrifolia Nakai) Wine (신고배(Pyrus pyrifolia Nakai)를 이용한 배술 제조 과정 중 성분 변화)

  • Park, Hae-Min;Lee, Ka-Soon;Hong, Jong-Sook;Oh, Man-Jin
    • Korean Journal of Agricultural Science
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    • v.36 no.2
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    • pp.199-209
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    • 2009
  • For increasing the consumption of pear, the pear wines were made by using eight different kinds of yeast. The chemical properties, such as pH, acidity, ethanol and sugar contents, and the consumer acceptance of various pear wines were analyzed. In analysis result of chemical properties, the value of pH was decreased and the acidity was increased until few days, and then retained during fermentation. The ethanol content was increased and the sugar content was decreased during fermentation. The pear wine brewed by B yeast (Lalnin, Saccharomyces cerevisiae) among eight different kinds of yeast had the highest content of ethanol, also this wine was represented the most consumer acceptance by the panels who consist of two age groups such as 20's to 30's and 50's to 60's. Therefore, we chose the yeast B for analyzing the effect of additives during fermentation. As the additives, the $K_2S_2O_5$ and ammonium phosphate as the disinfectant and hemicellulase and pectinase as fermenting conditioner were added into the pear wine brewed by yeast B. When additives are added, the chemical properties were the same as followed. Te values of pH was lower than when additives were not added(control). The acidity was he highest when ammonium phosphate was added, but the acidity was not changed after 4 day fermentation. Sugar contents when added $K_2S_2O_5$ 350ppm was shown the fastest deceasing, and it was orderly decreased as control, ammonium phosphate, hemicellulase, pectinase, and $K_2S_2O_5$ 175ppm. The decreasing rate of sugar content of these 6 test groups during fermentation gradually decreased without a big changes and the after 7 day fermentation, sugar contents were seldom decreased and the final sugar content was $9.5{\sim}9.8^{\circ}Brix$. In terms of change of the content of ethanol, all test groups generated 11~12.4% ethanol after 7 day fermentation. The group where ammonium phosphate was added generated 12.4% alcohol, which is the fastest speed and the group, which hemicellulase additive was added, showed generally slow alcohol generation rate. In terms of ethanol contents, the non-additive group and $K_2S_2O_5$ additive group showed 0.05%, which is very low, and hemicellulase and pectinase additive group is more than 0.5% which is rather high.

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Investigation of Slury Properties for Aqueous Casting of Nano-Size Barium Titanate (나도 티탄산 바륨의 수계 성형을 위한 슬러리 특성연구)

  • 김상우;신용욱;이해원;손용배
    • Journal of the Korean Ceramic Society
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    • v.36 no.7
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    • pp.705-710
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    • 1999
  • Stability and chemical durability for aqueous casting of BaTiO3 slurry with polycarylic acid(PAA) were studied. PAA was well chemisorbed on surface of BaTiO3 powder at neutral pH but did not chemically adsorbed at low pH. The amount of Ba dissolution in aqueous BaTiO3 slurry was abruptly increased at strong acid pH2 and also at high amount of PAA. Protection of Ba dissolution and stability of slurry could be obtained through the optimization of slurry conditions such as pH amount of surfactant and solid content.

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Study on Precipitation of the Minerals in the Soil of Imha Reservoir Watershed (임하호 유역 토양의 광물학적 침전성 연구)

  • Kim, Yeonjeong;You, Samhwan;Jeong, Hyungjin;Baek, Seungcheol;Lee, Sungmin;Seo, Eulwon
    • Journal of the Korean GEO-environmental Society
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    • v.11 no.4
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    • pp.13-18
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    • 2010
  • The present study was undertaken to investigate the characteristic of suspended matter in soils of Imha-Dam area by turbidity. Soil sampling was conducted at 5 points of Yeongyang (Turbid area) and 2 points of Cheongsong (Clean area). Experimental analysis was conducted using those samples. The pH of water in the soils at turbid area was higher than that of clean area. X-ray diffraction analysis showed that every sample consists in mainly quartz, illite and feldspar before precipitation. After precipitation for 3 days, the content of quartz and feldspar was decreased and the content of illite was increased at turbid area. The soil of Sinheung (St. 6) at clean area was analyzed only illite. SEM-EDS analysis showed the much content of $SiO_2$ as to every sample before precipitation, but $K_2O$, MgO, $Al_2O_3$, CaO and $Fe2O_3$ with illite was increased after precipitation for 3 days as to every sample. Experimental results exhibited that the major mineral of turbid water was illite at turbid area and clean area.

Effect of Swine Liquid Manure and Phosphorus Application on Chemical Properties and Microbial Population of Italian (제주화산회토지역에서 돈분액비와 인산시용이 이탈리안 라이그라스 재배 토양의 화학적 특성 및 미생물상에 미치는 영향)

  • 김문철;현해남;최대진;문봉춘;고용구;강태숙
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.21 no.4
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    • pp.181-190
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    • 2001
  • This study was conducted to investigate the effect of swine liquid manure(SLM) and phosphorus fertilizer from September, 1998 to July, 1999 on the soil fertility on Italian ryegrass field, Cheju volcanic ash soil. pH(lst investigated), Mg (2nd investigated) and Cu content (2nd investigated) on soil grown by Italian ryegrass were significantly increased by an increase of fertilizer P(P

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Effects of Hardener and Extender Contents on Curing Behavior of Urea-Melamine-Formaldehyde Resin

  • Eom, Young-Geun;XU, Guang-Zhu;Lee, Young-Kyu;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.5
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    • pp.42-48
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    • 2008
  • This study was conducted to discuss the effects of hardener and extender contents on peak temperature, reaction enthalpy (${\Delta}H$), gelation time, viscosity change, and pH value in three types of UMF (urea-melamine- formaldehyde) resin with the help of perpHecT LogR meter, differential scanning calorimetry (DSC), and advanced rheometric expansion system (ARES), The results indicated that the pH value of Control A steeply decreased to 5,2 in the early stage but relatively remained constant thereafter as in Synthesis 1 and Synthesis 2, The peak temperature and time decreased as well, whereas ${\Delta}H$ and viscosity increased with the increase of hardener content. On the other hand, ${\Delta}H$ was not changed up to the extender content of 5% and then decreased with its further addition, And the pH value and peak temperature showed no change with the increase of extender content at the hardener content of 5% in three types of UMF resin, The effect of hardener content in this experiment, however, appeared more conspicuous in Control A than in the other two types of Synthesis 1 and Synthesis 2, These results might be caused by higher molecular weight with longer chains of methylene ($-CH_2-$) and methylene ($-CH_2-O-CH_2-$) ether bridges or much more branched chains in Control A.