• Proceedings of the KIEE Conference
• /
• 1988.11a
• /
• pp.241-245
• /
• 1988

This paper reports the experiments regarding to diagnosis techniques for power transformers by measuring dissipation factor and moisture contents of mineral oils. Thermal aging environments of mineral oils were varied by the specially designed systems. Thermal aging of elevated temperature of $90^{\circ}C$ was performed for about 240 and 460 hours, respectively. Dissipation factor, permittivity, and water content were measured. Our test samples were not exposed to air. Dissipation factor increased while permittivity did not change. The level of dissipation factor determining the insulating quality of mineral oil was compared with the previous results of resistivity and several correction factor.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2002.10a
• /
• pp.24-28
• /
• 2002

Composite reinforced fiber materials are used in lots of fields such as a part of aeronautic space, ship, machinery and so on because can make structure wished for necessary condition by control fiber direction and laminated sequence. As the use of advanced composites increase, specific techniques have been developed to repair changed composite structures. In order to repair the damaged part production high quality composite reinforced fiber are completed by control the surrounding temperature and press in autoclave. The quality is influenced heat exposure degree by chemical reaction for precessing. This study considerated influence limit of using by repair structure part and change of properties according to heat exposure degree for repairing.

• Proceedings of the KSME Conference
• /
• 2001.06a
• /
• pp.517-522
• /
• 2001

The purpose of this study is to investigate the thermal embrittlement and the mechanical properties of 2.25Cr-1Mo steel aged at high temperature and stress for 250 hours. Original, aged artificially material were tested to obtain the hardness and impact absorbed energy. Hardness and impact absorbed energy decreased with the increasing aging time. The carbide morphology with the thermal embrittlement was found to contribute to the mechanical property change by X-Ray diffraction method.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.6 no.4
• /
• pp.285-290
• /
• 2005

Mechanical properties of rubber mat are influenced by many factors such as compounding ingredients and states of cure, process of rubber, and fillers. Our study aim is to investigate influence of N-isopropyl-N'-chloro-P-phenylene diamine antioxidant on the thermal aging and ozone cracking. In this work, the degradation of antiblastic rubber mat was studied and suggested mechanism to involve two-types of degradation, thermal-aging and ozone-cracking both of which can be contained antioxidant or non-antioxidant.

• Elastomers and Composites
• /
• v.44 no.4
• /
• pp.442-446
• /
• 2009

Recovery behaviors of unfilled NR, BR, and SBR vulcanizates after aging with a circular deformation were compared to prevent the influence of reinforcing agent. Samples were aged at room temperature, 50, 70, and $90^{\circ}C$ for 10 days. Recovery increased by increasing the measurement time. Instantaneous recoveries less than 1.0 sec were obtained using the recovery variations with the measurement time. For aging at room temperature, difference in the recoveries of the rubber samples was not significant because the aging time was too short. However, for accelerated thermal aging at 50, 70, and $90^{\circ}C$, difference in the recoveries of the rubber samples was significant. Degree of recovery of BR specimen was higher than those of the others, while that of SBR was lowest. However, for accelerated thermal aging at $90^{\circ}C$, recovery of the NR sample was higher than that of the BR one. The initial recovery decreased by increasing the aging temperature and the decrement of SBR was larger than the others. The experimental results were explained with the resilience properties of rubbers and the crosslink density changes by thermal aging.

• Korean Journal of Materials Research
• /
• v.28 no.12
• /
• pp.702-708
• /
• 2018

This study deals with the effect of microstructure factors on the strain aging properties of API X70 pipeline steels with different microstructure fractions and grain sizes. The grain size and microstructure fraction of the API pipeline steels are analyzed by optical and scanning electron microscopy and electron backscatter diffraction analysis. Tensile tests before and after 1 % pre-strain and thermal aging treatment are conducted to simulate pipe forming and coating processes. All the steels are composed mostly of polygonal ferrite, acicular ferrite, granular bainite, and bainitic ferrite. After 1 % pre-strain and thermal aging treatment, the tensile test results reveal that yield strength, tensile strength and yield ratio increase, while uniform elongation decreases with an increasing thermal aging temperature. The increment of yield and tensile strengths are affected by the fraction of bainitic ferrite with high dislocation density because the mobility of dislocations is inhibited by interaction between interstitial atoms and dislocations in bainitic ferrite. On the other hand, the variation of yield ratio and uniform elongation is the smallest in the steel with the largest grain size because of the decrease in the grain boundary area for dislocation pile-ups and the presence of many dislocations inside large grains after 1 % pre-strain.

• Journal of Adhesion and Interface
• /
• v.3 no.2
• /
• pp.30-39
• /
• 2002

The effect of cure accelerator content on the change in crosslink density by thermal aging was studied for silica-filled natural rubber (NR) vulcanizates. Influence of silane coupling agent was also investigated. N-tert-Butyl-2-benzothiazole sulfenamide (TBBS) and bis-(3-(triethoxysilyl)-propyl)-tetrasulfide (TESPT) were used as a cure accelerator and a silane coupling agent, respectively. The crosslink density increased by thermal aging and the increasing level became larger as the aging temperature increased. The degree of crosslink density change of the vulcanizates without the silane coupling agent was larger than that of the vulcanizates containing the silane coupling agent. For the vulcanizates silane coupling agent, the activation energy for the crosslink density change decreased with increase of the cure accelerator content in the vulvanizate.

• Proceedings of the KIEE Conference
• /
• 1997.07d
• /
• pp.1465-1468
• /
• 1997

In this study we investigated the aging characteristic such as leakage current, dielectric loss, contact angle, of EPDM for outdoor use by thermal treatment. And also observed the color change of surface, changing of chemical ingredient of the marterials by optical microscope. SEMI, FTIR and EDX at the section and surface. The test result show that leakage current is increased with thermal aging time. contact angle and dielectric loss is slightly decreased. Moreover, micro-void or crack in bulk is severely increased with aging time. However, the result affect to the tan $\delta$ at bulk of EPDM. It seems that carrier sources are removed by degassing with heat treatment.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2010.06a
• /
• pp.81-81
• /
• 2010

This paper presents results of experimental investigations on natural ester regarding the breakdown strength. Aging of insulating material in a pole transformer has been studied by performing accelerated thermal aging test. Sealed aging test vessels containing copper, laminated core, Krapt paper and insulating oil(Natural oil and Mineral oil) were aged at $140^{\circ}C$ for 30days. Compared to the conventional transformer oil, electric property of the natural ester fluid is excellent.

• Journal of Powder Materials
• /
• v.2 no.3
• /
• pp.208-215
• /
• 1995

The aging effects on the characteristics of the melt spun Cu based shape memory alloys have been investigated by the microhardness test, X-ray diffraction, differential scanning calorimetry, scanning electron microscopy and transmission electron microscopy. After aged for specific times, hardness of the ribbons began to increase and shape memory capacity diminished. At the initial stage of aging the austenitic transformation temperatures increased gradually, but at last became nearly constant: That is, the aging deteriorated the thermal stability. The increase in hardness was due to the formation of the $\gamma_2$ precipitates. The loss in the shape memory capacity was due to the decrement of solute atoms in the matrix by the formation of the $\gamma_2$ precipitates. In this study, it was confirmed that Mn is an effective element for Improving the thermal stability.