• Title/Summary/Keyword: wetting angle

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The Effcts of Temperature and Ni Addition on the Wetting Behaviour of Cu on W (텅스텐판상에서 구리액상의 습윤거동에 미치는 온도 및 니켈 첨가의 효과)

  • 이재성
    • Journal of the Korean institute of surface engineering
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    • v.16 no.2
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    • pp.41-47
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    • 1983
  • An investigation has been performed on the effects of temperature and Ni addition on the wetting behaviour of Cu on W substrate in hydrogen atmosphere. An sessile drop method was used to measure a wetting angle. The concentration profiles of W, Cu and Ni elements in W/Cu - 5 Ni specimen were made by EPMA. With increasing temperature, the wetting angle of Cu droplet on W plate decreases and the time to reach an equilibrium wetting angle is shortened in hydrogen atmosphere. The addition of Ni improves appreciably the wettability of Cu on W. With increasing Ni content in Cu liquid droplet(0, 1, 3, 5%), the wetting angle is decreased from 21$^{\circ}$to 0$^{\circ}$.

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Effect of Wetting Angle and Powder Content on the Optical Properties of Self-Assembled SiO2 Photonic Crystals (기판의 접촉각과 분말량이 자기조립을 통해 형성된 SiO2 광자결정의 광특성에 미치는 영향)

  • O, Yong-Taeg;Kim, Myung-Soon;Shin, Dong-Chan
    • Journal of the Korean Ceramic Society
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    • v.42 no.7 s.278
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    • pp.497-502
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    • 2005
  • This study investigated the effects of the substrate and powder content on the fabrication of SiO$_{2}$ photonic crystals by evaporation method. Photonic crystals were self-assembled on quartz, Corning 1737 glass, slide glass, and ITa glass to verify the effects of the wetting angle and surface morphology. The powder contents of the solution were varied from 0.2 to 2.0 wt$\%$. The number of photonic crystal layers increased according to the decrease of wetting angle and surface roughness. The resultant photonic crystals showed the best optical characteristics when the number of photonic crystal layers was within 40 and 50. In addition, the intensity peak of Fabry¡?Perot fringes increased when the wetting angle was large and the particle size was small. Photonic crystals coated on ITO glass showed the highest reflectance peak of 63$\%$ relative intensity.

A Study on the Comparison of Solderability Assessment

  • Salam, B.;Ekere, N.N.;Jung, J.P.
    • Journal of the Korean institute of surface engineering
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    • v.35 no.2
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    • pp.129-137
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    • 2002
  • The purpose of solderability assessment is to predict the effectiveness of soldering process. It is important for companies pursuing zero defects manufacturing because poor solderability is the major cause of two third of soldering failures. The most versatile solderability method is wetting balance method. However, there exist so many indices for wettability in the wetting balance test e.g. time to reach 2/3 values of maximum wetting force, tine to reach zero wetting force, maximum withdrawal force. In this study, three solderability assessment methods, which were the maximum withdrawal force, the wetting balance and the dynamic contact angle (DCA), were evaluated by comparing each other. The wetting balance technique measures the solderability by recording the forces exerted from the specimen after being dipped into the molten solder. Then the force at equilibrium state can be used to calculate a contact angle, which is known as static contact angles. The DCA measures contact angles occurred during advancing and withdrawing of the specimen and the contact angles are known as dynamic contact angles. The maximum withdrawal force uses the maximum force during withdrawal movement and then a contact angle can be calculated. In this study, the maximum withdrawal force method was found to be an objective index for measuring the solderability and the experiment results indicated good agreement between the maximum withdrawal force and the wetting balance method.

The Fluxless Wetting Properties of UBM-Coated Si-Wafer to the Pb-Free Solders (UBM이 단면 증착된 Si-Wafer에 대한 Pb-free 솔더의 무플럭스 젖음 특성)

  • 홍순민;박재용;김문일;정재필;강춘식
    • Journal of Welding and Joining
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    • v.18 no.6
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    • pp.74-82
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    • 2000
  • The fluxless wetting properties of UBM-coated Si-wafer to the binary lead-free solders(Sn-Ag, Sn-Sb, Sjn-In, Sn0Bi) were estimated by wetting balance method. With the new wettability indices from the wetting curves of one side coated specimen, the wetting property estimation of UBM-coated Si-wafer was possible. For UBM of Si-chip, Au/Cu/Cr UBm was better than au/Ni/TI in the point of wetting time/ At general reflow process temperature, the wettability of high melting point solders(Sn-Sb, Sn-Ag) was better than that of low melting point one(Sn-Bi, Sn-In). The contact angle of the one side coated Si-plate to the solder could be calculated from the force balance equation by measuring the static state force and the tilt angle.

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The Fluxless Wetting Properties of TSM-coated Glass Substrate to the Pb-free Solders (TSM(Top Surface Metallurgy)이 증착된 유리기판의 Pb-free 솔더에 대한 무플럭스 젖음 특성)

  • 홍순민;박재용;박창배;정재필;강춘식
    • Journal of the Microelectronics and Packaging Society
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    • v.7 no.2
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    • pp.47-53
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    • 2000
  • The fluxless wetting properties of TSM-coated glass substrate were evaluated by the wetting balance method. We could estimate the wettability of the TSM with new parameters obtained from the wetting balance test for one side-coated specimen. It was more effective in wetting to use Cu as a wetting layer and Au as a protection layer than to use Au itself as a wetting layer. The SnSb solder showed better wettability than SnAg, SnBi, and SnIn solders. The contact angle of the one side-coated glass substrate to the Pb-free solders could be calculated from the farce balance equation by measuring the static force and the tilt angle.

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Effects of Mg-Al Alloy and Pure Ti on High Temperature Wetting and Coherency on Al Interface Using the Sessile Drop Method (정적법을 이용한 Mg-Al계 합금과 순수 Ti의 고온 젖음현상 및 Al계면에서의 정합성에 미치는 영향)

  • Han, Chang-Suk;Kim, Woo-Suk
    • Korean Journal of Materials Research
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    • v.31 no.1
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    • pp.38-42
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    • 2021
  • In this study, high temperature wetting analysis and AZ80/Ti interfacial structure observation are performed for the mixture of AZ80 and Ti, and the effect of Al on wetting in Mg alloy is examined. Both molten AZ80 and pure Mg have excellent wettability because the wet angle between molten droplets and the Ti substrate is about 10° from initial contact. Wetting angle decreases with time, and wetting phenomenon continues between droplets and substrate; the change in wetting angle does not show a significant difference when comparing AZ80-Ti and Mg-Ti. As a result of XRD of the lower surface of the AZ80-Ti sample, in addition to the Ti peak of the substrate, the peak of TiAl3, which is a Ti-Al intermetallic compound, is confirmed, and TiAl3 is generated in the Al enrichment region of the Ti substrate surface. EDS analysis is performed on the droplet tip portion of the sample section in which pure Mg droplets are dropped on the Ti substrate. Concentration of oxygen by the natural oxide film is not confirmed on the Ti surface, but oxygen is distributed at the tip of the droplet on the Mg side. Molten AZ80 and Ti-based compound phases are produced by thickening of Al in the vicinity of Ti after wetting is completed, and Al in the Mg alloy does not affect the wetting. The driving force of wetting progression is a thermite reaction that occurs between Mg and TiO2, and then Al in AZ80 thickens on the Ti substrate interface to form an intermetallic compound.

The Wetting Properties of UBM-coated Si-wafer to the Lead-free Solders in Si-wafer/Bumps/Glass Flip-Chip Bonding System

  • Hong, Soon-Min;Park, Jae-Yong;Park, Chang-Bae;Jung, Jae-Pil;Kang, Choon-Sik
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2000.04a
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    • pp.74-79
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    • 2000
  • In an attempt to estimate the wetting properties of wettable metal layers by wetting balance method, an analysis of wetting curves of the coating layer was performed. Based on the analysis, wetting properties of UBM-coated Si-plate were estimated by the new wettability indices. The wetting curves of the one and both sides-coated UBM layers have the similar shape and show the similar tendency to the temperature. So the wetting property estimation of one side coating is possible with wetting balance method. For UBM of Si-chip, Cr/Cu/Au UBM is better than Ti/Ni/Au in the point of wetting time. At general reflow temperature, the wettability of high melting point solders(Sn-Sb, Sn-Ag) is better than that of few melting point ones(Sn-Bi, Sn-In).The contact angle of the one side coated plate to the solder can be calculated from the farce balance equation by measuring the static state force and the tilt angle.

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Experimental Study on the Wall-Wetting Formation and Spray Characteristics of Gasoline Engine Injector (가솔린엔진 인젝터의 벽류 및 분무특성에 관한 실험적 연구)

  • Lee, Sung-Won;Lee, Sang-In;Park, Sung-Young
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.3
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    • pp.815-820
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    • 2010
  • Fuel spray characteristics of the gasoline engine injector has been studied experimentally. Wall wetting fuel stream of the 4-hole and 12-hole injectors has been tested and measured with various installation angle and port masking shapes. Spray visualization has been performed to analyze spray formation, spray angle, and penetration length. Test result shows that wall wetting is greatly influenced by the induction air flow and injector installation angle. Wall wetting amount decreased as injector installation angle decreased. Masking decreased wall wetting amount by increasing local intake-air flow velocity due to the decreased section area. Spray visualization showed that the 12-hole injector has robust performance characteristics compared with the 4-hole injector.

Wettability Analysis of Solders using Wetting Balance Test (Wetting Balance Test를 이용한 솔더의 젖음성 분석)

  • Jung, Do-hyun;Lim, Dong-uk;Baek, Bum-gyu;Yim, Song-hee;Yoon, Jong-hyuk;Jung, Jae Pil
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.2
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    • pp.1-9
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    • 2017
  • Recently, there has been a continuous researches on solders having sophisticated and improved performance due to demand for high-density and miniaturization of electronics, and development of solder for automotive electronics which can be used in harsh environment. When developing a new solder alloy, there is a wettability of solder on substrate for things to consider, and the wetting balance test is one of the methods for measuring that one. In this paper, the wetting balance test is introduced, and the calculus of the surface tension of solder and the contact angle between solder and substrate using wetting curve obtained is introduced too. In detail, the principle and test method of the wetting balance test, the introduction of the parameters with important meaning in the wetting curve, the method of calculating the contact angle as well as the surface tension of the solder using the shape of the solder meniscus.

Validity of the Sessile Drop Test of the Molten Al-Mg Alloys on SiO2 under Various Atmospheres (분위기에서 Al-Mg합금의 SiO2에 대한 젖음실험의 타당성 고찰)

  • Jang, Hyung-Min;Lee, Chang-Myeon;Lee, Joon-Ho;Lee, Jae-Hoon;Lee, Jae-Chul
    • Korean Journal of Metals and Materials
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    • v.47 no.6
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    • pp.383-390
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    • 2009
  • The effects that processing atmospheres and alloy composition have on the wetting characteristics of Al-Mg alloys on the $SiO_{2}$ substrate were investigated by measuring the wetting angles. It was observed that the wetting behavior of the Al-Mg alloys on the $SiO_{2}$ substrate vary depending on the Mg content of the alloys and atmospheres. The results showed that the contact angle decreases with increasing Mg content, angle is generally larger in the $N_{2}$ atmosphere than in the Ar atmosphere. We discussed the validity of the results obtained from the wetting test on the basis of recent theories and the results observed from the actual penetration tests.