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Assessment of effect of accelerated aging on interim fixed dental materials using digital technologies

  • Omar, Alageel;Omar, Alsadon;Haitham, Almansour;Abdullah, Alshehri;Fares, Alhabbad;Majed, Alsarani
    • The Journal of Advanced Prosthodontics
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    • v.14 no.6
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    • pp.360-368
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    • 2022
  • PURPOSE. This study assessed the physical and mechanical properties of interim crown materials fabricated using various digital techniques after accelerated aging. MATERIALS AND METHODS. Three groups of interim dental restorative materials (N = 20) were tested. The first group (CO) was fabricated using a conventional manual method. The second group (ML) was prepared from prefabricated resin blocks for the milling method and cut into specimen sizes using a cutting disc. The third group (3D) was additively manufactured using a digital light-processing (DLP) 3D printer. Aging acceleration treatments using toothbrushing and thermocycling simulators were applied to half of the specimens corresponding to three years of usage in the oral environment (N = 10). Surface roughness (Ra), Vickers microhardness, 3-point bending, sorption, and solubility tests were performed. A 2-way analysis of variance (ANOVA) and Fisher's multiple comparison test were used to compare the results among the groups. RESULTS. The mean surface roughness (Ra) of the resin after accelerated aging was significantly higher in the CO and ML groups than that before aging, but not in the 3D group. All groups showed reduced hardness after accelerated aging. The flexural strength values were highest in the 3D group, followed by the ML and CO groups after accelerated aging. Accelerated aging significantly reduced water sorption in the ML group. CONCLUSION. According to the tested material and 3D printer type, both 3D-printed and milled interim restoration resins showed higher flexural strength and modulus, and lower surface roughness than those prepared by the conventional method after accelerated aging.

A Study on Quenching Speed Prediction Method of Specimen for Evaluating the Oxide Layer of Uncoated Boron Steel Sheet (비도금 보론강판 산화층 평가용 시편의 퀜칭속도 예측기법 연구)

  • Lee, J.H.;Song, J.H.;Bae, G.H.
    • Transactions of Materials Processing
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    • v.31 no.1
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    • pp.17-22
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    • 2022
  • Hot stamping is widely used to manufacture structural parts to satisfy requirements of eco-friendly vehicles. Recently, hot forming technology using uncoated steel sheet is being studied to reduce cost and solve patent problems. In particular, research is focused on process technology capable of suppressing the generation of an oxide layer. To evaluate the oxide layer in the hot stamping process, Gleeble testing machine can be used to evaluate the oxide layer by controlling the temperature history and the atmosphere condition. At this time, since cooling by gas injection is impossible to protect the oxide layer on the surface of a specimen, research on a method for securing a quenching speed through natural cooling is required. This paper proposes a specimen shape design method to secure a target quenching speed through natural cooling when evaluating the oxide layer of an un-coated boron steel sheet by Gleeble test. For the evaluation of the oxide layer of the un-coated steel sheet through the Gleeble test, dog-bone and rectangular type specimens were used. In consideration of the hot stamping process, the temperature control conditions for the Gleeble test were set and the quenching speed according to the specimen shape design was measured. Finally, the quenching speed sensitivity according to shape parameter was analyzed through regression analysis. A quenching speed prediction equation was then constructed according to the shape of the specimen. The constructed quenching speed prediction equation can be used as a specimen design guideline to secure a target quenching speed when evaluating the oxide layer of an un-coated boron steel sheet by the Gleeble test.

Charring Properties of Glued Laminated Timber Columns using Domestic Larch Exposed to High Temperatures (고온에 노출된 국내산 낙엽송 구조용 집성재 기둥의 탄화 특성)

  • An, Jae-Hong;Choi, Yun-Jeong;Kim, Se-Jong
    • Journal of the Korea Institute of Building Construction
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    • v.23 no.1
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    • pp.23-33
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    • 2023
  • It is widely known that the level of fire resistance of wooden structure is determined by a charring rate or charring depth, and these are adopted for fire design. In this study, specimens of domestic larch column with a lamination wooden type were prepared and the fire resistance properties such as the charring depth, load ratio and the specific charring rate suggested by EN Code investigated. Test results showed that as expected, the weakest part was the corner of the column, so that the charring depth of the corner was deeper than the other parts of the column. For the load ratio less than 0.9, it had little effect on the charring depth.

A taxonomic review of Korean Leontopodium R. Br. ex Cassini (Asteraceae) (한국산 솜다리속의 분류학적 재검토)

  • Lee, Dong-Hyuk;Park, Jong-Su;Choi, Byoung-Hee
    • Korean Journal of Plant Taxonomy
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    • v.46 no.2
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    • pp.149-162
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    • 2016
  • Five species of the genus Leontopodium are recognized in Korea, but their taxonomic positions have been controversial. To clarify the taxonomic entity of these Korean species, we examined their morphological characters based on herbarium specimens and field observations. Valuable distinguishing characters for identification included the plant height, the basal shape of cauline leaves, the type and position of inflorescence, the types of hairs, the presence of leaves at the anthesis, and hairs on the phyllaries. Based on our observations, we were able to determine the taxonomic relationships between L. japonicum and its relatives, L. coreanum and L. hallaisanense. We also included the morphological characters of L. seorakensis in continuous variations of L. leiolepis, which we treated as synonyms. Consequently, we classified these Korean Leontopodium species into four taxa - L. coreanum var. coreanum, L. coreanum var. hallaisanense, L. leiolepis, and L. leontopodioides - with appropriate descriptions and illustrations.

Effects of Carburizing Process on Sliding wear Behavior of Carburized SCM420H Steel (침탄처리한 SCM420H의 미끄럼 마모 특성에 미치는 침탄 조건의 영향)

  • Lee, Han-Young;Lee, Kyu-Hyun
    • Tribology and Lubricants
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    • v.36 no.1
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    • pp.18-26
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    • 2020
  • The effects of the carburizing process on the sliding wear behavior of SCM420H steel have been investigated. In particular, the effects of grain boundary corrosion observed in the surface layer after gas carburizing and the effects of hardness of the carburized cases after heat-treatment on the sliding wear properties were examined. Pin specimens carburized by two methods (gas carburizing and vacuum carburizing) were tempered at two temperatures of 180℃ and 400℃ after oil-quenching, respectively. Sliding wear tests were carried out against heattreated SKH51 steel at several sliding speeds using a pin-on-disc type test machine. As results, it can be found that there is no difference in the wear behavior between the pins carburized using two methods. This implies that the grain boundary corrosion that formed in the surface layer after gas carburizing has no effect on the sliding wear behavior of carburized SCM420H steels. Additionally, there is no significant difference in the wear behavior between carburized pins tempered at 400℃ and at 180℃ after oil-quenching, regardless of the carburizing method. This is because carburized pins tempered at 400℃ have a troostite structure, which exhibits higher tribochemical reactivity even though its hardness is lower than that of martensite structure. In this respect, it can be considered that good wear resistance of carburized cases is maintained at least until the effective case depth.

A Study on the Structural Integrity Considering the Installation of a Micro-tube Heat Exchanger (미세튜브 열교환기의 장착을 고려한 구조건전성에 관한 연구)

  • Oh, Se Yun;Kim, Tae Jin;Cho, Jong Rae;Jeong, Ho Sung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.4
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    • pp.447-451
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    • 2015
  • The objective of this study is to predict the structural characteristics of a heat exchanger mounted on an aircraft engine using finite element analysis. The plastic fracture and life of the heat exchanger were estimated by a thermo-mechanical analysis. Tensile tests were conducted under high temperature conditions (700, 800, 900, 1000 K) using five specimens to obtain the mechanical properties of the Inconel 625 tubes. To assess the structural characteristics of the heat exchanger, the full and partial models were applied under the operating conditions given by the thermo-mechanical and inertial load. As a result, the case, tubesheet, flange, and mounting components have a reasonable safety margin to the allowable stress assuming a fatigue strength of Inconel 625 of 10000 cycles under 1000 K.

Association of Matrix Metalloproteinase (MMP)-2 and -9 Expression with Extra-gastrointestinal Stromal Tumor Metastasis

  • Wang, Chao;Ma, Hong-Xi;Jin, Mei-Shan;Zou, Ya-Bin;Teng, Yong-Liang;Tian, Zhuang;Wang, Hai-Ying;Wang, Yin-Ping;Duan, Xiu-Mei
    • Asian Pacific Journal of Cancer Prevention
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    • v.15 no.10
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    • pp.4187-4192
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    • 2014
  • Matrix metalloproteinase (MMP)-2 and MMP-9 are important proteases involved in invasion and metastasis of various tumors. Extra-gastrointestinal stromal tumors (EGISTs) are rare neoplasms. This study was performed to assess MMP-2 and MMP-9 expression in EGIST tissue samples for association with clinicopathological data from the patients. Twenty-one surgical EGIST tissue specimens were collected for analysis of MMP-2 and MMP-9 expression using immunohistochemistry. MMP-2 and MMP-9 proteins were expressed in all of the epithelial cell types of EGISTs, whereas they were only expressed in 75% of the spindle cell type, although there was no statistically significant difference (p>0.05). Expression of MMP-2 and MMP-9 proteins was associated with tumor size, mitotic rate, tumor necrosis, and distant metastasis (p<0.05). MMP-2 expression was linked with MMP-9 levels (p<0.05). However, there was no correlation between MMP-9 expression and age, sex, primary site, or cell morphology in any of these 21 EGIST patients (p>0.05). Moreover, expression of MMP-2 and MMP-9 proteins increased with the degree of EGIST risk. This study provided evidence of an association of MMP-2 and MMP-9 expression with advanced EGIST behavior.

Dynamic Deformation Characteristics of Fiber Reinforced Soils (섬유혼합토의 동적물성변형특성)

  • Jung, Sung-Yong;Kim, Dae-Il;Park, Chul-Soo;Mok, Young-Jin
    • Proceedings of the Korean Geotechical Society Conference
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    • 2004.03b
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    • pp.968-976
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    • 2004
  • In the paper, deformation characteristics of fiber-mixed-soils, mixed polypropylene staple fibers of 0.3% fiber content with sands of various gradation, and their effectiveness of reinforcement were evaluated. A series of Resonant Column tests were performed with specimens prepared with varying Uniformity Coefficient and constant Curvature Coefficient. Maximum shear moduli 01 fiber-mixed-soils were increased by up to 30% and modulus reduction was also restrained in nonlinear range. Normalized shear modulus reduction curves of fiber-mixed-soils shift close to the upper limit of Seed curd Idriss's curves and are located within narrower band than those of unmixed soils, which proves the effectiveness on stiffness increment by reinforcing soils with fibers.

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A Study on the Impact-Induced Damage in CFRP Angle-ply Laminates (CFRP 사교적층판의 충격손상에 관한 연구)

  • 배태성;입야영;양동률
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.2
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    • pp.237-247
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    • 1993
  • Carbon fiber reinforced plastics(CFRP) have gained increased application in aerospace structures because of their specific strength and stiffness, but are sensitive to impact-induced damage. An experimental investigation was carried out to evaluate the impact resistance of CFRP according to the ply angle. The specimens of angle ply laminate composites were employed with [0.deg. $_{6}$/ .deg.$_{10}$/0.deg.$_{6}$], in which 6 kinds of ply angle such as .deg.=15.deg., 30.deg., 45.deg., 60.deg., 75.deg. and 90.deg. were selected. The impact tests were conducted using the air gun type impact testing machine by steel balls of diameter of 5 mm and 10 mm, and impact-induced damages were evaluated under same impact speed of V=60m/s. The impact damaged zones were observed through a scanning acoustic microscope (SAM). The obtained results were summarized as follows: (1) Delaminations on the interfacial boundaries showed th directional characteristics to the fiber directions. The delamination area on the impact side (interface A) was considerably smaller compared to that of the opposite side (interface B). (2) Cracks corresponding to other delaminations than those mentioned in SAM photographs were also seen on the impact damaged zone. (3) The delamination patterns were affected by the ply-angle, the dimensions of the specimen, and the boundary conditions. (4) The impact damaged zone showed zone showed the delamination on the interfacial boundaries, transverse shear cracks of the surface layer, and bending cracks of the bottom layer.r.r.r.

Evaluation of Effects of Rare Earth Element and Cooling Rate on the Eutectic Reaction of Flake Graphite Cast Irons by Cooling Curve Analysis (냉각곡선 분석을 통한 편상흑연주철의 공정반응에 미치는 희토류원소 및 냉각속도의 영향 평가)

  • Lee, Sang-Hwan;Park, Seung-Yeon;Lee, Sang-Mok;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.33 no.1
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    • pp.13-21
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    • 2013
  • The effects of rare earth element (R.E.) and cooling rate on the eutectic reaction of flake graphite cast irons were studied by combined analysis of macro/micro-structure and cooling curve data. The correlation between eutectic reaction parameter and macro/micro-structure was systematically investigated. Two sets of chemical compositions with the different addition of R.E. were designed to cast. Three types of molds for cylindrical specimens with the different diameters were prepared to analyze cooling rate effect. The difference between undercooling temperature and cementite eutectic temperature (${\Delta}T_1=T_{U}-T_{E,C}$), which is increased by adding R.E. and decreased by increasing cooling rate, is considered to be a suitable eutectic reaction parameter for predicting graphite morphology. According to the criterion, A-type graphite is mainly suggested to form for ${\Delta}T_1$ over $20^{\circ}C$. Eutectic reaction time (${\Delta}t$), which is decreased by adding R.E. or increasing cooling rate, is a suitable eutectic reaction parameter for predicting eutectic cell size. Eutectic cell size is found to decrease in a proportion to the decrease of ${\Delta}t$.