Proceedings of the Korean Magnestics Society Conference (한국자기학회:학술대회 개요집)
The Korean Magnetics Society (KMS)
- Semi Annual
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- 2233-9485(pISSN)
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- 2233-9574(eISSN)
Domain
- Physics > Particle Physics/Field Theory
2000.09a
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Park, Stuart in;M. Samant;D. Monsma;L. Thomas;P. Rice;R. Scheuerlein;D. Abraham;S. Brown;J. Bucchigano 5
MRAM, High performance MRAM using MTJS demostrated, fully integrated MTJ MRAM with CMOS circuits, write time ~2.3 nsec; read time ~3 nsec, Thermally stable up to ~350 C, Switching field distibution controlled by size & shape. Magnetic Tunnel Junction Properties, Magnetoresistance: ~50% at room temperature, enhanced by thermal treatment, Negative and Positive MR by interface modification, Spin Polarization: >55% at 0.25K, Insensitive ot FM composition, Resistance$\times$ Area product, ranging from ~20 to 10$^{9}$ $\Omega$ (${\mu}{\textrm}{m}$ )$^{2}$ , Spin valve transistor, Tunnel injected spin polarization for "hot" electrons, Decrease of MTJMR at high bias originates from anode. -
Demonstrated uniform MR and resistance across 6 inch wafer, Demonstrated successful integration of MTJ and CMOS, Measured address access time of 8ns and read cycle time of 18ns for 256
${\times}$ 2 arrays at 3.0V using a single transistor and MTJ for a cell -
Developed two GMR memory architectures, 1R/0T for high density applications, 2R/5T for high speed applications, Embedded GMR technology shall offer rad hard community, Dynamic Reprogrammability, Rapid System Reconfigurability, Code modification in flight, Embedded GMR technology is promising for commercial applications
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A novel system of magneto-optical microscope magnetometer (MOMM), capable of simultaneous local problems of magnetic properties as well as real-time magnetic domain evolution imaging of ferromagnetic thin films with 400-nm spatial resolution, New findings in domain reveral dynamics of Co-based multilayers: The reversal ratio of V/R is a governing physical parameter. The activation volumes of wall-motion and nucleation processes are generally unequal. Submicron-scale local coercivity variation determines domain reversal dynamics. A thermally activated relaxation process during domain reversal is existed on the submicron-scale in realistic films. Local variation of magnetic properties should be considered for a realistic simulation. The fantastic capabilities of the MOMM can open many possibilities to broaden and deepen our understanding of domain reversal phenomena in ferromagnetic thin films.
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The reflection-amplitude approximation is used to calculate the interlayer exchange coupling in (001) Co/Cu/Co multilayers. The dependence of the phase factor of the reflection amplitude on the energy and wave vector is included. The contribution of each period is calculated and the results are compared with those from the asymptotic behavior. It is shown that the energy and wave-vector dependence of the phase factor may affect the interlayer exchange coupling significantly.
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We have investigated the activation magnetic moment, which characterizes the basis magnetic moment acting as a single magnetic particle during magnetization reversal. The activation magnetic moment was measured from each local area on continuous ferromagnetic thin films, by analyzing the magnetic field dependence of magnetization reversal of the corresponding local area based on a thermally activated relaxation process. It was found that the activation magnetic moment was nonuniform on submicrometer scale; the fluctuation increased with increasing the number of layers in Co/Pd multilayers. The distribution could be well analyzed by exp(
$\delta$ m$\^$ 3/2/), where$\delta$ m is the deviation of the activation magnetic moment from the mean value. -
Soft x-ray standing waves produced by a multilayer interference substrate add depth-sensitivity to magnetic circular dichroism to resolve changes in Co magnetism across a 10
${\AA}$ distance from the Co center to the Co-Pd interface of a Pd/Co/Pd trilayer having in-plane magnetization. Large enhancements of in-plane orbital and spin magnetic moments, as well as the number of d holes, are strongly localized in thin interface layer. These results provide new insight into the phenomenon of magnetic anisotropy at buried interfaces, and suggest a broad applicability of such standing wave measurements to interface magnetism studies. -
The permalloy soft magnet was produced by powder injection molding process. Rheological characteristics of mixtures, debinding conditions and the magnetic properties of permalloy after sintering ware investigated. The permalloy soft magnet with a permeability of 14200 could be obtained by preparing a mixture with a powder loading of 65.4 vol.% and PP/PEG binder system, solvent extraction, thermal debinding and subsequent sintering at 1350
$^{\circ}C$ in hydrogen. The permalloy soft magnet sintered in hydrogen showed a 95 % of theoretical density and a magnetic induction of 13.2 kG at the applied magnetic field of 50 Oe -
Magnetic Fe nanoparticles were synthesized by CVC process using Fe(CO)
$\sub$ 5/ as precursors. The nanoparticles have core-shell structures with uniform dispersion. For the specific purposes, the micostructures as well as the magnetic states of Fe nanoparticles can be controlled by adjusting the process parameters, such as the carrier gases, the decomposition temperature, the cooling of powder, etc. -
We present the magnetisation reversal dynamics of epitaxial Fe thin films grown on GaAs(001) and InAs(001) studied as a function of field sweep rate in the range 0.01-160 kOe/s using magneto-optic Kerr effect (MOKE). For 55 and 250
${\AA}$ Fe/GaAs(001), we find that the hysteresis loop area A follows the scaling relation A ∝ H$\^$ ${\alpha}$ / with${\alpha}$ =0.03∼0.05 at low sweep rates and 0.33-0.40 at high sweep rates. For the 150${\AA}$ Fe/InAs(001) film,${\alpha}$ is found to be ∼0.02 at low sweep rates and ∼0.17 at high sweep rates. The differing values of${\alpha}$ are attributed to a change of the magnetisation reversal process with increasing sweep rate. Domain wall motion dominates the magnetisation reversal at low sweep rates, but becomes less significant with increasing sweep rate. At high sweep rates, the variation of the dynamic coercivity H$\sub$ c/ is attributed to domain nucleation dominating the reversal process. The results of magnetic relaxation studies for easy-axis reversal are consistent with the sweeping of one or more walls through the entire probed region (∼100$\mu\textrm{m}$ ). Domain images obtained by scanning Kerr microscopy during the easy cubic axis reversal process reveal large area domains separated by zigzag walls. -
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Jang, S.D.;P. Tenaud;H.Cano;E. Brando;F. Kools;A. Morel;R. Grossinger;J.M. Lebreton;J. Tehillet 247
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$m_{2}$ F$e_{17}$ $N_{x}$ film magnets using a S$m_{2}$ F$e_{17}$ target were prepared at$N_{2}$ gas atmosphere using a Nd-YAG laser ablation technique. The effect of nitrogen pressure, deposition temperature, pulsation time and film thickness on the structure and magnetic properties of S$m_{2}$ F$e_{17}$ $N_{x}$ film were studied. Increasing the nitrogen pressure up to 5 atm. was confirmed to lead the formation of complete S$m_{2}$ F$e_{17}$ $N_{x}$ compound. Optimized magnetic properties with the nitrogenation temperature ranging over 500-53$0^{\circ}C$ could be obtained by extending the nitrogenation time up to 4 hours. Relatively low coercivities of 400~600 Oe were exhibited from the S$m_{2}$ F$e_{17}$ $N_{x}$ films having the thickness of 50~100 nm while 4$\pi$ $M_{s}$ of 10~12 kG could be achieved. In-plane anisotropic characteristic, which was the basic goal in this study, was achieved by controlling the nitrogenation parameters.ameters.ers.ameters. -
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Oxygen-plasma effects of single crystal and thin film samples of L
$a_{0.7}$ C$a_{0.3}$ Mn$O_{3-}$ $\delta$ / have been studied. Our resistivity measurements indicate that oxygen plasma treatment gives rise to oxygen diffusion into bulk regions, which results in a decrease of M$n^{3+}$ concentration in oxygen nonstoichiometric L$a_{0.7}$ C$a_{0.3}$ Mn$O_{3-}$ $\delta$ / and in the activation energies of Holstein's small polarons in the paramagnetic region.n.egion.n.n. -
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Magnetic field dependence of magnetization reversal in Co/Pt multilayers has been quantitatively investigated. Serial samples of Co/Pt multilayers have been prepared by dc-magnetron sputtering under various Ar pressure. Magnetization reversal was monitored by magnetization viscosity measurement and direct domain observation using a magneto-optical microscope system, and the wall-motion speed and the nucleation rate R were determined using a domain reversal model based on time-resolved domain reversal patterns. Both and R were found to be exponentially dependent on the reversing applied field. From the exponential dependencies, the activation volumes of the wall motion and nucleation could be determined based on a thermally activated relaxation model, and the wall-motion activation volume was revealed to be slightly larger than the nucleation activation volume.
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We have developed a three-axis configurational in situ SMOKE apparatus by which three-dimensional vector magnetization reversal processes are studied for ultrathin Co films grown on a Pd (111) single crystal in the thickness range of spin-reorientation transition. This study provides a better understanding of magnetization reversal motions with the knowledge of 3 components of magnetization vector at the transition of an easy axis of magnetization from the film normal at 5 ML Co to in-plane at 6 ML Co (ML notes monolayer). For a 5.25 ML Co, it was observed that a slightly canted magnetization vector from the film normal rotated in the film plane under an applied field direction parallel to the film normal.
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In order to study the effect of the magnetic anisotropy on the giant magnetoresistance (GMR), the angle dependent magnetoresistance (MR) was measured. The experimental results show that the maximum MR ratio depends on the angle between the direction of the applied field and that of the easy axis. The angular modulation of the MR ratio can be explained by the alignments of the two 'effective' magnetization vectors that are bound to their own easy axes. The typical property of MR loops at 2
$\^$ nd/ antiferromangtic maximum (AFM) such as two maxima was discussed in relation with the magnetic anisotropy (MA). The simulated results under an assumption of the two in-plane easy axes, which exist in the sample, were compared with the experiments. -
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Low temperature diagnosis was performed as a probe for the integrity of MTJ(Magnetic tunnel junction) process which is optimised for the given plasma oxidation condition. TMR ratio increased slowly with decreasing temperature than that expected from spin wave exitation theory〔1〕. Junction resistance (RJ) does not follow T
$\^$ -$\frac{1}{2}$ / law below 200 K, indicating another conduction path besides spin polarized tunneling is involved at low temperature. Temperature dependence of conductance dip and bias dependence of TMR with temperature are discussed, from which the quality of tunnel barrier and its formation process can be inferred. -
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The spontaneous Hall effect in amorphous Tb-Fe and Sm-Fe thin films, which possess excellent magnetic softness, is investigated in this work to seek a possibility of practical applications of these thin films as sensors. The resistivity of Tb-Fe thin films ranges from 180 to 250 Ωcm as the Tb content varies from 35 to 46 at. %. Tb-Fe thin films show negative Hall resistivity ranging from - 7.3 to - 5.0 Ωcm in the same composition range, giving the normalized resistivity ratio in the range of -4.1 to -2.0 %. On the other hand, the resistivity of Sm-Fe thin films ranges from 150 to 166 Ωcm as the Sm content varies from 22 to 31 at. %. Sm-Fe thin films show positive Hall resistivity which varies from 7.1 to 2.8 Ωcm in the same composition range, giving the normalized resistivity ratio in the range of 4.8 to 1.7 %. These values are significantly high compared with the values of other R-T alloys, Tb-Co alloys for example, where the highest reported value is 2.5 %. Between the two different sets of samples, Tb-Fe thin films with perpendicular anisotropy are considered to be more suitable for practical applications, since saturation is reached at a los magnetic field, approximately 2 kOe in a Tb
$\sub$ 35.1/ Fe$\sub$ 64.9/ thin film, for example. -
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In this study, effects of novel VMn underlayer on magnetic properties of CoCrPt/VMn longitudinal medium was studied and compared with those of CoCrPt/Cr medium. It was found that the VMn film had (200) preferred orientation and the lattice constant was about 0.2967 nm, which is slightly larger than that of the Cr, 0.2888 nm. The grain size of VMn film was 9.3 nm at 30 nm thickness, and this is about 38 % smaller than that of a similarly deposited Cr film. The CoCrPt/VMn films showed higher coercivity in comparison with the CoCrPt/Cr films. The coercivity increase seems to be attributed to the increased Co (11.0) texture, improved lattice matching between Co (11.0) and VMn (200), and lower stacking fault density. Mn must have diffused into the CoCrPt magnetic layer more uniformly rather than preferentially along grain boundaries this reduced Ms at higher substrate temperature
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A study on magnetic layer thickness effects on magnetic properties of CoCrPt/Ti perpendicular media.Change of magnetic properties in CoCrPt/Ti perpendicular media with varying CoCrPt films thickness has been studied. As CoCrPt films thickness increase, the Ms(magnetization saturation) drastically increases at thinner thickness and gradually increases with further increase in thickness from 25nm. This Ms behaviour is associated with primarily the formation of "amorphous-like" reacted layer by intermixing of CoCrPt and Ti at CoCrPt/Ti interface and secondarily change of Cr segregation mode with varying the CoCrPt films thickness. Magnetic domain structure distinctively changes with increasing CoCrPt magnetic layer(ML) thickness. Also the strength of exchange coupling measured from the slope in demagnetizing region in M-H loop changes with ML thickness. Details of the above magnetic properties will be discussed. The expansion of lattice parameters a and c at thinner thickness suggests that Cr segregation mode may be connected with the residual stress of the films. Finally, negative nucleation field(Hn) behaviour with the exchange slope will be reported.
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By applying Current-applied Pressure-Assisted process, we could obtain full dense isotropic and anisotropic NdFeB magnets from rapidly quenched MQP-A powder. The Nd contents are found to play an important role during the CA-press and CA-deformation process. The (BH)
$\sub$ max/ of CA-pressed and CA-deformed magnets are 131 kJ/㎥(16.5 MGOe) and 352 kJ/㎥(44.2 MGOe), respectively. The texture of CA-deformed anisotropic NdFeB magnets with thickness reduction was investigated by pole figure, and the (006) texture was increase with the increase of thickness reduction. With the increment in thickness reduction from 50%, 60% to 80%, W$\sub$ 50/ decreases from 76$\^$ $^{\circ}$ /, 62.5$\^$ $^{\circ}$ / to 17$\^$ $^{\circ}$ /, respectively. -
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The magnetic alloy of
$Nd_{2}Fe_{14}B$ -type was synthesized by a mechano-chemical method, including the processes of spray-drying, de-binding, milling,$H_{2}$ - and Ca-reduction and washing. The very fine$Nd_{2}Fe_{14}B$ particles smaller than$1\mu\textrm{m}$ could be achieved without the inevitable pulverization step in conventional processes. -
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Hopkinson effect in the HDDR-treated Nd
$\sub$ 15/Fe$\sub$ 77/B$\sub$ 8/ alloy was examined in detail by means of a thermomagnetic analysis with low magnetic field (600 Oe). The emergence and magnitude of maximum in magnetisation in the thermomagnetic curve due to the Hopkinson effect was correlated to the grain structure and coercivity of the HDDR-treated material. the HDDR-treated materials showed clear Hopkinson effect (maximum in magnetisation just below the Curie temperature of the Nd$\sub$ 2/Fe$\sub$ 14/B phase) on heating in the thermomagnetic curve. Magnitude of the magnetisation rise due to the Hopkinson effect became smaller as the recombination time increased. The magnetisation recovery at room temperature on cooling from above the Curie temperature became smaller as the recombination time increased. The HDDR-treated materials with shorter recombination time, finer grain size and higher coercivity showed larger magnetisation maximum due to Hopkinson effect in the thermomagnetic curve. -
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Cheju Island has nature of typical trass through volcanic activities in many times. The soil in Cheju Island has principally sprung from basalt and partially made up of trachyte, trachyte's nature and site. Also ancient relics, plain coarse pottery's kilns and pantiles kilns are homogeneously distributed all over the Cheju Island. In this study, as a result of X-ray fluorescence spectrometer and Mossbauer spectroscopy of a sample are from plain coarse pottery and pantiles in 5 regions of Cheju Island. It is thought that these samples are partially formed from neutral volcanic rock like trachyte and Atomicity state of iron is almost Fe
$\^$ 3+/. Also the magnetic hyperfine field length of goethite, contained these samples is less than synthetic goethite magnetic hyperfine field length and this result shows that disintegration of inner magnetic order, created by partial substitution of diamagnetic positive ion containing Fe$\^$ 3+/ and Al$\^$ 3+/ in goethite lattice. -
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Barium ferrite particles were synthesized from Ba(NO
$_3$ )$_2$ , Fe(NO$_3$ )$_3$ and KOH mixed solutions using hydrothermal crystallization in supercritical water. The experimental apparatus for production of barium ferrite is a flow-type apparatus. Fine barium ferrite particles were produced because supercritical water causes the metal hydroxides to be rapidly dehydrated before significant growth takes place. The effects of Fe/Ba ratio and reaction time on the formation, particle size, and magnetic properties of barium ferrite were studied. When Fe/Ba ratio were varied from 0.5 to 12, single-phase barium ferrite powder was only produced in the range of 0.5〈Fe/Ba〈2. Also, with elevating reaction time, the BaO.6Fe$_2$ O$_3$ particle size grew smaller. Especially, uniform barium hexaferrite particles of size 100-200nm were obtained at 80sec. In this study, therefore, single-phase barium ferrite particles are highly stable and can be produced continuously in a reaction time of less then 2min. -
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We have investigated electronic structuresof antiferromagnetic YBaCo_2O_5 using the local spin-density approximation (LSDA) + U method. The charge and orbital ordered insulating ground state is correctly obtained with the strong on-site Coulomb interaction. Co^{2+} and Co^{3+} ions are found to be in the high spin (HS) and intermediate spin (IS) state, respectively. The tetragonal to orthorhombic structural transition is responsible for the ordering phenomena and the spin states of Co ions. The large contribution of the orbital moment to the total magnetic moment indicates that the effect of the spin-orbit coupling is very important in YBaCo_2O_5.
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The extremely soft magnetic behaviors in the nanocrystalline Fe
$_{81}$ B$_{11}$ Nb$_{7}$ Cu$_{1}$ alloy annealed at 450$^{\circ}C$ and 550$^{\circ}C$ for 1 hour respectively in a vacuum were obtained, and examined by means of the magnetoimpedance(MI) effect and the incremental permeability. Because the MI effect can be obtained only in ultra-soft magnetic materials, the improvement of magnetic softness by proper thermal treatment was carefully monitored by the MI effect for all annealed samples. The changes of the incremental permeability as a function of an external field were also measured to verify the magnetic softness along with the MI measurement.ent. -
The nanocrystalline Fe
$_{84}$ Zr$_{7}$ B$_{6}$ Cu$_{1}$ $Al_{2}$ alloy was annealed at 450$^{\circ}C$ and 550$^{\circ}C$ for l hour to achieve the ultra-soft magnetic properties such as large magnetoimpedence ratio(MIR), the incremental permeability ratio(PR), nearly zero coercivity, zero magnetostriction, etc. The PR and MIR of the sample were measured from 100 kHz to 10 MHz at a cryogenic chamber where the temperature can be varie from 10 K to 300 K. The increment of MIR value is proportional to increasing temperature. The maximum PR values measured at high frequency above 1 MHz remain almost same despite of the temperature variation from 10 K to 300 K except the sharpness in PR curves. However, the maximum PR values measured below 1 MHz show drastic increment at above 150K due to thermal activation of magnetic domains.s.s. -
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Co-Ni-Fe-N thin films were fabricated by a N
$\sub$ 2/ reactive rf magnetron sputtering method. The nitrogen partial pressure (P$\sub$ N2/) was varied in the range of 0∼10%. As P$\sub$ N2/ increases in this range, the saturation magnetization (B$\sub$ s/) linearly decreases from 19.8 kG to 14 kG and the electrical resistivity ($\rho$ ) increased from 27 to 155${\mu}$ $\Omega$ cm. The coercivity (H$\sub$ c/) exhibits the minimum value at 4% of P$\sub$ N2/. The magnetic anisotropy (H$\sub$ k/) are in the range of 20∼50 Oe. High frequency characteristics of (Co$\sub$ 22.2/Ni$\sub$ 27.6/Fe$\sub$ 50.2/)$\sub$ 100-x/N$\sub$ x/ films are excellent in the range of 3∼5% of P$\sub$ N2/. Especially the effective permeability of the film fabricated at 4% of P$\sub$ N2/ is 800, which is maintained up to 600 MHz. This film also shows Bs of 17.5 kG, H$\sub$ c/ of 1.4 Oe, resistivity of 98$\Omega$ cm and H$\sub$ k/ of about 25 Oe. Also, the corrosion resistance of (Co$\sub$ 22.2/Ni$\sub$ 27.6/Fe$\sub$ 50.2/)$\sub$ 100-x/N$\sub$ x/ were improved with the increase in N concentration. -
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We present a new procedure to evaluate the residual life of 1Cr-1Mo-0.25V steel by reversible magnetic permeability. The method is based on the existence of the first harmonics in the differential magnetization around the coercive force. The apparatus is based on the detection of the voltage induced in a coil using a lock-in amplifier tuned to a frequency of the exciting one. Results obtained for the first harmonics and Vickers hardness on the aged samples show that the peak interval of reversible permeability and Vickers hardness decrease as ageing time increases. The correlation between Vickers hardness and the peak interval of the reversible permeability could well be used to evaluate the residual life of 1Cr-1Mo-0.25V steel, nondestructively.
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A double rectangular spiral inductor is fabricated using FeTaN films. The inductor is composed of internal coils sandwiched by magnetic layers. Characteristics of inductor performance are investigated with an emphasis on planarization of magnetic films. In the absence of the planarization process, the grating topology of upper magnetic films over coil arrays degrades the soft magnetic properties and the inductor performance. It also induces a longitudinal magnetic anisotropy with the easy axis aligned to the magnetic flux direction. This alignment prevents the upper magnetic films from contributing to the total induction. Glass bonding is a viable method for achieving a completely planar inductor structure. The planar inductor with glass bonding shows excellent performance : inductance of 1.1 H, Q factor of 7 (at 5 MHz), and the dc current capability up to 100 mA.
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This paper describes the design method of the magnetic system to maximize the magnetic flux leakage (MFL) in non-destructive testing (NDT) system. The defect signals in MFL type NDT system mainly depends on the change of the magnetic leakage flux in the region of defect. The characteristics of the B-H curves are analyzed and the design method to define the operating point in B-H curves for the maximum leakage is performed. The computed MFL signal by nonlinear finite element method is verified by measurement using Hall sensors mounted on the 6 legs PIG in the 8 inches test tube with defects. The rhombic defects could be successfully composed from the defect signals.
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This paper describes the design and evaluation of a noise suppressing hydrophone that is robust to external noise without sacrificing its performance as a receiver. To increase robustness of the receiver to the external noise, first, effects of location of external noise on its performance are analyzed with the finite element method (FEM). Based on the results, geometrical variations are implemented on the structure with additional air pockets and damping layers that work as acoustic shields or scatterers of the noise, and fourteen trial models are developed for the noise suppressing hydrophone structures. The results show that the effect of the external noise is most significant when it is applied to near the mid-side surface of the hydrophone housing. The external noise is isolated most efficiently when two thin damping layers combined with five air pockets are inserted to the circumference of the hydrophone housing. Overall, of the fourteen structural variations of the hydrophone, the best one shows about 87% reduction in the response of the original structure to external noise.
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Electronic structures of ordered Fe$_3X (X = Al, Si), and their derivative ternary alloys of Fe_2TX (T = 3d transition metal) have been investigated by using the linearized muffin-tin orbital (LMTO) band method. The role of the coupling between substituted transition metal and its neighbors is investigated by calculating the magnetic moments and local density of states (LDOS). It is shown that it is essential to include the coupling beyond nearest neighbors in obtaining the magnetic moment of Fe alloy. The preferential sites of T impurities in Fe_3X are determined from the total energy calculations. The derivative ternary alloys of Fe_2TX have characteristic electronic structures of semi-metal for Fe_2VAI and (nearly) half-metal for Fe_2TAI (T = Cr, Mn) and Fe_2TSi (T = V, Cr, Mn)