• 전자공학회논문지T
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• 제36T권2호
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• pp.1-7
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• 1999

본 연구는 진공증착중합법에 의해 폴리이미드를 제작하고 박막의 절연파괴특성을 자기절연회복법에 의해 측정하였다. PMDA(Pyromellitic dianhydride)와 DDE(4,4'-diaminodiphenyl ether)를 증착 중합하여 Polyamic-acid(PAA)를 형성하고 이를 열처리함으로서 폴리이미드를 제조하였다. 제조된 박막의 특성을 조사하기 위해 주사형 전자현미경(SEM), 적외선분광장치(FT-IR) 및 오저전자분광장치(AES)를 사용하였다. 절연파괴특성 실험은 동일 시료에서 50회를 반복하였으며 25회 이상에서 절연파괴전계는 포화되었다. 열처리 온도를 200${^\circ}C$, 250$^{\circ}C$, 300$^{\circ}C$ 및 350${^\circ}C$로 변화했을 때 절연파괴전계는 1.21MV/cm, 3.94MV/cm, 4.61MV/cm, 4.55MV/cm로 변화하였다.

• 한국지반공학회논문집
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• 제27권3호
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• pp.75-83
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• 2011

일반적인 불포화지반의 거동뿐만 아니라, 열과 관련된 분야, 지반환경 분야 등 다양한 분야에서 불포화 다공질 재료의 열적-수리적-역학적으로 결합된 문제들이 대두되면서 이러한 문제들을 해석하기 위한 수치도구 개발의 필요성이 대두되고 있다. 본 논문에서는 거시적 접근법(macroscopic approach)에 근거하여 불포화지반에 대한 열-수리-역학거동의 수식화를 하였다. 흙, 물, 공기에 대한 질량보존의 법칙, 에너지 보존법칙, 그리고 하중평형 조건식으로부터 결합된(coupled) 4개의 지배방정식을 유도하였다. Galerkin 간략화와 시간적분으로부터 주 변수인 변위(u), 가스압($P_g$), 유체압($P_1$), 온도(T)를 Newton의 반복과정을 이용하여 구하는 유한요소 프로그램(FEM)을 작성하였다. 개발된 프로그램을 이용하여 다공질재료에서 2상 흐름 문제 중 일차원 배수실험(u-$P_g-P_1$), 온도 압밀(u-$P_1$-T), 그리고 지표면 온도변화에 의한 말뚝의 주변지반에 대한 영향(u-$P_1$-T)에 대하여 수치해석을 수행하고 논의하였다.

• Advances in materials Research
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• 제6권2호
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• pp.169-184
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• 2017

Electro-Discharge machining (EDM) is a thermal process comprising a complex metal removal mechanism. This method works by forming of a plasma channel between the tool and the workpiece electrodes leading to the melting and evaporation of the material to be removed. EDM is considered especially suitable for machining complex contours with high accuracy, as well as for materials that are not amenable to conventional removal methods. However, several phenomena can arise and adversely affect the surface integrity of EDMed workpieces. These have to be taken into account and studied in order to optimize the process. Recently, artificial neural networks (ANN) have emerged as a novel modeling technique that can provide reliable results and readily, be integrated into several technological areas. In this paper, we use an ANN, namely, the multi-layer perceptron and the back propagation network (BPNN) to predict the mean surface roughness of electro-discharge machined surfaces. The comparison of the derived results with experimental findings demonstrates the promising potential of using back propagation neural networks (BPNNs) for getting a reliable and robust approximation of the Surface Roughness of Electro-discharge Machined Components.

• 대한기계학회논문집B
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• 제28권12호
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• pp.1557-1566
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• 2004

A flame extinction phenomenon is a typical unsteady process in combustion. Flame extinction is characterized by various physical phenomena, such as convection, diffusion, and the production of heat and mass. Flame extinction can be achieved by either increasing the strain rate or curvature, by diluting an inert gas or inhibitor, or by increasing the thermal or radiant energy loss. Though the extinction is an inherently transient process, steady and quasi-steady approaches have been used as useful tools for understanding the flame extinction phenomenon. Recently, unsteady characteristics of flames have been studied by many researchers, and various attempts have been made to understand unsteady flame behavior, by using various extinction processes. Representative parameters for describing flame, such as flame temperature, important species related to reactions, and chemi-luminescence of the flame have been used as criterions of flame extinction. In these works, verification of each parameter and establishing the proper criterions of the extinction has been very important. In this study, a time-dependent flame temperature and an OH radical concentration were measured using optical methods, and the instantaneous change of the flame luminosity was also measured using a high-speed ICCD (HICCD) camera. We compare the unsteady extinction points obtained by three different methods, and we discuss transient characteristics of maximum flame temperature and OH radical distribution near the extinction limit.

• 한국재료학회지
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• 제26권1호
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• pp.54-60
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• 2016

We have investigated the crystallization mechanism of the lithium disilicate ($Li_2O-2SiO_2$, LSO) glass particles with different sizes by isothermal and non-isothermal processes. The LSO glass was fabricated by rapid quenching of melt. X-ray diffraction and differential scanning calorimetry measurements were performed. Different crystallization models of Johnson-Mehl-Avrami, modified Ozawa and Arrhenius were adopted to analyze the thermal measurements. The activation energy E and the Avrami exponent n, which describe a crystallization mechanism, were obtained for three different glass particle sizes. Values of E and n for the glass particle with size under $45{\mu}m$, $75{\sim}106{\mu}m$, and $125{\sim}150{\mu}m$, were 2.28 eV, 2.21 eV, 2.19 eV, and ~1.5 for the isothermal process, respectively. Those values for the non-isothermal process were 2.4 eV, 2.3 eV, 2.2 eV, and ~1.3, for the isothermal process, respectively. The obtained values of the crystallization parameters indicate that the crystallization occurs through the decreasing nucleation rate with a diffusion controlled growth, irrespective to the particle sizes. It is also concluded that the smaller glass particles require the higher heat absorption to be crystallized.

• 한국재료학회지
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• 제27권2호
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• pp.76-81
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• 2017

Recently, there have been many efforts to establish suitable processes for recycling fly ash, which is produced in thermal power plants and which poses serious environmental problems. Use of fly ash as a major ingredient of ceramic tiles can increase fly ash utilization, as well as reduce the cost of raw materials in ceramic tile production. In this study, the effects of fly ash addition on ceramic tile properties such as bending strength, water absorption and porosity were investigated. A manufacturing process of ceramic tile was developed for utilization of fly ash with high carbon content. In this approach, it is important to hold the ceramic tiles at a temperature that is sufficient for carbon oxidation, before the pores supplying oxygen to the inside of the ceramic tile are sealed. Ceramic wall tiles were manufactured with 0-40wt% of fly ash addition. The water absorption and porosity of the fired body were slightly changed with increasing fly ash content up to 30wt% and decreased with greater amounts of fly ash addition. The bending strength of ceramic tile including 10wt% fly ash increased, reaching a level comparable to that of ceramic tile without fly ash.

• 대기
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• 제16권3호
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• pp.203-213
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• 2006

The objective of this paper is to investigate the effects of physical parameterization on the simulation of a snowfall event over Korea caused by air-mass transformation by using the PSU/NCAR MM5. A heavy snowfall event over Korea during 3-5 January 2003 is selected. In addition to the control experiments employing simple-ice microphysics scheme, MRF PBL scheme, and original surface layer process, three consequent physics sensitivity experiments are performed. Each experiment exchanges microphysics (Reisner Graupel), boundary layer (YSU PBL) schemes, and revised surface layer process with a reduced thermal roughness length for the control run. The control run reproduces an overall pattern of snowfall over Korea, but with a high bias by a factor of about 2. As revealed in the previous studies, the cloud microphysics and PBL parameterizations do not show a significant sensitivity for the case of snowfall. A more sophisticated cloud processes does not reveal a discernible effect on the simulated snowfall. Further, high bias in snowfall is exaggerated when a more realistic PBL scheme is employed. On the other hand, it is found that the revised surface layer process plays a role in improving the prediction of snowfall by reducing it. Thus, it is found that a realistic design of surface layer physics in mesoscale models is an important factor to the reduction of systematic bias of the snowfall over Korea that is caused by air-mass transformation over the Yellow sea.

• 한국수산과학회지
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• 제31권6호
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• pp.829-834
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• 1998

옥수수 전분가수분해물의 용해도는 D.E. 값이 높을수록 증가하였고, 10 이상에서는 거의 차이가 없었다. $T_g^{'}$ 값은 D.E. 값이 증가함에 따라 감소하는 직선적인 관계를 나타내었다. Alkaline phosphatase의 동결계에서 거동은 glass cynamic mechanism, 즉 효소의 가수분해 속도는 첨가된 물질의 $T_g^{'}$ 이하의 온도에서 지연되거나 억제되었다. 옥수수전분 가수분해물은 동결계에서 유리전이온도를 높임으로서 동결계가 유리상태로 되고 따라서 점도는 높아지고 단백질은 분자간 접촉의 기회가 줄어들어 단백질이 보호된다는 cryostabilization mechanism으로 설명 가능하였다.

• 한국수산과학회지
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• 제18권4호
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• pp.374-380
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• 1985

12년간($1958{\sim}1969$) 동해의 경위도 2도 간격 격자상의 자료에 대한 조화분석을 통하여 동해의 표면수온, 기온 및 해면온도차의 계절적인 변화를 분석한 결과에 의하면, 동해에서 수온과 기온은 복사에너지 뿐만 아니라 해류와 계절풍에 의한 열이류의 영향을 크게 받고 있다. 동해에서 쓰시마난류가 흐르는 남동해역은 같은 위도상의 북서해역에 비하여 표면수온과 기온의 연평균이 높고 연교차의 폭이 작다. 이는 쓰시마난류에 의한 열이류 변화의 위상이 복사에너지 변화의 위상과 반대여서 계절적인 온도의 변화폭을 줄이기 때문이다. 동해에서 연평균 수온은 연평균 기온보다 $2{\sim}4^{\circ}C$ 높으며, 수온과 기온간의 차이는 계절에 따라 크게 변한다. 즉 여름에는 표면수온과 기온간에 차이가 거의 없지만, 겨울에는 수온이 기온보다 $6{\sim}10^{\circ}C$ 높으며, 겨울에 헌혈과 증발열을 통하여 해면으로부터 대기로 공급되는 에너지는 태양복사에너지의 2배에 달한다.

• Journal of Microbiology and Biotechnology
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• 제17권4호
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• pp.624-631
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• 2007

Thermostable protease is very effective to improve the industrial processes in many fields. Two thermostable extracellular proteases from the culture supernatant of the thermophilic fungus Chaetomium thermophilum were purified to homogeneity by tractional ammonium sulfate precipitation, ion-exchange chromatography on DEAE-Sepharose, and Phenyl-Sepharose hydrophobic interaction chromatography. By SDS-PAGE, the molecular mass of the two purified enzymes was estimated to be 33 kDa and 63 kDa, respectively. The two proteases were found to be inhibited by PMSF, but not by iodoacetamide and EDTA. The 33 kDa protease (PRO33) exhibited maximal activity at pH 10.0 and the 63kDa protease (PRO63) at pH5.0. The optimum temperature for the two proteases was $65^{\circ}C$. The PRO33 had a $K_m$ value of 6.6mM and a $V_{max}$ value of $10.31{\mu}mol/l/min$, and PRO63 l7.6mM and $9.08{\mu}mol/l/min$, with casein as substrate. They were thermostable at $60^{\circ}C$. The protease activity of PRO33 and PRO63 remained at 67.2% and 17.31%, respectively, after incubation at $70^{\circ}C$ for 1h. The thermal stability of the two enzymes was significantly enhanced by $Ca^{2+}$. The residual activity of PRO33 and PRO63 at $70^{\circ}C$ after 60min was approximately 88.59% and 39.2%, respectively, when kept in the buffer containing $Ca^{2+}$. These properties make them applicable for many biotechnological purposes.