Journal of Energy Engineering (에너지공학)

The Korean Society for Energy (한국에너지학회)
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Hydrothermal Synthesis of Fe Based MOFs with Energy Economy Approach

  • Israr, Farrukh (Department of Nuclear and Energy Engineering, Jeju National University) ;
  • Kim, Duk Kyung (Department of Chemistry, Auburn University Montgomery) ;
  • Kim, Yeongmin (Department of Nuclear and Energy Engineering, Jeju National University) ;
  • Oh, Seung Jin (Mechanical Engineering Department, National University of Singapore) ;
  • Ng, Kim Choon (Mechanical Engineering Department, National University of Singapore) ;
  • Chun, Wongee (Department of Nuclear and Energy Engineering, Jeju National University)
  • Received : 2015.04.24
  • Accepted : 2015.06.11
  • Published : 2015.06.30
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Abstract

The mesoporous metal organic framework structure Fe-BTC was successfully synthesized by hydrothermal process with noticeable yield. The synthesis operation was conducted at intermediate temperature and for shortened operation time as compared to conventional procedures. This process approach with reduced operating temperature and shortened operation time may open an opportunity window towards process economy with reduction in energy consumption. A simple mathematical approach of diffraction indexing using X-ray diffraction patterns of synthesized powder was employed to confirm its crystalline nature and to investigate its high temperature stability. The crystallite size was calculated by using Debye-Scherrer equation.

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