폐기물 매립지 토양에서의 PCBs 분석법

  • 이정화 (한국지질자원연구원 지질환경재해연구부) ;
  • 전치완 (한국지질자원연구원 지질환경재해연구부) ;
  • 정영욱 (한국지질자원연구원 지질환경재해연구부)
  • Published : 2005.04.01

Abstract

This paper describes a simple procedure for the quantitative analysis of 7 PCBs (polychlorinated biphenyls) in soils on the waste reclaimed land, The procedure involved sample clean up using silicagel column, acetonitrile partition and sulfuric acid procedures. The instrumental technique is applied GC/PDD(gas chromatography/pulsed discharge detector) and GC/ECD(gas chromatography/electron capture detector). Concentration of $sub-{\mu}g/g$ level was attainable with 20g soils on the waste reclaimed land.

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