• 한국재료학회지
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• 제23권4호
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• pp.219-226
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• 2013

Activated magnetite ($Fe_3O_{4-{\delta}}$) has the capability of decomposing $CO_2$ proportional to the ${\delta}$-value at comparatively low temperature of $300^{\circ}C$. To enhance the $CO_2$ decomposition capability of $Fe_3O_{4-{\delta}}$, $(Fe_{1-x}Co_x)_3O_{4-{\delta}}$ and $(Fe_{1-x}Mn_x)_3O_{4-{\delta}}$ were synthesized and then reacted with $CO_2$. $Fe_{1-x}Co_xC_2O_4{\cdot}2H_2O$ powders having Fe to Co mixing ratios of 9:1, 8:2, 7:3, 6:4, and 5:5 were synthesized by co-precipitation of $FeSO_4{\cdot}7H_2O$ and $CoSO_4{\cdot}7H_2O$ solutions with a $(NH_4)_2C_2O_4{\cdot}H_2O$ solution. The same method was used to synthesize $Fe_{1-x}Mn_xC_2O_4{\cdot}2H_2O$ powders having Fe to Mn mixing ratios of 9:1, 8:2, 7:3, 6:4, 5:5 with a $MnSO_4{\cdot}4H_2O$ solution. The thermal decomposition of synthesized $Fe_{1-x}Co_xC_2O_4{\cdot}2H_2O$ and $Fe_{1-x}Mn_xC_2O_4{\cdot}2H_2O$ was analyzed in an Ar atmosphere with TG/DTA. The synthesized powders were heat-treated for 3 hours in an Ar atmosphere at $450^{\circ}C$ to produce activated powders of $(Fe_{1-x}Co_x)_3O_{4-{\delta}}$ and $(Fe_{1-x}Mn_x)_3O_{4-{\delta}}$. The activated powders were reacted with a mixed gas (Ar : 85 %, $CO_2$ : 15 %) at $300^{\circ}C$ for 12 hours. The exhaust gas was analyzed for $CO_2$ with a $CO_2$ gas analyzer. The decomposition of $CO_2$ was estimated by measuring $CO_2$ content in the exhaust gas after the reaction with $CO_2$. For $(Fe_{1-x}Mn_x)_3O_{4-{\delta}}$, the amount of $Mn^{2+}$ oxidized to $Mn^{3+}$ increased as x increased. The ${\delta}$ value and $CO_2$ decomposition efficiency decreased as x increased. When the ${\delta}$ value was below 0.641, $CO_2$ was not decomposed. For $(Fe_{1-x}Co_x)_3O_{4-{\delta}}$, the ${\delta}$ value and $CO_2$ decomposition efficiency increased as x increased. At a ${\delta}$ value of 0.857, an active state was maintained even after 12 hours of reaction and the amount of decomposed $CO_2$ was $52.844cm^3$ per 1 g of $(Fe_{0.5}Co_{0.5})_3O_{4-{\delta}}$.

• 한국식품과학회지
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• 제31권5호
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• pp.1289-1294
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• 1999

마른 오징어를 실험실에서 직접 제조한 후 3종(투명, 흰색, 검정색)의 포장재에 포장하여 직사광선이 조사되는 상온조건(6월${\sim}$7월)에서 50일간 저장중 마른 오징어의 품질변화를 측정하였다. 저장 기간중 수분 함량 및 수분활성도의 변화는 극히 미미한 것으로 측정되었으며 총균수의 변화도 거의 변화가 없는 것으로 측정되어 수분 함량 및 미생물에 의한 마른 오징어의 품질변화가 거의 없는 것으로 생각되었다. 직시 색차계를 이용하여 저장중 마른 오징어의 색택 변화를 측정하였을 때 흰색, 검정색의 유색 포장재로 포장한 처리구의 경우 L값이 투명 포장재에 비하여 높게 측정되었으며 ${\Delta}E$값의 경우도 유사한 경향을 나타내었다. ${\Delta}E$ 값의 경우 저장 초기에 급속하게 증가하였으며 그 이후로는 완만하게 증가하는 경향이었다. TBA value를 측정하였을 경우 저장 초기에 급속하게 증가하였으며 그 이후로는 완만하게 감소하는 경향을 나타내어 마른 오징어의 갈색화는 저장 초기의 지질산화에 의해 진행되는 것으로 판단되었다. 또한 3종의 포장재에 대한 자외선 투과 실험 결과 흰색, 검정색의 포장재가 자외선 차단 효과가 있는 것으로 나타나 마른 오징어의 포장시 투명 포장재 보다는 유색포장재를 사용하는 것이 지질산화에 의한 갈변현상을 어느정도 억제할 수 있는 방법이라고 생각되었다.

• 대한치과보철학회지
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• 제37권4호
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• pp.425-432
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• 1999

The purpose of this study is to evaluate the color differences that can exist between different brands of dentin porcelain having identical shade designations. The instrumental colorimetric technique was used to determine these differences. The three brands of dentin porcelain used were Vita VMK-68, Shofu Vintage, and Ceramco II. The three shades selected were the Vita Lumin shades A2, B2, and C2. The color difference values were compared with each other using $L^*,\;a^*,\;b^*$, three variables of the CIELAB color system, and ${\Delta}E$. The results of this study were as follows: 1 Corresponding shades of different brands of dentin porcelain produced different $L^*,\;a^*,\;b^*$ values. 2. The greatest ${\Delta}E$ value in corresponding shade was found to exist between Ceramco II and Shofu Vintage, followed by between Vita VMK-68 and Ceramco II, and then between Vita VMK-68 and Shofu Vintage. 3. The ${\Delta}E$ values in shade C2 were mainly influenced by ${\Delta}L^*$ value ; however none of ${\Delta}L^*,\;{\Delta}a^*,\;{\Delta}b^*$ values had greater influence on ${\Delta}E$ values than the others in shade A2, B2. 4. Shofu Vintage had the highest $b^*$ value, followed by Vita VMK-68, and then Ceramco II.

• 대한화학회지
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• 제58권6호
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• pp.517-523
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• 2014

UV-Vis 분광도법을 이용하여 순수 물에서 TTAB(tetradecyltrimethylammonium bromide) 계면활성제분자의 미셀화와 그 용액에서 4-할로겐화 페놀유도체들의 가용화에 대해 연구하였다. 또한 이들 물성에 미치는 NaCl과 n-부탄올의 효과를 조사함으로써 미셀과 페놀유도체와의 상호작용과 미셀 내에서 가용화되는 위치를 추정하였다. 그 결과, 미셀화에 대한 ${\Delta}G^o_m$값과 가용화에 대한 ${\Delta}G^o_s$값은 모두 음의 값을 나타내었으며, 첨가제의 종류와 농도에 따라 이들 열역학적 함수값들은 각기 다른 변화를 보였다. 즉, NaCl의 농도를 증가하였을 때 ${\Delta}G^o_m$와 ${\Delta}G^o_s$값은 모두 감소하였다. 그러나 n-부탄올의 농도를 증가할수록 ${\Delta}G^o_m$값은 감소한 반면에 ${\Delta}G^o_s$값은 오히려 증가하였다.

• Journal of Electrical Engineering and Technology
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• 제5권2호
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• pp.255-263
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• 2010

The compensated-current-differential relay uses the same restraining current as a conventional relay, but the differential current is modified to compensate for the effects of the exciting current. Delta winding current is necessary to obtain the modified differential current for a $Y-\Delta$ transformer. This paper describes an estimation algorithm of the delta winding current and its application to a compensated-current-differential relay for a $Y-\Delta$ transformer. Prior to saturation, the core-loss current is calculated and used to modify the differential current. When the core first enters saturation, the initial value of the core flux is obtained by inserting the modified differential current into the magnetization curve. This flux value is used to derive the magnetizing current and consequently the modified differential current. The operating performance of the proposed relay was compared against a conventional current differential relay with harmonic blocking. Test results indicate that the proposed relay remained stable during severe magnetic inrush and over-excitation, and its operating time is significantly faster than a conventional relay. The relay is unaffected by the level of remanent flux and does not require an additional restraining or blocking signal to maintain stability. This paper concludes by implementing the proposed algorithm into a prototype relay based on a digital signal processor.

• 한국지반공학회논문집
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• 제29권10호
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• pp.19-27
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• 2013

Tatsuoka and Shibuya(1991)는 하나의 식으로 연약 점성토에서 연암에 이르는 광범위한 지반재료에 대해 적용 가능하며, 넓은 범위의 변형률 수준($10^{-6}{\sim}10^{-2}$)에 대해 적용할 수 있는 새로운 제안식을 발표하였다. 본 연구는 세계 각국의 주요 연구기관에서 사용되고 있는 7종류의 연구용 표준사 공시체 및 2종류의 유리 구슬(Glass beads) 공시체를 이용하여 평면변형률압축시험을 실시하고, 새롭게 제안된 식에 적용하여 각각의 파라메타의 경향성에 대해 연구하였다. 그 결과 구속압이 클수록 $C_1(X={\infty})$ 값이 크게 되지만, $C_2(X={\infty})$ 값은 거의 변화하지 않았다. ${\delta}$에 대한 $C_1(X={\infty})$ 값의 변화는 모래의 종류에 관계없이 ${\delta}$가 클수록 크게 되는 경향이 있지만, $C_2(X={\infty})$, $C_2$(X=Xe) 값은 ${\delta}$가 변화해도 그다지 변화하지 않았다. 한편, ${\alpha}$, ${\beta}$값은 ${\delta}$가 감소함에 따라 약간 감소하는 경향이 있었다.

• 대한임상검사과학회지
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• 제44권2호
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• pp.66-74
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• 2012

Test turnaround time (TAT) is the lead time from reception to reporting. In the complete blood cell count (CBC), 4 units of the XE-2100 (Sysmex Corp., Japan) processed around 80% of quantity, 1 unit of the LH-780 (Beckman-Coulter Incorp., USA) processed around 10% and 1 unit of ADVIA-2120 (Siemens AG, Munich, Germany) processed around 10%. We analyzed the change in the TAT for the CBC for over 7 years, from January of 2005 to December of 2011. The delta check made alterations of delta to WBC, hemoglobin, hematocrit, platelet and metamyelocyte, however, did not made them to band neutrophil, eosinophil, basophil and monocyte. The panic value check made alterations of panic value to hemoglobin, hematocrit, platelet and monocyte. In the criteria of currently slide review, LH-780 and ADVI-2120 analyzers prepared suspect flags of "Blast, Imm NE2, Immature granulocyte, Imm NE1, Left shift, Variant lymphocyte, Atypical lymphocyte, Platelet clumps and NRBC". The New slide review in the XE-2100 analyzer altered the preparations of a smear slide more than a "Platelet clumps flag(${\geq}200unit$), a single flag excluding the "Platelet clumps flag (${\geq}250unit$) and a multiple flag (${\geq}200unit$)". Also, below the 240 unit, medical technologists prepared manual slides selectively according to their evaluations. The automatic reporting rate was 33.4% without alterations, whereas it was 41.0% without alterations, and was thus improved by 7.6%. The slide review rate was 15.2% before using the Q-flag limit, whereas it was 12.1% for a reduce 3.1%. TAT was 45 minutes without the creation alterations of the delta and panic value checks, whereas it was 35 minutes after making alterations of the delta and panic value checks and thus was shortened by 10 minutes. We came to the conclusion that the establishment and operation of delta and panic value checks and slide review criteria suitable for laboratory environment can reduce unnecessary smear slides, re-checking, re-sampling, re-testing, telephone inquiries and concentrated workloads during specific times of the day.

• 한국식품과학회지
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• 제32권5호
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• pp.1149-1157
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• 2000

고추장 변색 요인을 확인하기 위하여 전통적인 방법으로 떡고추장과 식혜고추장을 만들고 가열처리, 포장중 질소치환 및 U.V 조사여부에 따른 변화를 관찰하였다. 각 고추장의 색도 변화는 일반적으로 숙성기간이 경과됨에 따라 L, a, b값은 감소하고 ${\delta}E$ 값은 증가하는 경향을 보였다. 그 중 떡고추장의 ${\delta}E$ 값은 자외선 조사구에서 다른 처리구에 비하여 높았고 식혜고추장의 ${\delta}E$ 값은 비열처리구에서 전반적으로 높게 나타났다. 갈변 요인 분석에서는 떡고추장의 주요 갈변 요인으로는 빛이, 식혜고추장에서는 열처리와 빛이 작용하였으며 각각의 갈변 요인들이 상호 작용함으로 서 고추장의 갈변에 관여함을 확인하였다. 고추장 추출물의 흡광도 변화에서는 고추장을 아세톤으로 추출하여 흡광도를 측정한 결과 $450{\sim}470$ nm에서, 물 추출물의 흡광도는 $200{\sim}205$ nm에서 가장 최고치를 나타내었다.

• 한국환경과학회지
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• 제27권9호
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• pp.753-762
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• 2018

The present study set out to investigate the adsorption of Cd(II) ions in an aqueous solution by using Peanut Husk Biochar (PHB). An FT-IR analysis revealed that the PHB contained carboxylic and carbonyl groups, O-H carboxylic acids, and bonded-OH groups, such that it could easily adsorb heavy metals. The adsorption of Cd(II) using PHB proved to be a better fit to the Langmuir isotherm than to the Freundlich isotherm. The maximum Langmuir adsorption capacity was 33.89 mg/g for Cd(II). The negative value of ${\Delta}G^o$ confirm that the process whereby Cd(II) is adsorbed onto PHB is feasible and spontaneous in nature. In addition, the value of ${\Delta}G^o$ increase with the temperature, suggesting that a lower temperature is more favorable to the adsorption process. The negative value of ${\Delta}H^o$ indicates that the adsorption phenomenon is exothermic while the negative value of ${\Delta}S^o$ suggests that the process is enthalpy-driven. As an alternative to commercial activated carbon, PHB could be used as a low-cost and environmentally friendly adsorbent for removing Cd(II) from aqueous solutions.

• 대한한방체열의학회지
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• 제3권1호
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• pp.1-5
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• 2004

This study examined the relationship between aminotransferase and DITI in the diagnosis of Liver Qi stagnation. An analysis was performed on the thermographic findings of 17 subjects with abnormally high aminotransferase value and 26 with no problem in blood sample at the Kangnam Korean Hospital, KyungHee University, Seoul, Korea, from March 2003 to May 2003. The body temperature was assessed by DITI thermographic measurements were performed on Rt. and Lt. subcostal area. Value of ${\delta}T$ and absolute value of ${\delta}T$ were tested by Mann-whitney U test. The absolute value of ${\delta}T$ was statistically significant(P<0.00). The ${\delta}T$ was also significant(P<0.01) and the temperature of Rt. area was higher than that of Lt. area. It is believed that DITI may be a favorable alternative to the diagnosis of Liver Qi stagnation.