• Journal of the Korean earth science society
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• v.43 no.3
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• pp.405-429
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• 2022

Detrital zircon LA-MC-ICP-MS U-Pb dating of the Cretaceous Gurye Group, Gurye Basin, was carried out. Gurye Group consists of Supyeongri, Geumjeongri, Togeum, and Obongsan formations in ascending order, and five samples were collected for age dating. Based on the dating results, the lowermost Supyeongri and the uppermost Obongsan formations show narrow age ranges. Only Precambrian and Late Cretaceous zircons were found in the Supyeongri and Obongsan formations, respectively. However, the upper and lower Geumjeongri, and Togeum formations show wide age ranges from the Precambrian to Cretaceous. The youngest detrital zircon U-Pb ages of each formation except the Supyeongri Formation, which lacks Cretaceous zircon, were calculated to be ca. 107.4 Ma in the lower Geumjeongri Formation, ca. 104.6 Ma in the upper Geumjeongri Formation, ca. 97.7 Ma in the Togeum Formation, and ca. 88.5 Ma in the Obongsan Formation. Such results indicate that the depositional age of the Gurye Group can be constrained from the Lower Cretaceous Albian to the Upper Cretaceous Coniacian. Based on the distribution of the detrital zircon ages from each formation, the source area of the Gurye Group is interpreted to have been extended from the adjacent Youngnam Massif to the Okcheon Belt throughout the basin evolution. The increase of the Cretaceous zircon with time is thought to reflect the slab roll-back of the proto-Pacific plate during the Cretaceous.

• The Journal of the Petrological Society of Korea
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• v.25 no.1
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• pp.29-37
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• 2016

A "granite boulder", ~70 cm in size, was reported from the Geumgang Limestone, and has been considered as a glaciogenic dropstone. Since this interpretation has enormous implications for unraveling the evolution history of the Ogcheon Metamorphic Belt, we re-examined the contact relationship and structure of the "granite boulder", and estimated its emplacement age based upon SHRIMP U-Pb zircon dating. The weighted mean $^{206}Pb/^{238}U$ age pooled from 6 spot analyses of two specimens is $170{\pm}2Ma$ ($2{\sigma}$, MSWD=2.2). This zircon age suggests that the "granite boulder" in the Geumgang Limestone is a part of Jurassic granite, rather than a glaciogenic dropstone.

• The Journal of the Petrological Society of Korea
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• v.25 no.4
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• pp.401-407
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• 2016

The SHRIMP zircon U-Pb age dating was carried out for the age-unknown Haeinsa Granite located in the middle Yeongnam Massif. SHRIMP zircon U-Pb age determinations of 7 samples from the Haeinsa Granite in Geochang area show two age groups. Ages from 5 samples (M-3-1, H-1, 3, 5, 10) are $192.4{\pm}1.4{\sim}195.5{\pm}1.9Ma$, whereas ages from 2 samples (H-11 and 12) are $187.7{\pm}3.3Ma$ and $188.2{\pm}3.6Ma$, respectively.

• Journal of the Mineralogical Society of Korea
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• v.26 no.3
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• pp.161-174
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• 2013

The geology of the weondong deposit area consists mainly of Cambro-Ordovician and Carboniferous-Triassic formations, and intruded quartz porphyry and dyke. The skarn mineralized zone in the weondong deposit is the most prospective region for the useful W-mineral deposits. To determine the skarn-mineralization age, U-Pb SHRIMP and K-Ar age dating methods were employed. The U-Pb zircon ages of quartz porphyry intrusion (WD-A) and feldspar porphyry dyke (WD-B) are 79.37 Ma and 50.64 Ma. The K-Ar ages of coarse-grained crystalline phlogopite (WD-1), massive phlogopite (WDR-1), phlogopite coexisted with skarn minerals (WD-M), and vein type illite (WD-2) were determined as $49.1{\pm}1.1$ Ma, $49.2{\pm}1.2$ Ma, $49.9{\pm}3.6$ Ma, and $48.3{\pm}1.1$ Ma, respectively. And the ages of the high uranium zircon of hydrothermally altered quartz porphyry (WD-C) range from 59.7 to 38.7 Ma, which dependson zircon's textures affected by hydrothermal fluids. It is regarded as the effect of some hydrothermal events, which may precipitate and overgrow the high-U zircons, and happen the zircon's metamictization and dissolution-reprecipitation reactions. Based on the K-Ar age datings for the skarn minerals and field evidences, we suggest that the timing of W-skarn mineralization in weondong deposit may be about 50 Ma. However, for the accurate timing of skarn mineralization in this area, the additional researches about the sequence of superposition at the skarn minerals and geological relationship between skarn deposits and dyke should be needed in the future.

• Journal of the Korean earth science society
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• v.45 no.1
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• pp.85-109
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• 2024

Detrital zircon U-Pb dating was performed to determine the depositional age and provenance of sediments in the Cretaceous Muju Basin in Muju-gun, Jeollabuk-do. Six samples were collected from the Seolcheon Tuff (SCT), Bangyiri Formation (BYR), Gobang Member of the Gilwangri Formation (GWR-G), Seochang Member of the Gilwangri Formation (GWR-S), Bukchang Member of the Gilwangri Formation (GWR-B), and Jeogsangsan Formation (JSS). Based on the dating results, the sedimentary strata of the Muju Basin were deposited for approximately 105.6-90.4 Ma corresponding to the Albian to Turonian. The youngest single zircon ages of about 94.4 Ma and 89.6 Ma were confirmed in the samples from the Bangyiri Formation and the Gobang Member of the Gilwangri Formation, respectively, distributed in the western part of the Muju Basin. The relative and numerical ages previously estimated based on the lithostratigraphic correlation of the Gilwangri conglomerate need to be revisited in further research. The results also suggest that most of the sediments filling the Muju Basin were supplied from a limited area adjacent to the basin.

• Journal of the Korean earth science society
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• v.42 no.1
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• pp.11-38
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• 2021

Detrital zircon U-Pb dating of samples from the Baekseoktan (Iljik Formation), Mananjaam (Jeomgok Formation), and Sinseongri (Sagok Formation) geosites in the Cheongsong Global Geopark were carried out to estimate the depositional age and provenance of the Hayang Group in the Gyeongsang Basin. In the Iljik Formation, Jurassic and Triassic zircons are dominant with minor Precambrian zircons, with no Cretaceous zircon. In contrast, the Jeomgok and Sagok formations show very similar age distributions, which have major age populations of Cretaceous, Jurassic, and Paleoproterozoic ages. The weighted mean ages of the youngest zircon age groups of the Jeomgok and Sagok formations are 103.2±0.3 and 104.2±0.5 Ma, respectively. Results suggest that the depositional ages of the Jeomgok and Sagok Formations are Albian. The detrital zircon age spectra indicate a significant change in provenance between the Iljik and Jeomgok formations. The sediments of the Iljik Formation are thought to have been supplied from nearby plutonic rocks. However, the Jeomgok and Sagok sediments are interpreted to have been derived from relatively young deposits of the Jurassic accretionary complex located in southwest Japan.

• The Journal of the Petrological Society of Korea
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• v.28 no.4
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• pp.237-249
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• 2019

The volcanic rocks around the Jayang caldera are classified in an order such as Jukjang Volcanics, Doil Rhyolite, Unjusan Tuff and Rhyolite intrusions. By the SHRIMP U-Pb zircon datings from zircons, eruption ages of the Unjusan Tuff are constrained as 66.65±0.96 Ma in the intracaldera, and 66.08±0.62 Ma in the extracaldera outflow, and intrusion age of the ring dike is investigated as 60.74±0.66 Ma. The age data indicate that the caldera was collapsed between 66.08 Ma and 60.74 Ma, just before the dike intruded after the explosive eruption of the Unjusan Tuff. The Jayang caldera shows the composite igneous process of a perfect volcanic cycle passing from ash-flow tuffs through caldera collapse into ring dikes in the Jayang area.

• The Journal of the Petrological Society of Korea
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• v.23 no.3
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• pp.209-220
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• 2014

SHRIMP zircon U-Pb age dating is carried out for the Yeongju and Andong granite batholiths intruding the Precambrian metamorphic complex and Paleozoic sedimentary formations within the NE Yeongnam Massif, Korea. Dating of zircons from a hornblende-biotite tonalite and an equigranular biotite granodiorite in the Yeongju granite has yielded ages of ca. 187 Ma and ca. 186 Ma, respectively. Also, dating of zircons from a biotite granodiorite and a very coarse-grained biotite granite in the Andong granite has yielded ages of ca. 182Ma and ca. 186Ma, respectively. These data indicate that the main intrusions of the Yeongju and Andong granite batholiths occur almost at the same age. The oldest age of ca. 194 Ma has been determined on zircons from a hornblende gabbro in the Andong granite, and the youngest age of 175 Ma is obtained from the Chunyang granite pluton, mainly consisting of fine-grained two-mica granite, of the Yeongju batholith. These results indicate that Jurassic Daebo magmatism in the Yeongju-Andong area, NE Yeongnam massif, started early at the Early Jurassic with an intrusion of mafic magma, and followed by an emplacement voluminous granite magma during the middle of the Early Jurassic, and was finalized with the emplacement of relatively small amount of much evolved granite magma at the end of Early Jurassic.

• The Journal of the Petrological Society of Korea
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• v.10 no.3
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• pp.179-189
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• 2001

The determination of trace concentration of U, Th and Pb was carried out for chemical dating of zircon and monazite by electron microprobe. Detection limit and error range should be considered to measure characteristic X-rays of M-line from those minerals, which are low in the ionization of atom and low peak intensity in the spectrum. The element of U, Th and Pb were simultaneously measured with 3 spectrometers equipped with PET crystal to reduce a total counting time and error due to drift of instrumental operating condition. Detection limit could be improved from increase of the peak/background ratio through adjusting pulse height analyzer about 1000 mv baseline. Under permissible maximum analytical conditions, theoretical detection limit of U, Th and Pb is down to 30 ppm (99% confidence level). The analytical result was maintained at a relative error $\pm$10% ($2{\sigma}$) in 800 ppm Pb, $\pm$5% ($2{\sigma}$) in 2330 ppm U and $\pm$10% ($2{\sigma}$) in dating from a single measurement of zircon at 15 keV and 100 nA. However, for the precise dating of zircon and monazite, if it is considered a 3 $\mu\textrm{m}$ spatial resolution, <100 ppm ($3{\sigma}$) detection limit and <$\pm$10% ($2{\sigma}$) relative error, optimum analytical conditions are given as 15~20 keV accelerating voltage, 100~200 nA beam current and 300~1200 sec total counting time. To reduce material damage by high current, there is need to be up to 3~5 $\mu\textrm{m}$ of electron beam diameter, or to use arithmetic average of multiple measuring at a shorter counting time. A younger or relatively low concentration rocks can be dated chemically by lower detection limit and improved precision resulted from increase of current and measuring time.

• Korean Journal of Mineralogy and Petrology
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• v.33 no.4
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• pp.339-347
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• 2020

We carried out the U-Pb age dating of zircon from basement rocks in the southern part of the Danyang National Geopark. Two migmatitic gneisses composed of biotite±sillimanite±garnet+feldspar+quartz were dated. Leucosomes in the samples were clearly distinguished from their melanosomes. The U-Pb isotopic compositions of zircon from sillimanite- and garnet-bearing migmatitic samples were measured using a secondary ion microprobe, yielding metamorphic ages, 1870±10 Ma (2σ)와 1863±6 Ma (2σ), respectively. 1.87~1.86 Ga metamorphic ages are consistent with those of the Paleoproterozoic low-P and high-T regional metamorphism (1.87~1.85 Ga) in the Yeongnam Massif. The maximum depositional age based upon the apparent 207Pb/206Pb ages of detrital zircon in the samples was estimated as 2.06 Ga, and thus sedimentation age of the protolith of the migmatitic gneisses ranges between 2.06 and 1.87 Ga.