• Title/Summary/Keyword: wet grinding

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Mineralogical Transformation of Gold-silver Bearing Sulfide Concentrate by Mechanochemical Activation, and their Gold-silver Leaching with Non-cyanide Solution (기계적-화학적 활성화에 따른 금-은-정광의 광물학적 상변화와 비-시안 용매에 의한 금-은 용출 향상)

  • Kim, Bong-Ju;Cho, Kang-Hee;Oh, Su-Ji;Choi, Nag-Choul;Park, Cheon-Young
    • Journal of the Mineralogical Society of Korea
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    • v.27 no.3
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    • pp.115-124
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    • 2014
  • In order to leach Au and Ag from gold-silver bearing sulfide concentrate, the sulfide concentrate was ground in a ball mill for a dry pre-treatment and a wet pre-treatment process. Mineralogical studies and thiourea leaching experiments were carried out with the pre-treated sulfide concentrate. The results of the pre-treatment with the concentrate samples showed the mean particle size and iso-electrical potential was smaller in the dry pre-treatment sample than in the concentrate sample, and the contents was lower in the wet pre-treatment sample than in the dry pre-treatment sample. In XRD analysis, amorphous properties were only shown in the wet pretreatment sample. The results of the concentrate sample leaching experiments showed that the best Au, Ag leaching parameters were when the addition of thiourea was at a 1.0 g concentration, ferric sulfate was 1.0 M, sulfuric acid was 2.0 M and the leaching temperature was at $60^{\circ}C$. The Au, Ag leaching rate was always much greater and faster with the wet pre-treatment samples than with the dry pre-treatment samples. Accordingly, it is expected that more Au, Ag can be leached in an eco-friendly methodology using wet pre-treatment. The pre-treatment could be improved with an optimized grinding additive reagent and through researching grinding time in future non-cyanide processes.

Recycling of EAF Dust by Semi-continuous High Kinetic Process

  • Zoz, H.;Kaupp, G.;Ren, H.;Goepel, K.;Naimi-Jamal, M. R.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.491-492
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    • 2006
  • The horizontal high energy rotor ball mill ($Simoloyer^{(R)}$) is used to break and activate dry solids. It is used for dry-milling and in the vertical mount for wet-milling in leaching processes. Technical electric arc furnace (EAF) dust with high contents of zinc oxide, zinc ferrite and magnetite is efficiently separated by ambient temperature leaching. The process shows promise for industrial application

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Effect of Si Wafer Ultra-thinning on the Silicon Surface for 3D Integration (삼차원 집적화를 위한 초박막 실리콘 웨이퍼 연삭 공정이 웨이퍼 표면에 미치는 영향)

  • Choi, Mi-Kyeung;Kim, Eun-Kyung
    • Journal of the Microelectronics and Packaging Society
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    • v.15 no.2
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    • pp.63-67
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    • 2008
  • 3D integration technology has been a major focus of the next generation of IC industries. In this study Si wafer ultra-thinning has been investigated especially for the effect of ultra-thinning on the silicon surface. Wafers were grinded down to $30{\mu}m\;or\;50{\mu}m$ thickness and then grinded only samples were compared with surface treated samples in terms of surface roughness, surface damages, and hardness. Dry polishing or wet etching treatment has been applied as a surface treatment. Surface treated samples definitely showed much less surface damages and better roughness. However, ultra-thinned Si samples have the almost same hardness as a bulk Si wafer.

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Comminution-Classification of Clay-type Minerals by Fluid Energy Mill (Fluid Energy Mill에 의한 점토성 무기소재 미립화 분급기술 소고)

  • 김태욱;김만영;정필조;이주완
    • Journal of the Korean Ceramic Society
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    • v.22 no.5
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    • pp.47-53
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    • 1985
  • In view of innovated utilization of Korean clay resources conventional techniques for pulverization are reviewed in comparison with fluid energy milling processes of fluidized-bed type. Throughout experiment indigenous halloysite ores (white grade) after usual pretreatment are employed as typical sample. It is evidenced that grinding by means of porcelain ball mills has limitation in reducing clay particles to less than 10${\mu}{\textrm}{m}$ in diameter regardless of whether it is processed in dry or wet. Upon use of tungsten carbide bull mill particulation to submicron sizes could be effected with relative ease but severe coloration in grey is attended indicating metallic contamination possibly from friction of the grinding apparatus itself. In contrast the modified fluid en ergy milling enables particulation to $\leq$10${\mu}{\textrm}{m}$ in diameter with simultaneous classification int olimited ranges of particle size distributions. Since this technique is in principle based on the interparticle collisions rather than on the frictions between particles and mill surfaces minimum impurity attendance would be an additional advantage. Evidence leads to the conclusion that the fluidized-bed type milling is regarded as highly effective in puverization as well as fractionation of the clay minerals under examination. This is especially so in contemplating high-value and/or high-purity clay products.

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Evaluation of Dewatering of Cellulose Nanofibrils Suspension and Effect of Cationic Polyelectrolyte Addition on Dewatering (셀룰로오스 나노피브릴 현탁액의 탈수성 평가 및 양이온성 고분자전해질 투입의 영향)

  • Ryu, Jaeho Ryu;Sim, Kyujeong;Youn, Hye Jung
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.46 no.6
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    • pp.78-86
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    • 2014
  • Since cellulose nanofibrils (CNF) has large specific surface area and high water holding capacity, it is very difficult task to remove water from the CNF suspension. However, dewatering of CNF suspension is a prerequisite of following processes such as mat forming and drying for the application of CNF. In this study, we evaluated the drainage of cellulose fibers suspension under vacuum and pressure conditions depending on the number of grinding passes. Also, the effect of the addition of cationic polyelectrolyte on dewatering ability of CNF suspension was investigated. Regardless of dewatering condition, the total drained water amount as well as the drainage rate were decreased with an increase in the number of grinding passes. Pressure dewatering equipment enables us to prepare wet CNF mat with relatively higher grammage. The cationic polyelectrolytes improved the dewatering ability of CNF suspension by controlling the zeta potential of CNF. The fast drainage was obtained when CNF suspension had around neutral zeta potential.

Effects of Preparation Conditions on Thermal and Electrical Properties of Oil-based Nanofluids for Transformer Application (변압기 냉각용 오일 기지 나노유체의 제조조건이 열 및 전기적 특성에 미치는 영향)

  • Choi, Cheol;Yoo, Hyun-Sung;Oh, Jae-Myung
    • Korean Journal of Materials Research
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    • v.17 no.9
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    • pp.493-499
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    • 2007
  • Oil-based nanofluids were prepared by dispersing nonconducting fibrous $Al_2O_3$ and spherical AlN nanoparticles in transformer oil. In this study, the effects of wet grinding and surface modification of particles on thermal and electrical properties of nanofluids were investigated. Grinding experiments were conducted with high-speed bead mill and ultrasonic homogenizer and nanoparticles were surface modified by oleic acid and polyoxyethylene alkyl acid ester(PAAE) in n-hexane or transformer oil, at the same time. It is obvious that the combination of nanoparticle, dispersant and dispersion solvent is very important for the dispersity of nanofluids. For nanofluids containing 1.0vol.% AlN particles in transformer oil, the enhancement of thermal conductivity was 11.6% compared with pure transformer oil. However, the electric-insulating property of AlN nanofluids was very low due to used dispersant itself. Therefore, the effect of the dispersant on thermal/electrical/physical properties of the transformer oil should be considered before selecting a proper dispersant.

Recovery of $\alpha$-iron from converter dust in a steel making factory -Utilization of the converter dust in a steel making factory- (제장소 전노 dust로부터 $\alpha$-장분말 회수에 관한 연구(II) -전노 dust의 이용에 관한 연구-)

  • Kim, Mi-Sung;Kim, Mahn;Cho, Moung-Ho;Oh, Jae-Hyun;Kim, Tae-Dong;Kim, Sung-Wan
    • Resources Recycling
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    • v.3 no.2
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    • pp.9-16
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    • 1994
  • In this study, the grinding and wet cyclone process of the dust for the effective separation of high purity iron powder and iron oxide were investigated. The results obtained in this study can be summarized as follows: 1. By applying the wet cyclone technique for the iron powder(+200 mesh) produced from EC dust of the Kwangyang 2nd steel making factory, the iron powder of high content more than 99.76% of Fe was obtained with 47.66% yield at grinding time of 5 minutes by attritor. 2. The particle size distribution of the iron powder recovered from converter dust is quite simillar with the iron powder of sweden Hoganas Co.(W40.24, W40.29, W40.37, W40.37OX). 3. By using iron powder, copper ions are all adsorbed and removed in any concentration ranges of copper sulfate solution(Cu:100, 200, 300, 600 ppm).

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An Experimental Study on the Effect of Concrete Surface Treatment Methods on the Bond Strength of Metal Spray Coating (콘크리트 표면처리 방법이 콘크리트 표면 금속용사 피막의 부착강도에 미치는 영향에 관한 실험적 연구)

  • Park, Jin-Ho;Kim, Sang-Yeol;Lee, Han-Seung
    • Journal of the Architectural Institute of Korea Structure & Construction
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    • v.36 no.1
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    • pp.147-154
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    • 2020
  • The exterior finishing of reinforced concrete buildings is one of the important factors to prevent durability and prevent natural environment or disaster such as temperature, snow, wind, rain from the outside as well as external design of buildings. Finishing methods can be divided into wet and dry methods. The wet method using paint is relatively easy to construct, but it requires repair and reinforcement every 1 to 5 years and requires a lot of LCC for maintenance. Finishing method using panel has good durability, but it is difficult to install and expensive. Therefore, in this paper, we evaluate the bond strength for the application of the metal spray method in order to overcome the problems of existing methods. Experimental results show that the sandblast + surface roughness agent(S-R(Y)) has a roughness of 41.16 ㎛ and the bond strength is about 3.19 MPa, which is the highest bond strength. In addition, the grinding + surface roughness agent(G-R(Y)) application showed roughness of about 36.59 ㎛ and secured the bond strength performance of 2.94 MPa.

Development and Characterization of Horse Bone-derived Natural Calcium Phosphate Powders

  • Jang, Kyoung-Je;Cho, Woo Jae;Seonwoo, Hoon;Kim, Jangho;Lim, Ki Taek;Chung, Pill-Hoon;Chung, Jong Hoon
    • Journal of Biosystems Engineering
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    • v.39 no.2
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    • pp.122-133
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    • 2014
  • Purpose: This study was to develop an effective process for fabricating biocompatible calcium phosphate powders (CPPs) using horse bones, and to investigate the characteristics of them. Methods: The characteristics of horse bone powders (HBPs) were investigated according to the different osseous tissue types (compact bone and cancellous bone), bone types (spine and tibia), pretreatment methods (cold water, $H_2O_2$, and hot water), sintering time (4, 8 and 12h), and sintering temperature (600, 900, 1100 and $1300^{\circ}C$). In addition, the grinding methods were compared based on the wet grinding (ball mill) and dry grinding (blade grinder) method to make it as powders. Finally, their cytotoxicity and cell viability were checked. Results: Regardless of the types of osseous tissues and bones, HBPs were well fabricated as biocompatible CPPs. It was also found that the pretreatment methods did not influence on the resultants, showing well-fabricated HBPs. Considering the processing time, the hot water method was the most suitable compared to other pretreatment methods. Further, 12h-sintering time was sufficient to remove residual organic compounds. The sintering temperatures greatly affected the properties of bone powders fabricated. The x-ray diffraction (XRD) peak of horse bone sintered at $600^{\circ}C$ was most closed to that of hydroxyapatite (HA). Our bioactivity study demonstrated that the HBPs fabricated by sintering horse bones at $1300^{\circ}C$ showed the best performance in terms of cell viability whereas the HBPs $1100^{\circ}C$ showed the cytotoxicity. Conclusions: Using various types of horse bone tissues, biocompatible CPPs were successfully developed. We conclude that the HBPs may have a great potential as biomaterials for various biological applications including bone tissue engineering.

Recovery of Petroleum Hydrocarbons from Oily Sludge Landfilled Soil

  • Shin, Su-Yeon;Park, Sang-Min;Ko, Sung-Hwan;Jung, Hong-Bae;Baek, Kitae
    • Journal of Soil and Groundwater Environment
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    • v.20 no.5
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    • pp.41-46
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    • 2015
  • Three types of experiments, based on the physical properties of oily sludge landfilled soil, were conducted to recover total petroleum hydrocarbons (TPH) from the soil. These experiments included gravity separation, solvent extraction using water, and air floatation. The oil portion was not easily separated from the wet (raw) soil because water molecules aggregate the soil particles, despite the fact that the soil was sandy. However, the drying and grinding processes destroyed the aggregates, causing the TPH recovery to increase to approximately 60% when air floatation was used. The drying process decreased the specific gravity of the soil sample, thereby enhancing the overall recovery of TPH from the soil. Although thermal desorption and/or incineration are common choices for heavily dumped sites, physical separation can recover the oil portion instead of simply removing it.