• Bulletin of the Korean Chemical Society
• /
• 제19권10호
• /
• pp.1032-1036
• /
• 1998

Intercalation compounds of organic anions into layered double hydroxides (LDH) are synthesized by the coprecipitation route. X-ray diffraction data reveal that the intercalated terephthalate (TP), naphthalene-2,6-disulfonate (NA26), and anthraquinone-2,6-disulfonate (AQ26) are arranged with their molecular planes perpendicular to the hydroxide layer. HPLC data show that 26.2% of TP and 73.8% of AQ26 are cointercalated, whereas NA26 is not intercalated into the Zn/Al-LDH. These results indicate the possibility of a molecular recognition ability of Zn/Al-LDH. The molecular recognition ability of intercalation into Zn/Al-LDH is in the order AQ26 > TP >> NA26.

• Bulletin of the Korean Chemical Society
• /
• 제19권10호
• /
• pp.1113-1116
• /
• 1998

A new graphite intercalation compound (GIC), n-octylammonium tetrachlorofeffate(Ⅲ)-graphite, has been derived from well-known ferric chloride graphite intercalation compound. X-ray diffration study shows that the basal spacing of this new GIC is 20.8 Å. In order to investigate the local geometry around the iron atom in the graphite layers, X-ray absorption spectroscopy experiments were performed. The first discharge capacity of its exfoliated form is found to be 862 mAh/g, which is more than double the value of pristine graphite (384 mAh/g). Such a drastic increase implies that the exfoliated graphite is a promising electrode material.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2007년도 춘계학술대회B
• /
• pp.2935-2940
• /
• 2007

To diagnose circulatory diseases in the viewpoint of hemodynamics, we need to get quantitative hemodynamic information of blood flows related with the vascular diseases with high spatial resolution of tens micrometer and high temporal resolution in the order of millisecond. For investigating in-vivo hemodynamic phenomena, a new diagnosing technique combining medical radiography and PIV method was newly proposed and developed. This angiographic PIV technique consists of a medical X-ray tube, an X-ray CCD camera, a shutter module for double pulses of X-ray, and a synchronizer. The feasibility of the angiographic PIV technique was tested and quantitative flow velocity field distribution of a flow inside an opaque conduit was acquired by the developed system. It can be used for measuring flow phenomena of nontransparent fluids inside opaque conduits.

• 한국전산유체공학회:학술대회논문집
• /
• 한국전산유체공학회 2008년도 춘계학술대회논문집
• /
• pp.683-686
• /
• 2008

To diagnose vascular diseases from the viewpoint of hemodynamics, detailed quantitative hemodynamic information of related blood flows with a high spatial resolution of tens micrometer and a high temporal resolution in the order of millisecond were required. For investigating the hemodynamic phenomena of vascular circulatory diseases, a new diagnosing technique combining a medical radiography and PIV method was newly developed. This technique consisted of a medical X-ray tube, an X-ray CCD camera, a shutter module for double pulse-type X-ray source, and a synchronizer. Through several preliminary tests, the feasibility of the angiographic PIV technique was verified. For in-vivo measurements to real blood flows, we developed tracer microcapsules which were optimized to this system by encapsulating a contrast material of iodine with a matrix material of PVA (polyvinylpyrrolidone). In near future, the angiographic PIV technique would be useful for diagnosing hemodynamic phenomena of vascular diseases and for their early detection.

• The Korean Journal of Physiology
• /
• 제5권1호
• /
• pp.19-22
• /
• 1971

The effect based upon changes of body weight and effect of X-ray irradiation on tryptophan pyrrolase (TPO) activity in liver homogenate of albino rats was studied. 1. The average TPO activity of control group of 33 rats weighing $95{\sim}172g$\;was\;2.372{\pm}0.165{\mu}$ moles kynurenine/g protein/hr. 2. Correlation between body weight of 33 rats and its TPO activity was not showed practically(r=0.011). 3. TPO activity of whole-body X-ray irradiated rats (700r) was increased about double at 3hours and increased for a period of 4 days after irradiation, but after 6 days it was decreased gradually. This result is that whole-body X-ray irradiation showed dual effect on TPO activity in rat liver.

• 비파괴검사학회지
• /
• 제30권5호
• /
• pp.429-436
• /
• 2010

최근에는 T-ray(terahertz ray)를 이용한 비파괴기술이 새로운 분야로 주목을 받고 있다. 본 연구에서는 FRP 복합재료의 내재결함이나 레이업(lay-up) 특성을 검사 및 평가하기 위한 T-ray 시간영역 분광기(time-domain spectroscopy)를 활용하였으며 또한 이 T-ray 분광기의 일반적인 반사 및 투과모드를 이용하여 T-ray 이미지를 구현하였다. 특히, 2개의 톱날 인공결함이 내재한 GFRP 복합재의 평가방법을 제시하였다. CFRP 복합재료에 대해서는 T-ray 전파는 탄소섬유로 인해 진행 장해를 받는다. 이에 따라 T-ray의 전기장(E-field)의 방향과 탄소섬유 방향의 의존성을 분석하였다. 한편 인공결함인 알루미늄 테이프, 박리, 충격손상, 이물혼입 등을 T-ray를 이용하여 비파괴 검사 및 평가하였다. 이를 통해 FRP 복합재료의 T-ray비파괴평가의 적용 가능성 및 한계 등을 확인 할 수 있었다.

• Bulletin of the Korean Chemical Society
• /
• 제35권2호
• /
• pp.441-447
• /
• 2014

$AgI/AgCl/H_2WO_4$ double heterojunctions photocatalyst was prepared via deposition-precipitation followed by ion exchange method. The structure, crystallinity, morphology, chemical content and other physical-chemical properties of the samples are characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive x-ray spectra (EDX), UV-vis diffuse reflectance spectroscopy (DRS), and photoluminescence (PL). The photocatalytic activity of the $AgI/AgCl/H_2WO_4$ was evaluated by degrading methyl orange (MO) under visible light irradiation (${\lambda}$ > 400 nm). The double heterojunctions photocatalyst displayed more efficient photocatalytic activity than pure AgI, AgCl, $H_2WO_4$ and AgCl/$H_2WO_4$. Based on the reactive species and energy band structure, the enhanced photocatalytic activity mechanism of $AgI/AgCl/H_2WO_4$ was discussed in detail. The improved photocatalytic performance of $AgI/AgCl/H_2WO_4$ double heterojunctions could be ascribed to the enhanced interfacial charge transfer and the inhibited recombination of electron-hole pairs, which was in close relation with the $AgI/AgCl/H_2WO_4$ heterojunctions formed between AgI, AgCl and $H_2WO_4$.

• 한국진공학회지
• /
• 제10권1호
• /
• pp.22-26
• /
• 2001

Plasma assisted molecular beam epitaxy(PAMBE)를 사용하여 Si 기판위에 성장시킨 AlN 박막에 대하여 성장온도 및 기판의 방향성에 따른 박막의 결정성 변화를 분석하였다. Reflection high energy electron diffraction(RHEED) 패턴을 이용하여 성장 중의 결정성을 관찰하였고, 성장 후에는 X-ray diffraction(XRD), double crystal X-ray diffraction(DCXD), transmission electron microscopy/diffraction(TEM/TED)분석을 하였다. $850^{\circ}C$이상의 온도에서 Si(100)위에 성장된 AlN박막은 육방정계의 c축 방향으로 우선 배향되어 있음을 확인하였으며 Si(111)위에 성장된 AlN박막의 경우 AlN(0001)/Si(111), AlN(1100)/Si(110), AlN(1120)/Si(112)의 결정방위를 가지고 성장하였음을 확인하였다. 또한 Si(111) 기판 위에서는 전위와 적층결함 등 많은 결정결함에 의해 DCD패턴의 반치폭이 2$\theta$=$36.2^{\circ}$에서 약 3000arcsec에 이르는 등 결정성은 좋지 않았으나 AlN박막이 단결정으로 성장된 것으로 나타났다.

• 설비공학논문집
• /
• 제24권6호
• /
• pp.515-520
• /
• 2012

A daylighting system includes three parts; light collector, light transformer and light distributor. A DBLP(Double blind light pipe) daylighting system consists of a double blind light collector, a mirror duct type light transformer and a prism film light pipe distributor. The double blinds for a light collection are used to track the sun's altitude and azimuth movements throughout the day. Behind both sets of blinds is the light transformer, which is based on a rectangular cone shaped light duct. The light transformer was designed to efficiently deliver the light into the light pipe within a 30 degree radial spread for the efficient light into the distributor. In this study, DBLP system efficiency was simulated, evaluated and optimized by Tracepro as a popular ray trace light design simulation program. The results indicated that DBLP system efficiency evaluated a maximum 22.4% in case of Spring/Fall season solar noon time. While the overall average system efficiency in the morning and afternoon is evaluated about 10%.

• Journal of Chest Surgery
• /
• 제28권1호
• /
• pp.60-65
• /
• 1995

Congenital diverticula of the cardiac ventricle have been reported as arising either from the left ventricle or, rarely from both ventricles. A diverticulum arising from the right ventricle alone is very rare. Furthermore the diverticulum associated with double chambered right ventricle was extremely rare. We experienced a 62 years old female of double chambered right ventricle combined with congenital right ventricular true diverticulum. She had complained intermittent chest pain and mild dyspnea on exertion during 8 months. The chest X-ray and chest CT showed protruded abnormal density at anterolateral side of right ventricular outflow tract. Preoperative angiography demonstrated a double chambered right ventricle and a right ventricular diverticulum. In operative finding, there was found a anomalous muscle band, dividing the right ventricle into an inflow and outflow portion, and a 5x6cm sized right ventricular diverticulum arised from conus region with a stenotic orifice of 1.5cm in diameter. The diverticulum was open toward the infundibulum, and its orifice was approximately 1cm in diameter. On treatment, the diverticulum orifice was closed directly and the abnormal muscle band was resected in order to widen the right ventricular outflow tract. The postoperative result was satisfactory and good without specific complications.