• 제목/요약/키워드: uniform grain size

검색결과 176건 처리시간 0.027초

스핀 코팅법으로 증착한 $(Bi,La)_4Ti_3O_{12}$ 박막의 후속 열공정에 따른 입자 크기 및 결정 방향성 변화 (Thermal Process Effects on Grain Size and Orientation in $(Bi,La)_4Ti_3O_{12}$ Thin Film Deposited by Spin-on Method)

  • 김영민;김남경;염승진;장건익;류성림;권순용
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 추계학술대회 논문집 Vol.19
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    • pp.192-193
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    • 2006
  • A 16Mb ITIC FeRAM device was fabricated with BLT capacitors. The average value of the switchable 2 polarization obtained m the 32k-array (unit capacitor size: 068 ${mu}m^2$) capacitors was about 16 ${\mu}C/cm^2$ at 3V and the uniformity within an 8-inch wafer was about 2.8%. But a lot of cells were failed randomly during the measuring the bit-line signal of each cell. It was revealed that the Grain size and orientation of the BLT thin film were severely non-uniform. Therefore, the uniformity of the grain size and orientation was improved by changing the process conditions of post heat treatment. The temperature of nucleation step was the very effective on varying the microstructure of the BLT thin film. The optimized temperature of the nucleation step was $560^{\circ}C$.

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단어재인에 있어서 처리단위의 적응적 변화 (Adaptive Changes in the Grain-size of Word Recognition)

  • Lee, Chang H.
    • 한국인지과학회:학술대회논문집
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    • 한국인지과학회 2002년도 춘계학술대회
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    • pp.111-116
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    • 2002
  • The regularity effect for printed word recognition and naming depends on ambiguities between single letters (small grain-size) and their phonemic values. As a given word is repeated and becomes more familiar, letter-aggregate size (grain-size) is predicted to increase, thereby decreasing the ambiguity between spelling pattern and phonological representation and, therefore, decreasing the regularity effect. Lexical decision and naming tasks studied the effect of repetition on the regularity effect for words. The familiarity of a word from was manipulated by presenting low and high frequency words as well as by presenting half the stimuli in mixed upper- and lowercase letters (an unfamiliar form) and half in uniform case. In lexical decision, the regularity effect was initially strong for low frequency words but became null after two presentations; in naming it was also initially strong but was merely reduced (although still substantial) after three repetitions. Mixed case words were recognized and named more slowly and tended to show stronger regularity effects. The results were consistent with the primary hypothesis that familiar word forms are read faster because they are processed at a larger grain-size, which requires fewer operations to achieve lexical selection. Results are discussed in terms of a neurobiological model of word recognition based on brain imaging studies.

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알루미나의 소결 중 CaO 불순물의 미세구조에 미치는 영향 (Effects of CaO Impurity on Microstructural Evolution during Sintering of Alumina)

  • 김상섭;백성기
    • 한국세라믹학회지
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    • 제29권1호
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    • pp.1-8
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    • 1992
  • The effect of CaO impurity on the microstructural evolution during the sintering of ultrapure alumina(>99.999%) was studied under "clean" firing conditions. The sinterability of undoped alumina was low, but its microstructure was maintained uniform. In the case of CaO-doped alumina, the distribution of grain size and that of grain boundary dihedral angle became wider, and facetted pores observed frequently. When MgO was doped in addition to CaO, the sinterability increased drastically and the uniform microstructural characteristics resumed. This study suggests that the effect of CaO is to induce inhomogeneous microstructures presumably by anisotropic segregation to grain boundaries and pore surfaces, and that MgO suppresses the anisotropic segregation of Ca.

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알루미나-지르코니아 복합체의 제조공정 및 미세구조에 미치는 폴리머 첨가의 영향 (Effect of Polymer Content on Synthesis Process and Microstructure of Alumina-Zirconia Composite)

  • 이상진;권명도;이충효;조경식
    • 한국분말재료학회지
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    • 제10권5호
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    • pp.310-317
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    • 2003
  • Two-component ceramic (alumina-zirconia) composites were fabricated by a soft-solution process in which polyethylene glycol (PEG) was used as a polymeric carrier. Metal salts and PEG were dissolved in ethyl alcohol without any precipitation in 1:1 volume ratio of alumina and zirconia. In the non-aqueous system, the flammable solvent made explosive, exothermic reaction during drying process. The reaction resulted in formation of volume expanded, porous precursor powders by a vigorous decomposition of organic components in the precursor sol. The PEG content affected the grain size of sintered composites as well as the morphology of precursor powders. The difference of microstructure in sintered composite was attribute to the solubility and homogeneity of metal cations in precursor sol. At the optimum amount of the PEG polymer, the metal ions were dispersed effectively in solution and a homogeneous polymeric network was formed. It made less agglomerated particles in the precursor sol and affected on uniform grain size in sintered composite.

반용융 압출을 위한 AA7075 합금의 조직제어 (Microstructural Control of AA7075 Alloy for Thixoextrusion)

  • 윤영옥;김영직;김세광;조형호
    • 한국주조공학회지
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    • 제25권6호
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    • pp.249-253
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    • 2005
  • The present study focuses on 7075 aluminum wrought alloy to investigate the potential industrial applications of thixoextrusion process. The microstructural evolution of 7075 aluminum wrought alloy for thixoextrusion has been investigated as a function of isothermal holding temperature and time in the partially remelted semisolid state. The results showed that the liquid fraction increased with increasing isothermal holding temperature and time while the average grain size was inversely proportional to isothermal holding temperature and time up to 5min. However, there was no big change of liquid fraction and average grain size with respect to isothermal holding temperature and time. The important fact that the liquid fraction and average grain size were almost uniform after 5 min holding time is considered very useful for thixoextrusion in terms of process control.

EFFECT OF Al UNDERLAYER ON THE MICROSTRUCTURES OF CoCrTa/Cr FILMS

  • Chang, H.S.;Shin, K.H.;Lee, T.D.;Park, J.K.
    • 한국자기학회지
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    • 제5권5호
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    • pp.614-617
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    • 1995
  • Thin CoCrTa/Cr films were deposited on glass substrates at $280^{\circ}C$ with or without Al underlayer. The coercivity of CoCrTa increased considerably by introducing an Al underlayer. The grain size of Cr thin film deposited on Al underlayer became smaller than that of Cr thin film deposited on glass substrate. The grain size of CoCrTa thin film was determined by Cr grain size. The cause of the coercivity increase seems to be associated with the refinement and uniform distribution of CoCrTa grains.

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Incoloy 825 합금의 기계적 성질에 미치는 열간단조비의 영향 (Effect of Hot Forging Ratio on the Mechanical Properties in Incoloy 825 Alloy)

  • 박영태;정영훈;강창룡
    • 열처리공학회지
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    • 제29권6호
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    • pp.259-263
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    • 2016
  • This study was carried out to investigate the effect of hot forging ratio on the microstructure and mechanical properties of incoloy 825 alloy. Hot forging was carried out at the forging ratio of 0%, 60% and 90% respectively in a range of $900^{\circ}C{\sim}1,140^{\circ}C$ and followed solution treatment was conducted at $1,000^{\circ}C$ for 1 hr. In all the specimens of hot forged of 0%, 60% and 90%, precipitates were not observed. The average grain size of 0% specimen is $82{\mu}m$ and that of 60% and 90% is $56{\mu}m$ and $31{\mu}m$, respectively. The range of grain size in the 0% specimen is uneven in $182{\mu}m$ to $31{\mu}m$, but the grain size of 90% specimen is uniform. With increasing hot forging ratio, the mechanical properties such as tensile strength, elongation, hardness increased and impact toughness increased by grain refinement.

용융드래그방법으로 제작한 마그네슘합금 박판의 특성에 미치는 기본적인 공정조건 확립 (Establishment of Fundamental Process Conditions on Properties of Magnesium Alloy Thin Plates Fabricated by the Melt Drag Method)

  • 한창석;이찬우
    • 한국재료학회지
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    • 제32권7호
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    • pp.326-331
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    • 2022
  • AZ31 magnesium alloy was used to manufacture a thin plate using a melt drag method. The effects of roll speed, molten metal temperature, and molten metal height, which are the basic factors of the melt drag method, on the surface shape, the thickness of the thin plate, Vickers hardness, and microstructure of the thin plate were investigated. It was possible to manufacture AZ31 magnesium alloy thin plate at the roll speed range of 1 to 90 m/min. The thickness of the thin plate, manufactured while changing only the roll speed, was about 1.8 to 8.8 mm. The shape of the solidified roll surface was affected by two conditions, the roll speed and the molten metal height, and the Vickers hardness of the manufactured magnesium alloy thin plate value ranged from Hv38~Hv60. The microstructure of the thin plate produced by this process was an equiaxed crystal and showed a uniform grain size distribution. The grain size was greatly affected by the contact state between the molten metal and the solidification roll, and the amount of reactive solids and liquids scraped at the same time as the thin plate. The average grain size of the thin plate fabricated in the range of these experimental conditions changed to about 50-300 ㎛.

6.4cm 크기의 일방향 성장된Y$Ba_2$$Cu_3$$O_x$ 제조 (Fabrication of 6.4 cm single grain $YBa_2$$Cu_3$$O_x$)

  • 박병삼;한상철;한영희;정년호;윤희중;김경진;성태현;오제명
    • Progress in Superconductivity
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    • 제5권2호
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    • pp.114-117
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    • 2004
  • We fabricated large single grain YBa$_2$Cu$_3$O$_{x}$ (Y-123) superconductors. The single grain Y-123 was grown by top seeded melt growth (TSMG) method. In a conventional box furnace with uniform temperature distribution, it was very difficult to grow large single grain Y-123 superconductors due to the size limitation in growth. To overcome the size limitation, we applied a radial thermal gradient (lower temperature at sample center and higher temperature on the sample edge) to the TSMG process. In this case, large single grain Y-123 could be easily grown. This is attributed that the liquid of the sample edge was maintained at the high temperature compared to the growth front. Using this method, we successfully fabricated a large single grain Y-123 of 6.4 cm X6.4 cm

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도핑된 알루미나 여과막의 미세구조 변화 (Microstructural Change of Doped-Alumina Membrane)

  • 이진하;최성철;한경섭
    • 한국세라믹학회지
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    • 제36권10호
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    • pp.1040-1047
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    • 1999
  • After alumina sol was prepared by Yoldas process supported membranes were fabricated by adding ce and Re solution and SiO2 sol into alumina sol. The particle size of alumina sol was 11 nm and it was monodispersed transparent and stable for long time. The pore size of un-doped membrane started to increase to about 7,5nm at 1000$^{\circ}C$ and it was grown to twice (about 15nm) at 1100$^{\circ}C$ However the pore size of doped alumina was uniform to 1100$^{\circ}C$. The effect of retardation of grain growth was superior in SiO2 addition to that of Ce and Ru Because SiO2 doped samples transformed to needed-like phase and densified at 1200$^{\circ}C$ their application in membranes was limited. Ce and Ru doped sample showed vermicular structure identical to the un-doped ones at 1200$^{\circ}C$ But the particle size was smaller than that of un-doped ones.

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