• Title/Summary/Keyword: wet ash method

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Comparison of the analytical methods for Cd in brown rice (현미중(玄米中) 카드뮴의 분석방법(分析方法)에 관(關)한 비교연구(比較硏究))

  • Kim, Bok-Young;Lee, Min-Hyo
    • Korean Journal of Environmental Agriculture
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    • v.14 no.3
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    • pp.338-344
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    • 1995
  • The wet ash method has been used as an official standard procedure for the analysis of Cd in brown rice in Korea, but this method involves several disadvantages. Thus, four analytical methods were compared in this experiment in order to find a more efficient method for the Cd analysis in brown rice. Evaluation was made based on both the Cd recovery percentages from the Cd-spiked samples and the relationships between Cd contents obtained by the official procedure and other methods. Results showed that ashing 50g brown rice at $600^{\circ}C$(dry ash method) recovered nearly 80% of the spiked Cd. This recovery percentage was a little lower than that of the wet ash method(87%) but higher than those of other methods. The dry ash method had the lowest standard deviations and revealed the highest correlation coefficient($r=0.98^{\ast\ast}$) in Cd contents with the standard wet ash method. These results demonstrated that the dry ash method, ashing 50g brown rice at $600^{\circ}C$, would be as efficient as the wet ash method and could be employed as a recommended procedure for the Cd analysis of brown rice.

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Trends of phosphorus recovery technology from sewage sludge ash by wet chemical method (습식 화학적 방법에 의한 하수 슬러지 소각재에서의 인 회수 기술동향)

  • Lee, Min-Su;Kim, Dong-Jin
    • Journal of Korean Society of Water and Wastewater
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    • v.32 no.2
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    • pp.131-143
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    • 2018
  • Phosphorus (P) is a limited, essential, and irreplaceable nutrient for the biological activity of all the living organisms. Sewage sludge ash (SSA) is one of the most important secondary P resources due to its high P content. The SSA has been intensively investigated to recover P by wet chemicals (acid or alkali). Even though $H_2SO_4$ was mainly used to extract P because of its low cost and accessibility, the formation of $CaSO_4$ (gypsum) hinders its use. Heavy metals in the SSA also cause a significant problem in P recovery since fertilizer needs to meet government standards for human health. Therefore, P recovery process with selective heavy metal removal needs to be developed. In this paper some of the most advanced P recovery processes have been introduced and discussed their technical characteristics. The results showed that further research is needed to identify the chemical mechanisms of P transformation in the recovery process and to increase P recovery efficiency and the yields.

Reviews on the Phosphorus Recovery from Incinerated Sewage Sludge Ash (하수슬러지 소각재 중의 인 회수방법의 사례 연구)

  • Yoon, Seok-Pyo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.29 no.1
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    • pp.5-17
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    • 2021
  • This study is a literature review on the recovering phosphorus from Incinerated Sewage Sludge Ash(ISSA), which has relatively high content of phosphorus. Experimental conditions and influencing factors related to the recovery of P and removal of heavy metals by wet and thermochemical methods were discussed. For the practical application of the recovery of P from ISSA, an integrated process linked to incineration facilities is required in terms of economy from the perspective of the entire system including disposal of wastewater and residues generated during the recovery process, and minimizing added chemicals and energy consumption.

A Study on the Mineral Contents of Korean Common Foods and Analytic Methods 1. Sodium (한국인의 상용 식품중 무기질 함량과 분석 방법 비교연구 1. 나트륨)

  • 송범호;황성희;이주돈;김희재;정해랑;문현경
    • Journal of Food Hygiene and Safety
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    • v.6 no.3
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    • pp.139-145
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    • 1991
  • In order to observe the Na contents, Korean common foods, especially processed foods were analyzed by Atomic Absorption Spectrophotometer. 1. The Na contents of instant noodle (ramen) was 400-900 mg/100 g and Na contents of their soup powder was 10000-16000 mg/100 g. 2. The Na contents of corns and beans was very low but their processed foods, com Dake and soybean milk, had relatively high Na contents. 3. The Na contents of meats was 40-60 mg/100 g but the Na contents of meats products was 700-900 mg/100 g. 4. The Na contents of Davoring salt was 12000-38000 mg/100 g, those of soybean products was 3000-6OOO mg/100 g, and that of seasoning MSG was 8000-17000 mg/100 g. 5. There was no statistical difference between the results of wet ash method and dry ash method in the Na contents of all food groups.

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The Determination of Glass content in fly Ash by X-Ray Diffraction (분말X선회절법에 의한 플라이 애시의 유리질 정량)

  • 이승헌;김홍주
    • Proceedings of the Korea Concrete Institute Conference
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    • 2000.04a
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    • pp.159-162
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    • 2000
  • The purpose of this study is to develope an accurate procedure for measuring the glass content of fly ash produced by bituminous coal to assist in predicting their behavior in concrete. Quantitative mineralogical compositions of fly ashes were obtained by internal standard method using powder X-ray diffraction analysis. In the X-ray diffraction method, the specimen and standard fluorite were cautiously mixed and pulverized to 22$\mu$m in wet process so as to avoid the prefered orientation of the crystal and microabsorption effect of X-ray. calibration curve were fitted for several references peaks of four phases:$\alpha$-quartz. mullite, magnetite, hematite. The amount of glass was calculated by subtracting the amount of crystal phase and loss on ignition from the total amount. Glass content determined with this method ranged from 66.7 to 75.wt%.

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Synthesis of modified polyacrylamides and their applications for the retention system of papermaking (변성 폴리아크릴 아미드의 합성 및 제지공정의 보류시스템에 응용)

  • Son, Dong-Jin;Yoon, Ji-Hyun;Choi, Eun-Jeong;Kim, Bong-Yong
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2009.04a
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    • pp.23-28
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    • 2009
  • The purpose of this study was to improve not only wet-end performances but also paper characteristics by the modification of various factors like molecular design and ionic characteristics of polyacrylamides First of all physical characteristics were observed after modify molecular design of the cationic polyacrylamides to linear, branched and cross-linked. In addition it was found analysis method to confirm branch degree of cationic polyacrylamides to combine ionic titration characteristics and spectroscopic behavior, After application of these structure modified polyacrylamides to the multiple retention systems with inorganic microparticles, it was found adjusting of branch degree of polyacrylamides was very important to optimize wet-end improvement. Second, After polymerization of amphoteric polyacrylamide to have both of cationic and anionic functional group in the polymer, we observed not only physical characteristics but also wet-end improvement to apply recycled pulp and found that the improvement of solution stability to prevent hydrolysis and increase of ash retention dramatically to compare traditional cationic polyacrylamide retention aid, Finally, After polymerization of anionic polyacrylamide, we observed not only wet-end improvement but also paper characteristics to apply preflocculation of PCC and it was found the improvements of flocculation efficiency, retention, ash retention, optical properties of the paper and bursting strength to compare traditional preflocculant of cationic polyacrylamide.

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A study on the Mineral Contents of Korea Common Foods and Analytical Methods. 2. Potassium (한국인의 상용식품 중 무기질 함량과 분석방법 비교 연구 2. 칼륨)

  • 송범호;황성희;이주돈;김희재;정해랑;문현경
    • Journal of Food Hygiene and Safety
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    • v.7 no.1
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    • pp.37-44
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    • 1992
  • In order to observe the K contents, Korean common foods, especially processed foods were analyzed by Atomic Absorption Spectrophotometer. The results obtained were summarized as followed; (I) The K contents of instant noodle(ramyon) was 105-180 mg/100g and K ontents of their soup powder was 500-1000 mg/100g. (2) The K contents of potato products and bean products were less than those of original foods. So it was recongnized that the K contents might reduced during the food process. (3) The K contents of meats was 130-475 mg/I00g and those of meats products was relatively low, 80-260 mg/100g. (4) The K contents of carbonate beverage was very low but that of instant coffed was very high, 2400-2600 mg/100g. (5) There was no Statistical difference between the results of wet ash method and dry ash method in the K contents of all food groups.

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Control of Grade Change Operations in Paper Plants Using Model Predictive Control Method (모델예측제어 기법을 이용한 제지공정에서의 지종교체 제어)

  • Kim, Do-Hun;Yeo, Yeong-Gu;Park, Si-Han;Gang, Hong
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2003.11a
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    • pp.230-248
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    • 2003
  • In this work an integrated model for paper plants combining wet-end and dry section is developed and a model predictive control scheme based on the plant model is proposed. Closed-loop process identification method is employed to produce a state-space model. Thick stock, filler flow, machine speed and steam pressure are selected as Input variables and basis weight, ash content and moisture content are considered as output variables. The desired output trajectory is constructed in the form of 1st-order dynamics. Results of simulations for control of grade change operations are compared with plant operation data collected during the grade change operations under the same conditions as in simulations. From the comparison, we can see that the proposed model predictive control scheme reduces the grade change time and achieves stable steady-state.

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Resistance to Corrosion of Reinforcing Steel and Critical Chloride Content of High Volume Fly Ash Concrete (하이볼륨 플라이애시 콘크리트의 철근부식 저항성 및 임계 염화물량)

  • Lee, Hyun-Jin;Bae, Su-Ho;Jung, Sang-Hwa
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.4
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    • pp.375-381
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    • 2017
  • Recently, due to the increasing of interest about the eco-friendly concrete, it is being increased to use concretes containing by-products of industry such as fly ash, ground granulated blast furnace slag, silica fume, and etc. Especially, these are well known for improving the resistance to reinforcement corrosion in concrete and decreasing chloride ion penetration. The purpose of this experimental research is to evaluate the resistance to corrosion of reinforcement and critical chloride content of high volume fly ash concrete(HVFAC) which is replaced with fly ash for approximately 50% cement content. For this purpose, corrosion monitoring of reinforcement by half cell potential method was carried out for the cylindrical test specimens that the upper of reinforcement in concrete was exposed to detect the time of corrosion initiation for reinforcement. It was observed from the test result that the the time of corrosion initiation for reinforcement of HVFAC by the accelerated corrosion tests increased 1.2~1.3 times than plain concrete and the critical chloride contents of plain concrete and HVFAC were found to range $0.80{\sim}1.20kg/m^3$, $0.89{\sim}1.60kg/m^3$, respectively.

Manufacture of Biodegradable Polymer with Wastepaper(I) - Pretreatment and Analysis of Chemical Components On Wastepaper - (폐지를 이용한 생분해성 고분자의 제조(I) - 폐지의 화학적 조성 분석 및 전처리 -)

  • Kwon, Ki-Hun;Lim, Bu-Kug;Yang, Jae-Kyung;Chang, Jun-Pok;Lee, Jong-Yoon
    • Journal of the Korean Wood Science and Technology
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    • v.28 no.3
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    • pp.34-41
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    • 2000
  • Recently many scientists have tried to synthesize biodegradable polymers due to durable and non-biodegradable products of conventional synthetic plastics when these were wasted in nature. So to reuse the wastepapers for biodegradable polymer resources, ONP (old newsprint), OCC (old corrugated containerbpard) were carried out by the pretreatment of chlorinite, hypochlorite and oxygen-alkali treatment conditions. For manufacturing of biodegradable polymer with wastepaper, this study performed to investigate change of chemical components and optimal pretreatment condition. The summarized results in this study were as follows: Lignin content in ONP and OCC was was higher than in MOW and ash content was the highest in MOW. More amount of ash components were reduced by wet defiberation than by dry defiberation. Wet defiberation fiber are better than dry defiberated fiber in chemical pretreatment condition for wastepapers, and the best result was obtained in the condition of sodium chlorite at $70^{\circ}C$, because it has high delignification ratio, ${\alpha}$-cellulose contents and degree of polymerization in this treatment condition. Oxygen-alkali treatment condition is the worst method because of low yield, low degree of polymerization in this pretreatments.

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