• Title/Summary/Keyword: thermal processes

Search Result 1,085, Processing Time 0.027 seconds

Synthesis and Characterization of Alumina Composite Membrane by Al Evaporation and Thermal Oxidation (알루미늄의 진공증발과 열산화에 의한 알루미나 복합분리막의 제조 및 특성분석)

  • 이동호;최두진;현상훈
    • Journal of the Korean Ceramic Society
    • /
    • v.32 no.3
    • /
    • pp.349-358
    • /
    • 1995
  • The ceramic composite membrane was synthesized by thermal oxidation after evaporation of Al on the support prepared by slip casting process. Oxidation was performed at $700^{\circ}C$ and 80$0^{\circ}C$ under dry oxygen atmosphere. It was considered as optimum oxidation condition that the membrane showed a knudsen behaviro. A further oxidation resulted in an increase of gas permeability because top layer became densified. Then, a multi-layered composite membrane was synthesized through a sol-gel method, evaporation and thermal oxidation of Al coating processes. While the membrane was thermally stable up to 80$0^{\circ}C$, gas permeability was rapidly decreased even at a slight amount of deposition of Al.

  • PDF

Evaluation of Thermal Property and Fluidity with Underfill for BGA Package (BGA 패키지를 위한 언더필의 열적 특성과 유동성에 관한 연구)

  • Noh, Bo-In;Lee, Bo-Young;Kim, Soo-Jung;Jung, Seung-Boo
    • Journal of Welding and Joining
    • /
    • v.24 no.2
    • /
    • pp.57-63
    • /
    • 2006
  • In this study, the curing kinetics and thermal degradation of underfill were investigated using differential scanning calorimetry (DSC) and thermo gravimetry analysis (TGA). The mechanical and thermal properties of underfill were characterized using dynamic mechanical analysis (DMA) and thermo-mechanical analysis (TMA). Also, we presented on underfill dispensing process using Prostar tool. The non-isothermal DSC scans at various heating rates, the exothermic reaction peak became narrower with increasing the heating rate. The thermal degradation of underfill was composed of two processes, which involved chemical reactions between the degrading polymer and oxygen from the air atmosphere. The results of fluidity phenomena were simulated using Star CD program, the fluidity of the underfills with lower viscosity was faster.

Spray Coating Technology (스프레이 코팅 기술)

  • Lee, Chang-Hee
    • Journal of ILASS-Korea
    • /
    • v.13 no.4
    • /
    • pp.193-199
    • /
    • 2008
  • Spray coating is a versatile surface modification technology in which coating is built-up based on the successive deposition of micron-scaled particles. Depending on the coating materials, the coatings can meet the required mechanical properties, corrosion resistance, and other properties of base materials. Spraying processes are mainly classified into thermal and kinetic spraying according to their bonding mechanism and deposition characteristics. Specifically, thermal spraying process can be further classified into many categories based on the design and mechanism of the process, such as frame spraying, arc spraying, atmospheric plasma spraying (APS), and high velocity oxygen-fuel (HVOF) spraying, etc. Kinetic spraying or cold gas dynamic spraying is a newly emerging coating technique which is low-temperature and high-pressure coating process. In this paper, overall view of thermal and kinetic spray coating technologies is discussed in terms of fundamentals and industrial applications. The technological characteristics and bonding mechanism of each process are introduced. Deposition behavior and properties of technologically remarkable materials are reviewed. Furthermore, industrial applications of spray coating technology and its potentials are prospected.

  • PDF

Analysis and Experiment on Cryogenic Refrigeration Using Solid Nitrogen (고체 질소를 이용한 극저온 냉동의 해석 및 실험)

  • 변정주;이윤숙;장호명
    • Progress in Superconductivity and Cryogenics
    • /
    • v.3 no.2
    • /
    • pp.77-83
    • /
    • 2001
  • The thermal characteristics of solid nitrogen are investigated by experiment and analysis for the purpose of evaluating its feasibility as a cooling medium for HTS (high T$_{c}$ superconductor) magnets. A cryostat to refrigerate a liquid-nitrogen container well below its freezing temperature with a 2-stage GM cryocooler is designed and constructed. The spatial distribution of temperature is measure as a function of time during the freezing and melting processes. from which the thermal diffusivity of solid nitrogen can be approximately calculated. the freezing process is formulated and solved by the integral method with an assumption of phase equilibrium at the solid-liquid interface and experimental observation. It may be concluded that the thermal diffusion in solid phase is much slower than in liquid and the degree of super-saturation is quite severe in the solidification of nitrogen.n.

  • PDF

Overview on Thermal Management Technology for High Power Device Packaging (파워디바이스 패키징의 열제어 기술과 연구 동향)

  • Kim, Kwang-Seok;Choi, Don-Hyun;Jung, Seung-Boo
    • Journal of the Microelectronics and Packaging Society
    • /
    • v.21 no.2
    • /
    • pp.13-21
    • /
    • 2014
  • Technology for high power devices has made impressive progress in increasing the current density of power semiconductor, system module, and design optimization, which realize high power systems with heterogeneous functional integration. Depending on the performance development of high power semiconductor, packaging technology of high power device is urgently required for efficiency improvement of the device. Power device packaging must provide superior thermal management due to high operating temperature of power modules. Here we, therefore, review critical challenges of typical power electronics packaging today including core assembly processes, component materials, and reliability evaluation regulations.

Effects of Thermal Treatments on Resonance Characteristics of FBAR Devices

  • Mai, Linh;Song, Hae-Il;Tuan, Le Minh;Su, Pham Van;Yoon, Gi-Wan
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
    • /
    • v.9 no.1
    • /
    • pp.376-380
    • /
    • 2005
  • The paper presents some methods to improve characteristics of film bulk acoustic resonator (FBAR) devices. The FBAR devices were fabricated on Bragg reflectors. Thermal treatments were done by sintering and/or annealing processes. The measurement showed a considerable improvement of return loss (S$_{11}$) and quality factor (Q$_{s/p}$). These thermal techniques seem very promising for enhancing FBAR resonance performance.

  • PDF

The Improvements of FBAR Devices performances by Thermal Annealing Methods

  • Mai, Linh;Song, Hae-Il;Le, Minh-Tuan;Pham, Van-Su;Yoon, Gi-Wan
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
    • /
    • v.9 no.2
    • /
    • pp.311-315
    • /
    • 2005
  • In this paper, we emphasize the advantage of thermal annealing treatments for improvement characteristics of film bulk acoustic resonator (FBAR) devices. The FBAR devices were fabricated on multi-layer thin films, namely, Bragg reflectors. Sintering and/or annealing processes were applied in our experiments. The measurements confirm once again a considerable improvement of return loss $(S_{11})$ and quality factor $(Q_{s/p})$. these thermal treatment techniques are really promising for enhancing performance of FBAR resonators in industry fabrication of RF devices.

  • PDF

Specimen Tests for a Process Development of the Electro-Nickel/Chrome Coating for a Thrust Chamber (연소기 적용 전해니켈/크롬도금 공정개발을 위한 시편시험)

  • Lim, Byoung-Jik;Ryu, Chul-Sung;Choi, Hwan-Seok
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2011.04a
    • /
    • pp.113-116
    • /
    • 2011
  • A total of 9 coating specimens were fabricated through 3 different processes to evaluate the availability and performance of a nickel/chrome coating for the protection of the inner wall of a thrust chamber operating on a condition of high temperature and pressure. Thickness and thermal conductivity of the specimens were measured and thermal shock test was conducted.

  • PDF

Thermal stability of nitric acid solutions of reducing agents used in spent nuclear fuel reprocessing

  • Obedkov, A.S.;Kalistratova, V.V.;Skvortsov, I.V.;Belova, E.V.
    • Nuclear Engineering and Technology
    • /
    • v.54 no.9
    • /
    • pp.3580-3585
    • /
    • 2022
  • The thermal stability of carbohydrazide, hydrazine nitrate, acetohydroxamic acid in nitric acid solutions has been studied at atmospheric pressure and above atmospheric pressure. The volumes of gaseous products of thermolysis and the maximum rate of gas evolution have been determined at atmospheric pressure. It has been shown that, despite the high rate of gas evolution and large volumes of evolved gases, the conditions for the development of autocatalytic oxidation are not created. Exothermic processes are observed in a closed vessel in the temperature range of 50-250 ℃. With an increase in the concentration of nitric acid, the temperatures of the onset of exothermic effects for all mixtures decrease, and the values of the total thermal effects of reactions increase, to the greatest extent for solutions with carbohydrazide.

Thermal Protection Shield Concept for Diamond Impregnated Tools

  • Tillmann, W.;Gathen, M.;Kronholz, C.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.875-876
    • /
    • 2006
  • For dry machining of mineral materials the Institute of Materials Engineering pursues a novel thermal protection shield concept for diamond tools, in which thermal insulating materials in diamond composite structures act as heat shield, which protects diamonds in deeper layers against high temperature and graphitisation. Before the effectiveness of this concept could be investigated suitable composites have to be manufactured. In this paper the powder metallurgical production processes of diamond-alumina-cobalt-composites with varying alumina and cobalt particle sizes, their microstructures and porosities are described. It could be observed that the distribution of small-sized alumina particles ($<70{\mu}m$) in the cobalt matrix is uniform and the porosity of the composite decrease.

  • PDF