Journal of Energy Engineering (에너지공학)

The Korean Society for Energy (한국에너지학회)
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Cost effective and low energy consuming hydrothermal synthesis of Ni based MOF

  • Israr, Farrukh (Department of Nuclear and Energy Engineering, Jeju National University) ;
  • Kim, Duk Kyung (Department of Chemistry, Auburn University Montgomery) ;
  • Kim, Yeongmin (Department of Nuclear and Energy Engineering, Jeju National University) ;
  • Oh, Seung Jin (Mechanical Engineering Department, National University of Singapore) ;
  • Ng, Kim Choon (Mechanical Engineering Department, National University of Singapore) ;
  • Chun, Wongee (Department of Nuclear and Energy Engineering, Jeju National University)
  • Received : 2015.04.24
  • Accepted : 2015.06.12
  • Published : 2015.06.30
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Abstract

The mesoporous metal organic framework structure of Ni-BTC was successfully synthesized in a low temperature and short operation time via hydrothermal synthesis process. Such operational route virtuously consumed less electrical and thermal energy. It proved time saving along with acceptable product yield (38%). The product was characterized through FESEM, FT-IR, XRD and $N_2$ gas adsorption measurement. Hightemperature stability of synthesized MOF was gauged by diffraction indexing of XRD patterns of as synthesized and heat treated samples of MOFs. The mathematically calculated particle size of Ni-BTC was found to be 42nm.

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References

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