• Title/Summary/Keyword: vacuum extract

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Isolation of Volatiles from Panax ginseng Root by Vacuum-Distillation with Freeze-Drying (동결건조시 감압증류되는 인삼의 휘발성물질의 분리)

  • Park, Hoon;Sohn, Hyun-Joo;Cho, Byung-Goo
    • Journal of Ginseng Research
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    • v.14 no.3
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    • pp.353-356
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    • 1990
  • The isolation of volatile compounds by vacuum-distillation with freeze-drying was tested 1 with fresh ginseng roots. The roots were frozen at-8$0^{\circ}C$; they were dried at-4$0^{\circ}C$ tinder vacuum(40 tory), for 24 hours; and the ice condensed at the silrface of condenser in the freeze-dryer was thauved at room temperature. The ether extract of the resulting aqueous solution was analyzed by gas chromatography (GC) equipped with a flame ionization detector (FID) or a nitrogen-phosphorils detecto(NPD) and by gas : chromatography/mass spectrometry(GC/MS). More than forty peaks were observed in the CG(FID) profile. and more than ten peaks were observed in the GC(NPD) profile. Among them, thirteen components 1including one aldehyde, four hydrocarbons, two esters, folly alcohols, and two vyrazines were identified: six components the molesuiar ions of which were m/z, 204 were estimated to be a series of azulene compounds; and the other components unidentified were estimated to have molecular weights of lower than 254. Therefore, the freeze-drying technicue is thought to be usefu1 for the isolation of volatile compounds of such low molecufilar weights from vegetables, fruits and biological fluids as well as fresh ginseng roots under the tested conditions.

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Implementing Database for Designing Super High Temperature Vacuum Furnace (초고온 진공로 설계를 위한 데이터베이스 구축)

  • Kim, Jong-Hwa;Do, Sang-Yun;Lee, Jae-U;Jeong, Gap-Ju
    • Proceedings of the Korean Operations and Management Science Society Conference
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    • 2004.05a
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    • pp.273-276
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    • 2004
  • Multidisciplinary Design Optimization (MDO) is an individual and parallel design framework applied in designing large and complex systems. for successful implementation of MDO framework it is essential to manage data in efficient and integrated manner. In this study, we present a case study to implement database to support designing super high temperature vacuum furnace with MDO technology. For that purpose we first extract required data based on the analysis of design process and then data flows between different programs are analyzed. Finally an E-R diagram is presented to design database schema.

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Distinct Mechanisms of DNA Sensing Based on N-Doped Carbon Nanotubes with Enhanced Conductance and Chemical Selectivity

  • Kim, Han Seul;Lee, Seung Jin;Kim, Yong-Hoon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.415.1-415.1
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    • 2014
  • Carrying out first-principles calculations, we study N-doped capped carbon nanotube (CNT) electrodes applied to DNA sequencing. While we obtain for the face-on nucleobase junction configurations a conventional conductance ordering where the largest signal results from guanine according to its high highest occupied molecular orbital (HOMO) level, we extract for the edge-on counterparts a distinct conductance ordering where the low-HOMO thymine provides the largest signal. The edge-on mode is shown to operate based on a novel molecular sensing mechanism that reflects the chemical connectivity between N-doped CNT caps that can act both as electron donors and electron acceptors and DNA functional groups that include the hyperconjugated thymine methyl group[1].

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An investigation of the Photospheric and Chromospheric Layers of Sunspots

  • Kim, Hyun-Nam;Solanki, Sami. K.;Lagg, Andreas;Kim, Kap-Sung;Choe, G.S.;Kwon, Yong-Jun
    • The Bulletin of The Korean Astronomical Society
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    • v.36 no.2
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    • pp.95.2-95.2
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    • 2011
  • The most powerful technique for deducing the magnetic structure of the Sun is spectro-polarimetry. Detailed measurements of the polarization signal of the spectral lines (Stokes vector) allow us to infer the physical conditions in the solar atmosphere prevailing during the line formation. Inversion codes are the main tool to extract this information from the Stokes spectra. This study will focus on measurements of the chromospheric He I 1083.0 nm triplet and the photospheric Si I 1082.7 nm line. A spectropolarimetric data set of sunspots, obtained with the German Vacuum Tower Telescope (VTT) at the Teide observatory on Tenerife, is analyzed using an inversion technique. We will introduce the German Vacuum Tower Telescope and the inversion code HeLix, and will show data sets that are analyzed by HeLix.

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Preventive Efficacy of Kam Doo Extract Against Dichlovos Intoxication in Mouse (유기인중독에 대한 감두추출액의 방제효과)

  • 김학엽;임국환
    • Journal of Environmental Health Sciences
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    • v.15 no.2
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    • pp.75-83
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    • 1989
  • To evaluate the effect of Kam Doo-extract (KDE) on organophosphorous (OP)intoxication in mouse, this research was conducted. KDE prescribed with the equal weights of both Padix Glycyrrizae and Simen Glycine was extracted in water at 100$^{\circ}$C for 2hr, and concentrated in a vacuum evaporator. Animmal used in this research was ICR-strained male mice (bodyweight: 20 ~ 25g), and induction material for OP intoxication was DDVP(Dichlovos). Toxicity parameters used to evaluate KDE-preventive effect on DDVP were cholinesterase activity, and protection index of KDE against LDso values of DDVP. As the results, KDE prevented the inhibition of cholinesteranse activity due to DDVP-treatment, and inhanced the protecion index. Consequently our experimental data show the KDE will be useful as an preventive agent in respect that KDE is safe and effective against OP intoxication in mouse.

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The Parameters Extraction in Poly TFT Using Optimization Technique (최적화 기법에 의한 다결정 TFT(Thin Film Transistor)의 매개 변수 추출)

  • 김홍배;손상희;박용헌
    • The Transactions of the Korean Institute of Electrical Engineers
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    • v.40 no.6
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    • pp.582-589
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    • 1991
  • We used Cd Se as the semiconductor to analyze the Poly-TFT. Cd Se TFT is fabricated by the vacuum evaporation method and the characteristics curves of the current-voltage are obtained using the results of measurement of Cd Se TFT devices. Employing least square method and Rosenbrock algorithm, we can extract the device parameters(grain boundary mobility, trap density). The current-voltage relations calculated by extracted parameters are in good agreement with experimental results.

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Compaction and Sintering Behaviour of Zirconia Powders: I. Compaction Response (지르코니아 분말의 치밀화와 소결거동 : I. 가압에 따른 치밀화 응답)

  • ;Frank L. Riley
    • Journal of the Korean Ceramic Society
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    • v.29 no.6
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    • pp.489-495
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    • 1992
  • The continuous compaction response of zirconia powders prepared by different processing treatments was investigated. Though the yield point could be or not below 1 MPa, the change of slope was always observed at high pressure range around 60 MPa. Powder compaction was mainly governed by second compaction stage and compaction rate was decreased with increasing forming pressure. Rotary vacuum dried powder favored a high compaction density, whereas freeze dried and calcined powders favored an increase in the pressing efficiency. In order to extract more reliable information about powder compaction, it was necessary to use not only compaction response diagram but also compaction rate diagram.

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Carbohydrase inhibition and anti-cancerous and free radical scavenging properties along with DNA and protein protection ability of methanolic root extracts of Rumex crispus

  • Shiwani, Supriya;Singh, Naresh Kumar;Wang, Myeong Hyeon
    • Nutrition Research and Practice
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    • v.6 no.5
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    • pp.389-395
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    • 2012
  • The study elucidated carbohydrase inhibition, anti-cancerous, free radical scavenging properties and also investigated the DNA and protein protection abilities of methanolic root extract of Rumex crispus (RERC). For this purpose, pulverized roots of Rumex crispus was extracted in methanol (80% and absolute conc.) for 3 hrs for $60^{\circ}C$ and filtered and evaporated with vacuum rotary evaporator. RERC showed high phenolic content ($211{\mu}g$/GAE equivalent) and strong 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging ($IC_{50}$ = 42.86 (absolute methanol) and $36.91{\mu}g/mL$ (80% methanolic extract)) and reduced power ability. Furthermore, RERC exhibited significant protective ability in $H_2O_2/Fe^{3+}$/ascorbic acid-induced protein or DNA damage and percentage inhibition of the HT-29 cell growth rate following 80% methanolic RERC exposure at $400{\mu}g/mL$ was observed to be highest ($10.2%{\pm}1.03$). Moreover, methanolic RERC inhibited ${\alpha}$-glucosidase and amylase effectively and significantly (P < 0.05). Conclusively, RERC could be considered as potent carbohydrase inhibitor, anti-cancerous and anti-oxidant.

Effects of Antioxidants and Packaging Methods on the repression of Lipid Oxidation in Plain Dried Large Anchovy (소건 대멸치 지질의 산화억제에 미치는 항산화제와 포장의 병행효과)

  • CHO Young-Je;KIM Tae-Jin;SHIM Kil-Bo;CHOI Young-Jun
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.33 no.3
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    • pp.238-242
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    • 2000
  • The antioxidants and packaging methods affecting on lipid oxidation of the plain dried large anchovy were investigated. Antioxidants resulted in decrease of lipid oxidation of dried large anchovy. The addition of BHT remarkably repressed lipid oxidation during storage of the dried large anchovy at $37^{\circ}C$, followed by ${\alpha}-tocopherol$, rosemary extract and sage extract. The addition of rosemary extract mixed with 0.1{\%} {\alpha}-tocopherol$ showed similar effect to BHT during storaBe at $25^{\circ}C\;in\;0.1{\%}$ rosemary extract mixed with $0.1{\%}\;{\alpha}-tocopherol$. When the dried anchovy were packed in polyethylene film after treatment with antioxidants, the vacuum package increased the antioxidative effect in repression of lipid oxidation during storage of dried large anchovy.

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Hepatoprotective Effect of Gagam-GongJin-dan extract against Acetaminophen-Induced Liver Injury in Mice (Acetaminophen 유도 마우스 간 손상에 대한 가감공진단(加減拱辰丹) 추출물의 간보호 효과)

  • Kim, Hong-Hun;Mok, Ji-Ye;Park, Kwang-Hyun;Jeong, Seung-Il;Hwang, Byung-Soon;Hwang, Sung-Yeoun;Cho, Jung-Keun;Jang, Seon-Il
    • The Korea Journal of Herbology
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    • v.25 no.3
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    • pp.149-157
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    • 2010
  • Objective:Gagam-Gongjin-dan (GGD) is an oriental medicinal prescription composited with Cervi parvum Cornu, Corni Fructus, Angelica Gigantis Radix, Lycii Fructus, Dioscoreae Rhizoma, Citri Pericarpium, Gastrodiae Rihzoma, Agastachis Herba, Cassiae cortex, Scutellariae Radix and Schisandrae Fructus. The purpose of this study was to investigate the effects of GGD extract against acetaminophen (APAP)-induced liver injury in mice. Methods:GGD extract was prepared by extracting with methanol for 7 days. The extract was freeze-dried following filtration through vacuum distillation system. The first, we investigated the antioxidant effects of GGD extract on electronic donating ability (DPPH), nitrite (NO) scavenging and superoxide dismutase (SOD)-like activity. The next, we investigated the possible hepatoprotective effect of GGD extract administration against acetaminophen-induced liver injury in mice. Mice were orally administrated with or without GGD extract of different doses (25-100 mg/kg/day) one times per day for 6 days. After 3 days, APAP was orally applied with a single dose (400 mg/kg). Results:GGD extract increased DPPH, NO and SOD-like activities in dose dependant. APAP treatment significantly increased aspartate aminotransferase (AST) and alanine aminotransferase (ALT) activities in plasma. Also, APAP treatment significantly evaluated lipid peroxidation product thiobarbituric reacting substances (TBARS) and depleted some antioxidant enzymes (superoxide dismutase, catalase, d-aminolevulinate dehydratase and gluthathione peroxidase activities) in liver homogenates compared to the control group. However, the orally administration of GGD extract was able to counteract these effects. Histological studies provided supportive evidence for biochemical analysis Conclusions:These results suggest that GGD extract has a potential antioxidant and hepatoprotective effect against APAP-induced liver injury, these properties may contribute to liver disease care.