Purpose: There are some advantages of the acrylic resin denture base ; appropriate strength, volume safety, simple processing apparatus, and low cost. But, it have a weakness for fracture by intense pressure or shock. However, the repairs for resin denture base are possible using various materials and techniques. There is a few studies in repairs for resin denture base, but not clinical researches. And there is no studies in absorbed saliva into the region of fracture and bond strength. This study is to observe re-bond strength of resin denture base after repairing under saliva absorption. Methods: The samples were made of heat curing resin and the rectangular parallelepiped specimens which were 50mm long, 10mm wide and 3mm high. The four different groups immersed in the artificial saliva for 2 weeks were prepared, 1) no repaired control samples, 2) immediately repaired samples, 3) repaired samples after 1 day dry, and 4) repaired samples after 3 days dry. The prepared samples were repaired by two different curing materials, self curing resin and heat curing resin method. Each groups composed of 10 specimens were experimented with the three point bending tests for bonding strength measuring Results: There were under condition absorbed in the artificial saliva and repaired by self curing resin method, repaired specimens after 1 day and 3 days dry groups had higher values of bonding strengths than control group, and bonding strengths of immediately repaired samples were similar to those of control samples (p<0.05). There were under condition immersed in the artificial saliva and repaired by heat curing resin method, immediately repaired samples showed similar values to bonding strengths of control groups, and repaired samples after 1 day and 3 days dry groups were lower than those of control group (p>0.05). Conclusion: In this study, the repairs for resin denture base were remarkably high values of bonding strengths than those of the past, and showed that have stable bonding strengths independent of saliva absorption of denture base, so present repairs for resin denture base can be performed, regardless of saliva conditions.
Cifuentes, Hector;Lozano, Miguel;Holusova, Tana;Medina, Fernando;Seitl, Stanislav;Fernandez-Canteli, Alfonso
International Journal of Concrete Structures and Materials
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v.11
no.2
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pp.215-228
/
2017
A new approach for measuring the specific fracture energy of concrete denoted modified disk-shaped compact tension (MDCT) test is presented. The procedure is based on previous ideas regarding the use of compact tension specimens for studying the fracture behavior of concrete but implies significant modifications of the specimen morphology in order to avoid premature failures (such as the breakage of concrete around the pulling load holes). The manufacturing and test performance is improved and simplified, enhancing the reliability of the material characterization. MDCT specimens are particularly suitable when fracture properties of already casted concrete structures are required. To evaluate the applicability of the MDCT test to estimate the size-independent specific fracture energy of concrete ($G_F$),the interaction between the fracture process zone of concrete andthe boundary of theMDCTspecimens at the end of the test is properly analyzed. Further, the experimental results of $G_F$ obtained by MDCT tests for normal- and high-strength self-compacting concrete mixes are compared with those obtained using the well-established three-point bending test. The procedure proposed furnishes promising results, and the $G_F$ values obtained are reliable enough for the specimen size range studied in this work.
The paper presents the study on a change in modal parameters and structural stiffness of cable-stayed Fiberline Bridge made entirely of Glass Fiber Reinforced Polymer (GFRP) composite used for 20 years in the fjord area of Kolding, Denmark. Due to this specific location the bridge structure was subjected to natural aging in harsh environmental conditions. The flexural properties of the pultruded GFRP profiles acquired from the analyzed footbridge in 1997 and 2012 were determined through three-point bending tests. It was found that the Young's modulus increased by approximately 9%. Moreover, the influence of the temperature on the storage and loss modulus of GFRP material acquired from the Fiberline Bridge was studied by the dynamic mechanical analysis. The good thermal stability in potential real temperatures was found. The natural vibration frequencies and mode shapes of the bridge for its original state were evaluated through the application of the Finite Element (FE) method. The initial FE model was created using the real geometrical and material data obtained from both the design data and flexural test results performed in 1997 for the intact composite GFRP material. Full scale experimental investigations of the free-decay response under human jumping for the experimental state were carried out applying accelerometers. Seven natural frequencies, corresponding mode shapes and damping ratios were identified. The numerical and experimental results were compared. Based on the difference in the fundamental natural frequency it was again confirmed that the structural stiffness of the bridge increased by about 9% after 20 years of service life. Data collected from this study were used to validate the assumed FE model. It can be concluded that the updated FE model accurately reproduces the dynamic behavior of the bridge and can be used as a proper baseline model for the long-term monitoring to evaluate the overall structural response under service loads. The obtained results provided a relevant data for the structural health monitoring of all-GFRP bridge.
Seung Won Choi;Cho Won Baek;Seon Yeol Lee;Van Thong Nguyen;Dong Joo Kim
Journal of the Korean Recycled Construction Resources Institute
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v.11
no.4
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pp.332-340
/
2023
This study investigated the effects of nanoparticles on the fracture toughness of cement mortar. Three-point bending tests, compressive tests, and slump tests were conducted on cement mortars reinforced with carbon nanotubes(CNTs), nanosilica(NS), and nano calcium carbonate(NC), respectively. Cement mortar with a water-to-cement ratio and a sand-to-cement ratio of 0.45 and 1.5, respectively, and reinforced with 0 and 2 vol.% of 19.5 mm steel fibers, respectively, was used. Reinforcement with nanoparticles partially improved the fracture toughness and compressive strength of the cement mortar. However, in the case of cement mortar reinforced with steel fibers, the reinforcement with nanoparticles was found to reduce the flowability of the mortar, adversely affecting the dispersion of steel fibers, and ultimately leading to a decrease in fracture toughness, contrary to the intended enhancement. Additional research is needed to improve the decrease in mortar fluidity caused by the reinforcement with nanoparticles.
In this study, partially stabilized zirconia was synthesized using a chemical $Y_2O_3$ stabilizer and hydrothermal method. First, $YCl_3-6H_2O$ and $ZrCl_2O-8H_2O$ was dissolved in distilled water. Y-TZP (a $Y_2O_3$-doped toughened zirconia polycrystalline precursor) was also prepared by conventional co-precipitates in the presence of an excess amount of $NH_4OH$ solution under a fixed pH of 12. The Y-TZP precursors were filtered and repeatedly washed with distilled water to remove $Cl^-$ ions. $ZrO_2$-Xmol%$Y_2O_3$ powder was synthesized by a hydrothermal method using Teflon Vessels at $180^{\circ}C$ for 6 h of optimized condition. The powder added with the Xmol%- $Y_2O_3$ (X = 0,1,3,5 mol%) stabilizer of the $ZrO_2$ was synthesized. The crystal phase, particle size, and morphologies were analyzed. Rectangular specimens of $33mm{\times}8mm{\times}3$ mm for three-point bend tests were used in the mechanical properties evaluation. A teragonal phase was observed in the samples, which contains more than 3 mol% $Y_2O_3$. The $3Y-ZrO_2$ agglomerated particle size was measured at $7.01{\mu}m$. The agglomerated particle was clearly observed in the sample of 5 mol % $Y_2O_3-ZrO_2$, and and the agglomerated particle size was measured at 16.4 um. However, a 20 nm particle was specifically observed by FE-SEM in the sample of 3 mol% $Y_2O_3-ZrO_2$. The highest bending fracture strength was measured as 321.3 MPa in sample of 3 mol% $Y_2O_3-ZrO_2$.
Kwon, Yongchai;Seok, Jongwon;Lu, Jian-Qiang;Cale, Timothy;Gutmann, Ronald
Korean Chemical Engineering Research
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v.45
no.5
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pp.466-472
/
2007
A technology platform for wafer-level three-dimensional integration circuits (3D-ICs) is presented, and that uses wafer bonding with low-k polymeric adhesives and Cu damascene inter-wafer interconnects. In this work, one of such technical platforms is explained and characterized using a test vehicle of inter-wafer 3D via-chain structures. Electrical and mechanical characterizations of the structure are performed using continuously connected 3D via-chains. Evaluation results of the wafer bonding, which is a necessary process for stacking the wafers and uses low-k dielectrics as polymeric adhesive, are also presented through the wafer bonding between a glass wafer and a silicon wafer. After wafer bonding, three evaluations are conducted; (1) the fraction of bonded area is measured through the optical inspection, (2) the qualitative bond strength test to inspect the separation of the bonded wafers is taken by a razor blade, and (3) the quantitative bond strength is measured by a four point bending. To date, benzocyclobutene (BCB), $Flare^{TM}$, methylsilsesquioxane (MSSQ) and parylene-N were considered as bonding adhesives. Of the candidates, BCB and $Flare^{TM}$ were determined as adhesives after screening tests. By comparing BCB and $Flare^{TM}$, it was deduced that BCB is better as a baseline adhesive. It was because although wafer pairs bonded using $Flare^{TM}$ has a higher bond strength than those using BCB, wafer pairs bonded using BCB is still higher than that at the interface between Cu and porous low-k interlevel dielectrics (ILD), indicating almost 100% of bonded area routinely.
We examined various existing threshold methods for the determination of the first arrival time of acoustic emission (AE), and developed a new variable threshold method that could determine the first arrival time of AE more accurately and more quickly than existing methods. The new method, a modification of an existing threshold method, does not fix the threshold, but applies variable thresholds for the AE signals according to noise analysis. Two- and three-dimensional models were established to test the effectiveness of the new method. It could determine source locations of AE in a two-dimensional model 38.3% more accurately than the pre-existing threshold methods. Its accuracy improvement over the existing methods in a three-dimensional model was about 15.2%. A practical test involved measuring the source locations of AE during three-point bending tests of granite cores. The new method placed the sources closer to the fracture plane than did the pre-existing methods, indicating its superior (and quicker) ability to determine the source locations of AE.
Journal of the Computational Structural Engineering Institute of Korea
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v.35
no.2
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pp.73-82
/
2022
The study presents a three-dimensional approach to simulate the nonlinear behavior of a 72 m long Ultra High Performance Fiber Reinforced Concrete (UHPFRC) pre-stressed box girder for a pedestrian bridge in Busan, South Korea. The concrete damage plasticity (CDP) model is adopted to model the non-linear behavior of the UHPFRC material, in which the material properties are obtained from uniaxial compressive and tensile tests. The simulation model based on the proposed stress-strain curve is validated by the results of four-point bending model tests of a 50 m UHPFRC pre-stressed box girder. The results from the simulation models agree with the experimental observations and predict the flexural behavior of the 50 m UHPFRC pre-stressed box girder accurately. Afterward, the validated model is utilized to investigate the flexural behavior of the 72 m UHPFRC pre-stressed box girder. Here, the load-deflection curve, stress status of the girder at various load levels, and connection details is analyzed. The load-deflection curve is also compared with design load to demonstrate the great benefit of the slender UHPFRC box girder. The obtained results demonstrate the applicability of the nonlinear finite element method as an appropriate option to analyze the flexural behavior of pre-stressed long-span girders.
Altunisik, Ahmet Can;Bayraktar, Alemdar;Ozdemir, Hasan
Smart Structures and Systems
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v.10
no.2
/
pp.131-154
/
2012
In this paper, it is aimed to determine the seismic behaviour of highway bridges by nondestructive testing using ambient vibration measurements. Eynel Highway Bridge which has arch type structural system with a total length of 216 m and located in the Ayvaclk county of Samsun, Turkey is selected as an application. The bridge connects the villages which are separated with Suat U$\breve{g}$urlu Dam Lake. A three dimensional finite element model is first established for a highway bridge using project drawings and an analytical modal analysis is then performed to generate natural frequencies and mode shapes in the three orthogonal directions. The ambient vibration measurements are carried out on the bridge deck under natural excitation such as traffic, human walking and wind loads using Operational Modal Analysis. Sensitive seismic accelerometers are used to collect signals obtained from the experimental tests. To obtain experimental dynamic characteristics, two output-only system identification techniques are employed namely, Enhanced Frequency Domain Decomposition technique in the frequency domain and Stochastic Subspace Identification technique in time domain. Analytical and experimental dynamic characteristic are compared with each other and finite element model of the bridge is updated by changing of boundary conditions to reduce the differences between the results. It is demonstrated that the ambient vibration measurements are enough to identify the most significant modes of highway bridges. After finite element model updating, maximum differences between the natural frequencies are reduced averagely from 23% to 3%. The updated finite element model reflects the dynamic characteristics of the bridge better, and it can be used to predict the dynamic response under complex external forces. It is also helpful for further damage identification and health condition monitoring. Analytical model of the bridge before and after model updating is analyzed using 1992 Erzincan earthquake record to determine the seismic behaviour. It can be seen from the analysis results that displacements increase by the height of bridge columns and along to middle point of the deck and main arches. Bending moments have an increasing trend along to first and last 50 m and have a decreasing trend long to the middle of the main arches.
Carbon woven fabric/C/SiC composites were fabricated by multiple impregnations of carbon woven fabric/carbon preform with the polymer precursor of SiC, i.e., polycarbosilane. In addition, two kinds of low density carbon/carbon preforms which had different fiber volume fraction and fiber orientation, i.e., a carbon woven fabric(${\thickapprox}$55 vol%)/carbon and a chopped carbon fiber${\thickapprox}$40 vol%)/carbon composites, were reaction-bonded with a silicon melt at 1$700^{\circ}C$ in a vacuum to fabricate dense carbon fiber/Si/SiC composites. The reaction-bonding process increased the density to ~2.1 g/$cm^3$ from 1.6 g/$cm^3$ and 1.15 g/$cm^3$ of a carbon woven and a chopped carbon preforms, respectively. All of the composites fractured with extensive fiber pull-out. The higher the density the higher the stiffness and proportional limit stress. The mechanical properties obtained from a three-point bend and tension tests were compared. The ratios of the peak tensile stresses to the bending strengths of a carbon woven and a chopped carbon composites were about one-third, respectively. The carbon woven fabric/Si/SiC composites with density of 2.06 g/$cm^3$ showed ~120 MPa of ultimate strength and ~80 MPa of proportional limit in bend testing.
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