• 제목/요약/키워드: tungsten(W)

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달성광산(達成鑛山) 주변지역(周邊地域)에서의 중금속오염(重金屬汚染)과 이의 제거방안(除去方案) (Heavy Metal Contamination and Process for Its Removal in the Vicinity of the Dalsung Cu-W Mine)

  • 김경웅;홍영국;김택남
    • 자원환경지질
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    • 제29권1호
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    • pp.57-63
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    • 1996
  • The Dalsung copper-tungsten mine in the Taegu area, Korea was closed in 1975 and may be the sources of the heavy metal contamination in the tributary system and soil-plant system due to the mine drainage derived from the mine wastes and tailings. To examine the degree and extent of heavy metal contamination in the vicinity of Dalsung mine area, stream water and soil samples were taken and analyzed for heavy metals by ICP-AES and AAS. Highly contaminated soils are found near the Lower Tunnel No.0 ranging up to $1760{\mu}g/g$ As, $2060{\mu}g/g$ Cu, $1120{\mu}g/g$ Pb and 346 ${\mu}g/g$ Zn. From the results of the sequential extraction methods for the metal speciation, the heavy metals in soils may be derived from soil parent materials and acid mine drainage. With the processes for the heavy metal removal, most of the heavy metal ions in the acid mine drainage are removed by being exchanged with Ca ions held by the bentonite, hydroxyapatite and calcium hydoxide.

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포항가속기 저장링챔버의 헬륨누설검사 (Helium Leak Test for the PLS Storage Ring Chamber)

  • 최만호;김형종;최우천
    • 비파괴검사학회지
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    • 제13권3호
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    • pp.31-38
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    • 1993
  • 포항가속기 저장링 진공챔버는 진공도가 $10^{-10}Torr$로 유지될 수 있도록 설계되었고, 초고진공에 적합하도록 TIG용접을 하여 헬륨에 대한 누설률이 $1{\times}10^{-10}Torr{\cdot}{\ell}/sec$ 이하의 기밀성이 요구되고 있다. 저장링 진공챔버에 적용된 TIG용접방법과 결함에 대해 논하고 누설검사에 사용된 헬륨누설검사기의 원리 및 검사방법에 대해서 보고하고자 한다.

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전자빔 drip 용해횟수가 Mo 잉고트 특성에 미치는 영향 (Effect of the Number of Electron Beam Drip Melting on the Characteristics of Molybdenum ingot)

  • 최국선;이강인;이동희
    • 한국주조공학회지
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    • 제15권3호
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    • pp.283-290
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    • 1995
  • Molybdenum ingot of 50mm in diameter were obtained from sintered Mo bars by EB drip melting technique. Macroscopic observation of EB remelted ingot indicates that coarse and columnar grains grow in the direction parallel to ingot pulling direction. This can be explained by slow solidification (3mm/min), large temperature gradient and heat flow to this direction. The orientation of columnar structure was found to be <110>, <200> and <211> by the analysis of X-ray diffraction patterns. The contents of typical metallic impurities in Mo sintered bar are 1.2ppm Cr, 3ppm Fe, 44ppm Zr, 150ppm W. Most of metallic impurities were reduced below the order of ppm except zirconium and tungsten by the selective evaporation. In the removal of nonmetallic impurities, oxygen and carbon impurities were lowered from 120 to 6ppm and from 157 to 106ppm, respectively, after first melting. Although the purification effect was not significant with the number of remelting, Vickers hardness was reduced from 217 to 195 and 184 in sequence with increasing the number of remelting.

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DOE를 적용한 카메라폰 모듈용 비구면 Glass 렌즈의 가압성형조건 연구 (A Study on Pressing Conditions in the molding of Aspheric Glass Lenses for Phone Camera Module using Design of Experiments)

  • 김혜정;차두환;이준기;김상석;김정호
    • 한국전기전자재료학회논문지
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    • 제20권8호
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    • pp.720-725
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    • 2007
  • This study investigated the pressing conditions in the molding of aspheric glass lenses for the mega pixel phone camera module using the DOE method. Tungsten carbide (WC; Japan, Everloy Co., 002K),which contained 0.5 w% cobalt (Co), was used to build the mold. The mold surface was ultra-precision ground and polished, and its form accuracy (PV) was 0.85um in aspheric surface. We selected four factors, pressing temperature, force and time of first step, and force of second step, respectively, as the parameters of the pressing process. in order to reduce the number of experiments, we applied fractional factorial design considering the main effects and two-way interactions. The analysis results indicate that the only two main effects, the pressing temperature and the time of pressing step 1, are available for the form accuracy (PV) of the molded lens. The analysis results indicated that the best combination of the factors for lowering the form accuracy(PV) value of molded lens was to have them at their low levels.

고주파유도가열 연소합성에 의한 치밀한 WSi2-20vol.%SiC 복합재료 제조 및 기계적 특성 (Fabrication and Mechanical Properties of Dense WSi2-20vol.%SiC Composite by High-Frequency Induction-Heated Combustion Synthesis)

  • 오동영;김환철;이상권;손인진
    • 한국분말재료학회지
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    • 제12권1호
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    • pp.17-23
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    • 2005
  • Dense $WSi_2$-20vol.%SiC composite was synthesized by high-frequency induction-heated combustion synthesis(HFIHCS) method within 2 minutes in one step from elemental powder mixture of W, Si and C. Simultaneous combustion synthesis and densification were accomplished under the combined effects of an induced current and mechanical pressure. Highly dense $WSi_2$-20vol.%SiC with relative density of up to 97% was produced under simultaneous application of 60MPa pressure and the induced current. The average grain size of $WSi_2$ was about $5.2{\mu}m$. The hardness and fracture toughness values obtained were 1700kg/$mm^2$ and $4.4MPa{\cdot}m^{1/2}$, respectively.

$WO_3$를 이용한 박막형 슈퍼캐패시터의 제작 및 특성 평가 (Fabrication and Characterization of Thin Film Supercapacitor using $WO_3$)

  • 신호철;신영화;임재홍;윤영수
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 추계학술대회 논문집
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    • pp.575-578
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    • 2000
  • In this work, all solid-state thin film supercapacitor(TFSC) was fabricated using tungsten trioxide (WO$_3$) with a structure WO$_3$/LiPON/WO$_3$/Pt/TiO$_2$/Si (substrate). After TiO$_2$ was deposited on Si(100) wafer by d.c. reactive sputtering, the Pt current collector films were grown on TiO$_2$glue layer without breaking vacuum by d.c. sputtering. Fabrication conditions of WO$_3$ thin film were such that substrate temperature, working pressure, gas ratio of $O_2$/Ar and r.f. power were room temperature, 5 mTorr, 20% (O$_2$(8sccm)/Ar(32sccm)) and 200W, respectively. LiPON electrolyte film were grown on the WO$_3$ film using r.f. magnetron sputtering at room temperature. The XRD pattern of the as-deposited WO$_3$ thin film were shown no crystalline peak (amorphous). The SEM image of as-deposited WO$_3$ thin film showed that the surface is smooth and uniform. The capacitiy of as-fabricated TFSC was 0$\times$10$^{-2}$ F/$\textrm{cm}^2$-${\mu}{\textrm}{m}$.

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RF 마그네트론 스퍼터링에 의해 증착된 SMR 구조 FBAR 소자의 Bragg 반사층의 미세구조 특성에 관한 연구 (Micro structural characteristics of Bragg reflector of SMR type FBAR device deposited by RF magnetron sputtering)

  • 박성현;이순범;이능헌;신영화
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2005년도 제36회 하계학술대회 논문집 C
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    • pp.1992-1994
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    • 2005
  • In this study, Bragg reflector was formed as tungsten(W) and $SiO_2$ deposited by RF magnetron sputtering according to variable conditions of RF power and working pressure to apply to the SMR type FBAR device, one of the next generation mobile communication devices. The micro-structural properties such as a crystal orientation, roughness and micro- structure were measured by XRD, AFM and SEM and the best condition of Bragg reflector was elicited with analyzing that results of the thin films about each conditions. Finally, FBAR device was fabricated with applying the Bragg reflector was formed on the best condition and measured the resonance properties and compared other research and considered it.

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달성폐광산 주변 식물의 중금속 오염에 대한 지화학적 연구 (Geochemical Study on Heavy Metal Pollution of Plants at Dalseong Abandoned Mine)

  • 이재영;이인호;김석기
    • 자원환경지질
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    • 제31권3호
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    • pp.223-233
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    • 1998
  • The environments in the vicinity of the Dalseong mine has been much contaminated by heavy metals related to CuW ore deposit, which is of hydrothermal pipe type mineralized by quartz monzonite in the andesitic rocks. Chalcopyrite and wolframite are major ore minerals and sphalerite, galena and others are associated. To investigate the contamination of heavy metals in plants, samples of plants and soils were analysed by ICP for Fe, Mn, Cu, Pb, Zn, Ni, Co, Cd and Cr. Most of ore-related heavy metals are anomalously high in plants and soils, which were contaminated by the development of Taehan Tungsten Mining Company. The mine produced 48,704 tons (M/T) of 4 wt.% Cu and 1,620 tons (S/T) of 70 wt.% of $WO_3$ during active mining activity from 1961 to 1971 but was closed in 1975. Wild plants growing at the mine area may be used to remove heavy metals form soils, which cause contaminations of plants, stream waters and groundwaters in the vicinity of the mine.

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촉매반응 화학기상증착법을 이용한 유기발광소자의 박막 봉지 (Thin Film Passivation of Organic Light Emitting Diodes by Catalyzer Enhanced Chemical Vapor Deposition (CECVD))

  • 김한기;문종민;배정혁;정순욱;김명수
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.71-72
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    • 2006
  • We report on plasma damage free chemical vapor deposition technique for the thin film passivation of organic light emitting diodes (OLEDs), organic thin film transistor (OTFT) and flexible displays using catalyzer enhanced chemical vapor deposition (CECVD). Specially designed CECVD system has a ladder-shaped tungsten catalyzer and movable electrostatic chuck for low temperature deposition process. The top emitting OLED with thin film $SiN_x$ passivation layer shows electrical and optical characteristics comparable to those of the OLED with glass encapsulation. This indicates that the CECVD technique is a promising candidate to grow high-quality thin film passivation layer on OLED, OTFT, and flexible displays.

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미세 와이어의 전단에 관한 연구 (A study on the shearing of the straightened micro-wire)

  • 신용승;홍남표;김병희;김헌영;김웅겸
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 금형가공,미세가공,플라스틱가공 공동 심포지엄
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    • pp.175-180
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    • 2005
  • In this study, we have developed a novel wire straightener which uses the direct heating method (DHM) fer straightening the micro wire. Also, we have developed a shearing device for cutting the micro wire. In order to avoid the surface oxidization, we supplied the inert gas(Ar) during the heating process and examined the effect of gas flow rate. The effects of the tension and the current applied to the tungsten micro wires were also thoroughly studied. From various experiments and analyses, we could obtain fine straightness $(\approx1\;{\mu}m/1000\;{\mu}m)$ and roundness $(<{\pm}2{\mu}m\;/100{\mu}m)$ when the tension is $500\~~600gf$ and the current is about 1.5A. for burrfree cutting, counter-punch method which two cutters moving contrary was used. The cutting blade has various U-groove angle where upper $10^{\circ}$, $mid:25^{\circ}$, lower $0^{\circ}$. After the shearing process, we confirmed the shearing section.

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